X pert pro mpd

All utilized solvents and materials that were commercially available, has been purchased from Merck and Fluka and used as soon as opening. FT-IR (Fourier transform infrared spectroscopy), UV–Vis (Ultraviolet visible spectroscopy), EDS, Map and FESEM (Energy dispersive spectroscopy) (Field emission scanning electron microscopy), AFM (Atomic force microscopy), 2D Fluorescence Microscopy, ¹H-NMR (Nuclear magnetic resonance), PXRD (Powder X_Ray diffraction), DLS and Zeta potential (Dynamic light scattering), AST and ALT liver index, and TEM (Transmission electron microscopy) analysis have been performed by flowing devices respectively: Unicam Maston 1000 FT-IR spectrophotometer (room temperature, 400–4000 cm⁻¹, KBr pellets), Carrying 100 Bio Varian spectrophotometer (quartz cells,10 mm path length), MIRA3 TESCAN, ARA-AFM, FACSCalibur (BD, Germany), Bruker FT-NMR 500 MHZ spectrometer (¹H-NMR of L and PdL, DMSO-d₆ and CDCl₃), PANalytical company X’Pert Pro MPD, HORIBA SZ-100, Selectra pro autoanalyzer spectrophotometer, and ZEISS em900.

The synthesized Cu foam@Co₃O₄ NWs and Cu@Co₃O₄@Ag SERS substrate were characterized by SEM (JEOL, Japan, 15 kV), XRD (X’ Pert PRO MPD, The Netherlands, 5°/min, 10°–90°), Raman spectra were recorded from a Horiba JY iHR550 (France) system with excitation wavelength at 532 nm (~1.5 mW). During measurements, the laser beam was focused on a spot of 2 μm diameter by a microscope objective with a magnification of 50×. The contact angle is measured by the SINDIN contact angle measuring instrument (SDC-100, Qingdao, China), TEM and HRTEM images were acquired using a JEM-2100 electron microscopy (JEOL), with an Operating Voltage at 200 kV.