Reference materials were used for the validation and stability analysis. All chemicals and solvents used were of analytical grade. Methanol was purchased from Fisher Chemicals (Loures, Portugal), formic acid was purchased from Merck (Darmstadt, Germany), and ethanol was purchased from Merck (Darmstadt, Germany). 4-methylmethcathinone (mephedrone), butylone, pentylone, eutylone, ephylone, 4-methyl-α-ethylaminopentiophenone (4-MEAPP), 4-methoxyamphetamine (PMA), para-methoxymethamphetamine (PMMA), deschloroketamine (DCK), mephedrone-D3, butylone-D3, 3,4-methylenedioxyamphetamine-D5 (MDA-D5), and ketamine-D4 were purchased from Cerilliant (Texas, USA). 2-fluorodechloroketamine (2-FDCK) was purchased from Cayman Chemicals (Ann Arbor, MI, USA).
Mephedrone d3
Manufactured by Cerilliant
Sourced in United States
Mephedrone-d3 is a deuterated (containing three deuterium atoms) analog of the synthetic stimulant mephedrone. It is used as an internal standard or reference material in analytical chemistry applications.
Automatically generated - may contain errors
Lab products found in correlation
Methanol, by Thermo Fisher Scientific (2 mentions)
Mephedrone, by Cerilliant (2 mentions)
Methylone, by Cerilliant (2 mentions)
Methcathinone, by Cerilliant (2 mentions)
Methylone d3, by Cerilliant (2 mentions)
Para methoxymethamphetamine, by Cerilliant (1 mentions)
Ketamine d4, by Cerilliant (1 mentions)
Ethanol, by Merck Group (1 mentions)
Formic acid, by Merck Group (1 mentions)
Pseudoephedrine, by Cerilliant (1 mentions)
Hydroxybupropion, by Cerilliant (1 mentions)
Methylphenidate, by Cerilliant (1 mentions)
Methedrone, by Cerilliant (1 mentions)
Amphetamine d11, by Cerilliant (1 mentions)
Mda d5, by Cerilliant (1 mentions)
Mdea d5, by Cerilliant (1 mentions)
Methylphenidate d9, by Cerilliant (1 mentions)
Mdma d5, by Cerilliant (1 mentions)
Bupropion d9, by Cerilliant (1 mentions)
Hydroxybupropion d6, by Cerilliant (1 mentions)
3 protocols using mephedrone d3
1
Analytical Validation of Novel Psychoactive Substances
2
Comprehensive Synthetic Cathinone Analysis
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The stock standard solutions of amphetamine (A), methamphetamine (MA), phenylpropanolamine (PHPR), ephedrine, pseudoephedrine (PSE), 3,4-methylenedioxyamphetamine (MDA), 3,4-methylenedioxymethamphetamine (MDMA), 3,4-methylenedioxy-N-ethylamphetamine (MDEA), phentermine (PHRM), methylphenidate (MPHD), bupropion, hydroxybupropion, methcathinone (ephedrone), methedrone (PMMC), mephedrone (4-MMC), methylone (MDMC), ethylone (MDEC), 3,4-methylenedioxypyrovalerone (MDPV), and alpha-pyrrolidinopentiophenone (alpha-PVP) at a concentration of 1.0 mg mL -1 for each analyte in methanol were purchased from Cerilliant (Round Rock, Texas, USA). Stock standard solutions of the internal standards (ISTDs), namely amphetamine-d11, methamphetamine-d11, ephedrine-d3, pseudoephedrine-d3, norpseudoephedrine-d3, MDA-d5, MDMA-d5, MDEA-d5, phentermine-d5, methylphenidate-d9, bupropion-d9, hydroxybupropion-d6, mephedrone-d3, and methylone-d3, were also purchased from Cerilliant (Round Rock, TX, USA) at a concentration of 100 µg mL -1 in methanol.
3
Quantification of Novel Psychoactive Substances
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Cathinone, methcathinone, methylone, N-ethylcathinone, buphedrone, mephedrone, 4-methylethcathinone, α-pyrolidinovarophenone (PVP), MDPV, and naphyrone (1 mg/mL), and internal standards MDPV-d8, mephedrone-d3, methylone-d3, and naphyrone-d5 (100 µg/mL) were obtained from Cerilliant (Round Rock, TX, USA). Solid phase extraction (SPE) cation exchange cartridges Strata Drug-X B 60 mg/3 mL were from Phenomenex (Torrance, CA, USA). Glacial acetic acid, acetonitrile, ammonium hydroxide, and formic acid were acquired from Pharmco-Aaper (Shelbyville, KY, USA). Methanol, dichloromethane, and isopropanol were acquired from Fisher Scientific (Pittsburgh, PA, USA). All solvents used in the extraction were high performance liquid chromatography (HPLC) grade and in the chromatographic instrument were liquid chromatography-mass spectrometry (LC-MS) grade. Quantisal buffer was obtained from Immunalysis Corp. (Pomona, CA, USA) and Oral-Eze buffer from Capitol Vial, Inc. (Auburn, AL, USA). Neat drug-free OF was obtained from healthy volunteers by spitting into a Corning® polypropylene 50 mL tube (Fisher Scientific).
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