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Sulfonimide lithium salt

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Sulfonimide lithium salt is a laboratory chemical compound used as a reagent or intermediate in various chemical reactions and synthesis processes. It is a white, crystalline solid with a molecular formula of (CH3)2NSO2Li. Sulfonimide lithium salt is commonly used in organic chemistry, medicinal chemistry, and materials science applications.

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Lab products found in correlation

Dimethyl sulfoxide (dmso), by Merck Group (3 mentions) Acetonitrile, by Merck Group (3 mentions) Chlorobenzene, by Merck Group (3 mentions) Pyrrole, by Merck Group (1 mentions) Ethylene glycol, by Merck Group (1 mentions) Propylene carbonate, by Merck Group (1 mentions) Sodium dodecylbenzenesulfonate, by Merck Group (1 mentions) Toluene, by Thermo Fisher Scientific (1 mentions) Hydroiodic acid, by Merck Group (1 mentions) Titanium diisopropoxidebis, by Merck Group (1 mentions) Copper iodide, by Merck Group (1 mentions) Bismuthbromide, by Merck Group (1 mentions) Bismuth iodide, by Merck Group (1 mentions) 4 tert butylpyridine 4 tbp, by Merck Group (1 mentions) 9 9 spirobifluorene spiro ometad, by Lumtec (1 mentions) Iron 2 chloride tetrahydrate, by Merck Group (1 mentions) 4 4 bipyridine, by Merck Group (1 mentions) 2 2 6 2 terpyridine, by Merck Group (1 mentions) Ammonium tetrafluoroborate, by Merck Group (1 mentions) Lithium metal, by Merck Group (1 mentions)

Spelling variants of this product

Bis(trifluoromethane)sulfonimide lithium salt (16 citations) Bis(trifluoromethane)sulfonimide lithium salt (LiTFSI (10 citations) Sulfonimide lithium salt (Li-TFSI) (2 citations)

8 protocols using sulfonimide lithium salt

1

Synthesis of Highly Porous Carbide-Derived Carbon

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Carbide derived carbon (CDC, amorphous TiC-800, specific surface area of 1470 m2 g−1, total volume of pores 0.71 cm3 g−1, volume of micro-pores 0.59 cm3 g−1 and average pore size of 0.97 nm) was obtained from Skeleton Technologies Ltd. (Tallinn, Estonia). Sodium dodecylbenzenesulfonate (NaDBS, 99%), ethylene glycol (EG, 99.8%), bis(trifluoromethane) sulfonimide lithium salt (LiTFSI, 99.95%), phosphotungstic acid hydrate (PTA, PW12O403−, reagent grade), ethanol (technical grade) and propylene carbonate (PC, 99%) were obtained from Sigma-Aldrich (Taufkirchen, Germany) and used as supplied. Pyrrole (Py, ≥98%) from Sigma-Aldrich was distilled prior to use and stored at low temperature. Milli-Q+ (deionized water, Tallinn, Estonia) was applied as a solvent.
Tran C.B., Zondaka Z., Le Q.B., Velmurugan B.K, & Kiefer R. (2021). Polypyrrole with Phosphor Tungsten Acid and Carbide-Derived Carbon: Change of Solvent in Electropolymerization and Linear Actuation. Materials, 14(21), 6302.
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2

Perovskite Solar Cell Fabrication

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Bismuth iodide (BiI3), bismuth
bromide (BiBr3), copper iodide (CuI), titanium diisopropoxide
bis(acetylacetonate) (TDBA, 75 wt % in isopropanol), dimethylsulfoxide
(DMSO), hydroiodic acid (HI, 57%), chlorobenzene (CB, extra dry, 99.8%),
acetonitrile (99.9%), 4-tert-butylpyridine (4-tBP),
and bis(trifluoromethane)sulfonimide lithium salt (LiTFSI, 99.95%)
were purchased from Sigma-Aldrich. Tris[2-(1H-pyrazol-1-yl)-4-tert-butylpyridine]cobalt(III)tri[bis(trifluoromethane)sulfonimide]
(FK209 Co(III), >98%) was purchased from Dyenamo. Dimethylformamide
(DMF), silver iodide (AgI), and toluene were purchased from Alfa Aesar.
2,2′,7,7′-Tetrakis(N,N-di-p-methoxy phenylamino)-9,9-spirobifluorene (Spiro-OMeTAD)
was purchased from Lumtec. Fluorine-doped tin(IV) oxide (FTO)-coated
glass substrates of 2 cm × 2 cm were purchased from Yingkou Opv
Tech New Energy Technology Co.
Sugathan V., Liu M., Pecoraro A., Das T.K., Ruoko T.P., Grandhi G.K., Manna D., Ali-Löytty H., Lahtonen K., Muñoz-García A.B., Pavone M, & Vivo P. (2024). Halide Engineering in Mixed Halide Perovskite-Inspired Cu2AgBiI6 for Solar Cells with Enhanced Performance. ACS Applied Materials & Interfaces, 16(15), 19026-19038.
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3

Fabrication of Lithium-Ion Solid Electrolyte

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All chemicals and solvents were used as received without further purification. Titanium foil (99.5%, 100 μm in thickness), copper foil (99.9%, 30 μm in thickness), and copper mesh were purchased from Nilaco Corporation. Iron(ii) chloride tetrahydrate (FeCl2·4H2O, 98%), ammonium tetrafluoroborate (NH4BF4, 97%), 4,4′-bipyridine, 2,2′:6′,2′′-terpyridine (98%), 1-iodohexane, bis(trifluoromethane) sulfonimide lithium salt (LiTFSI, 99.95%), and lithium metal were purchased from Sigma-Aldrich. The Li+-ion solid electrolyte was purchased from Ohara Corporation. Ethylene carbonate (EC, water content < 30 ppm) and dimethyl carbonate (DMC, water content < 30 ppm) were obtained from Kishida Chemicals. The polyvinylidene fluoride (PVDF) binder was obtained from MTI Corporation. N-Methyl-2-pyrrolidone (NMP) was obtained from J&K Chemicals. Super P carbon was obtained from TIMCAL.
Chen C., Zhang S., Zhu Y., Qian Y., Niu Z., Ye J., Zhao Y, & Zhang X. (2018). Pyridyl group design in viologens for anolyte materials in organic redox flow batteries. RSC Advances, 8(34), 18762-18770.
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4

Perovskite Solar Cell Fabrication

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Camphorsulfonic acid (CSA) (≥98.0%), dimethylformamide (DMF), dimethylsulfoxide (DMSO), 1-butanol, acetonitrile, bis(trifluoromethane)sulfonimide lithium salt, 2,2′,7,7′-Tetrakis(N,N-di-p-methoxyphenylamine)-9,9′-spirobifluorene (Spiro-OMeTAD), methylammonium iodide (MAI), and PbI2 were acquired from Sigma-Aldrich. Titanium diisopropoxide bis(acetylacetonate) (TAA) and cobalt dopant FK209 TFSI salt were acquired from Merck.
Wincukiewicz A., Wierzyńska E., Bohdan A., Tokarczyk M., Korona K.P., Skompska M, & Kamińska M. (2022). Enhanced Performance of Camphorsulfonic Acid-Doped Perovskite Solar Cells. Molecules, 27(22), 7850.
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5

Halloysite-Nickel Hybrid Anode Protocol

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Esan Eczacıbaşı Industrial Raw Materials Company supplied halloysite. Sulfuric acid (H2SO4, 98%), nickel chloride hexahydrate (NiCl2·6H2O, 99.9%), ammonium chloride (NH4Cl, 99.5%), ammonia solution (NH3·H2O, 28 wt.%), anhydrous ethanol, lithium nitrate (LiNO3, 99.99%), bis(trifluoromethane) sulfonimide lithium salt (LiTFSI, anhydrous, 99.99%), N‐methyl‐2‐pyrrolidone (NMP, anhydrous, 99.5%), polyvinylidene fluoride (PVdF), 1, 2‐dimethoxyethane (DME, anhydrous, 99.5%), sulfur powder, and 1, 3‐dioxolane(DOL, anhydrous, 99.8%) were purchased from Sigma–Aldrich. All reagents and materials were utilized without any further treatments or purifications.
Elibol M.K., Jiang L., Xie D., Cao S., Pan X., Härk E, & Lu Y. (2023). Nickel Oxide Decorated Halloysite Nanotubes as Sulfur Host Materials for Lithium–Sulfur Batteries. Global Challenges, 7(7), 2300005.
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6

Perovskite Solar Cell Precursor Materials

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Formamidinium iodide (FAI, 99.5%), methylammonium iodide (MAI, 99.5%), and methylammonium bromide (MABr, 99.5%) were obtained from Xi'an Polymer Light Technology Corp, China. Lead iodide (PbI2, 99.99%), lead bromide (PbBr2, 99%), and cesium iodide (CsI, 99%) were purchased from TCI. Bis(trifluoromethane) sulfonimide lithium salt (Li-TFSI, 99.95%), anhydrous dimethyl sulfoxide (DMSO, 99.9%), anhydrous N,N-dimethylformamide (DMF, 99.8%), 4-tert-butylpyridine (98%), anhydrous chlorobenzene (CB, 99.8%), anhydrous acetonitrile (99.8%), anhydrous 1-butanol (99.8%), and SnCl2·2H2O (99.995%) were received from Sigma-Aldrich. K2SnO3·3H2O (99.5%), urea (99.995%), YCl3·6H2O (99.99%), LaCl3·6H2O (99.99%), ScCl3·6H2O (99.9%), and ethylene glycol (EG, 99%) were obtained from Aladdin. All the chemicals were used as received without further purification. Deionized water (resistivity > 18 MΩ) was obtained through a Millipore water purification system. Prepatterned fluorine-doped tin oxide-coated (FTO) substrates with a sheet resistance of 14 Ω sq−1 were purchased from Pilkington.
Guo Q., Wu J., Yang Y., Liu X., Lan Z., Lin J., Huang M., Wei Y., Dong J., Jia J, & Huang Y. (2019). High-Performance and Hysteresis-Free Perovskite Solar Cells Based on Rare-Earth-Doped SnO2 Mesoporous Scaffold. Research, 2019, 4049793.
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7

Perovskite Solar Cell Fabrication Protocol

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Cesium iodide (CsI, 99.998%), lead bromide (PbBr2, 99.999%), lead iodide (PbI2, 99.999%), phenethylammonium bromide (PEABr, 99.5%), and Spiro‐OMeTAD were purchased from Xi'an Polymer Light Technology Corp. Cesium bromide (CsBr, 99.9%) and SnO2 colloid precursor (tin (IV) oxide) were purchased from Alfa‐Aesar. Dimethyl sulfoxide (DMSO, 99.8%), bis‐(trifluoromethane) sulfonimide lithium salt (LiTFSI, 96% purity), 4‐tBP (96% purity), methanol (99.8%), chlorobenzene (99.8%), 2‐methoxyethanol (99.8%), ethanolamine (99.5%), and zinc acetate dihydrate (Zn(CH3COO)2 · 2H2O, 99.0%) were purchased from Sigma‐Aldrich. Tris(2‐(1H‐pyrazol‐1‐yl)‐4‐tert‐butylpyridine)‐cobalt(III)Tris(bis‐(trifluoromethylsulfonyl)imide)) (FK209) was purchased from Dyesol. All the materials were used without purification.
He J., Su J., Lin Z., Ma J., Zhou L., Zhang S., Liu S., Chang J, & Hao Y. (2021). Enhanced Efficiency and Stability of All‐Inorganic CsPbI2Br Perovskite Solar Cells by Organic and Ionic Mixed Passivation. Advanced Science, 8(17), 2101367.
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8

Synthesis and Stability of Perovskite Solar Cells

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Cs 2 CO 3 (99.9%), octadecene (ODE, 90%), oleic acid (OA, 90%), oleylamine (OlAm, technical grade, 70%), lead(II) iodide (PbI 2 , 99%), hexane (≥95%), methyl acetate (MeOAc, anhydrous), ethyl acetate (EA, 97%), titanium diisopropoxide bis(acetylacetonate) (TDBA, 75 wt% in isopropanol), bis(trifluoro-Fig. 6 Stability of unencapsulated PSCs with 135@NCs, 150@NCs, or methane)sulfonimide lithium salt (Li-TFSI, 99.95%), chlorobenzene (extra dry, 99.8%), acetonitrile (99.9%), and 4-tertbutyilpyridine (4-tBP) were purchased from Sigma-Aldrich. 2,2′,7,7′-Tetrakis[N,N-di(4-methoxyphenyl)amino]-9,9′-spirobifluorene (Spiro-OMeTAD, 99%) and tris[2-(1H-pyrazol-1-yl)-4tert-butylpyridine]cobalt(III)tri[bis-(trifluoromethane) sulfonimide] (FK209, >98%) were purchased from Lumtec and Dyenamo, respectively. All chemicals were used without further purification.
Matuhina A ., Grandhi GK ., Liu M ., Smått JH ., Viswanath NSM ., Ali-Löytty H ., Lahtonen K , & Vivo P . (2021). Octahedral distortion driven by CsPbI3 nanocrystal reaction temperature - the effects on phase stability and beyond. Nanoscale, 13(33).
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