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2 protocols using n pentanol

1

Pyrene Fluorescence Probe in Ionic Liquids

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3-methylpyridinium (97%), 1-bromododecane (97%), 1-bromotetradecane (97%), 1-bromohexadecane (97%), toluene (99%), ethyl acetate (97%), ethanol (99%), n-propanol (99%), n-butanol (99%), and n-pentanol (99%), pyrene (97%), lithium bromide (LiBr analytical reagents, ≥99%), sodium bromide (NaBr analytical reagents, ≥99%), magnesium bromide (MgBr2 analytical reagents, ≥99%), was obtained from Macklin Reagent. Dilute stock solutions of pyrene (1 × 10−3 mol L−1) were prepared by dissolving pyrene in methanol in a volumetric flask. Samples for UV were prepared as follows: equivalent amounts of probe stock solutions were transferred into test tubes and evaporated with nitrogen. Then the ILs solution was added.
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2

Synthesis of Silica-Coated Platinum Nanoparticles

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Polyvinylpyrrolidone (PVP, M.w.: 40,000 Da) and tris‐(hydroxymethyl)aminomethane were bought from Sigma Aldrich. N‐pentanol (99%), tetrabutylorthosilicate (TBOS, ≥98%), and hydrofluoric acid (HF) were provided by Shanghai Macklin Biochemical Co., Ltd. Trisodium citrate dihydrate was purchased from Sinopharm Chemical Reagent Co., Ltd. (3‐chloropropyl) trimethoxysilane (CPTMS, ≥98%) was purchased from Acros. Dopamine hydrochloride (99.9%) was purchased from Adamas‐beta reagent co., Ltd. Hexachloroplatinic (IV) acid hexahydrate (H2PtCl6·6H2O) and sodium borohydride (NaBH4) were purchased from Beihua Fine Chemicals. Aqueous ammonia (NH3·H2O, 25 ∼ 28%), absolute ethanol (99.5%), and methylene blue (MB) were obtained from Beijing Chemical Reagent Company. The water with a resistivity of higher than 18.2 MΩ·cm was produced by a Millipore Milli‐Q Plus 185 purification system.
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