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Cryoprobe 5 mm txi probe of z gradient

Manufactured by Bruker

The CryoProbe: 5 mm TXI probe of Z-Gradient is a specialized lab equipment designed for nuclear magnetic resonance (NMR) spectroscopy. It features a 5 mm triple-resonance (1H, 13C, 15N) probe with z-axis gradient coils. The core function of this probe is to provide enhanced sensitivity and resolution in NMR experiments by maintaining the sample at cryogenic temperatures.

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2 protocols using cryoprobe 5 mm txi probe of z gradient

1

NMR Spectroscopy of Oxidized Peptides

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Concentrations of peptide samples were obtained using ultraviolet absorbance of Tyrosine (ε= 1450) in 8 M urea. Peptide Y-MetOx (YGGSAAEAFAKAM(ox)AR-NH2) was dissolved in deuterated methanol (3 mM). F-MetOx (YGGSAAEAFAKAM(ox)AR-NH2) was dissolved in acidic (pH 3.5) D2O, taken at 4°C. 1H-1H ROESY experiments (mixing time = 200 ms) were performed on a Bruker 700 MHz spectrometer with a CryoProbe: 5 mm TXI probe of Z-Gradient. 1H experiments comparing control peptide, A-MetOx to F-MetOx in MeOD were performed on a Bruker Advance III HD 500 MHz instrument with a 5 mm Prodigy TCI cryoprobe with z-axis gradients. Data was processed and analyzed using Bruker Topspin 3.2.
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2

NMR Spectroscopy of Oxidized Peptides

Check if the same lab product or an alternative is used in the 5 most similar protocols
Concentrations of peptide samples were obtained using ultraviolet absorbance of Tyrosine (ε= 1450) in 8 M urea. Peptide Y-MetOx (YGGSAAEAFAKAM(ox)AR-NH2) was dissolved in deuterated methanol (3 mM). F-MetOx (YGGSAAEAFAKAM(ox)AR-NH2) was dissolved in acidic (pH 3.5) D2O, taken at 4°C. 1H-1H ROESY experiments (mixing time = 200 ms) were performed on a Bruker 700 MHz spectrometer with a CryoProbe: 5 mm TXI probe of Z-Gradient. 1H experiments comparing control peptide, A-MetOx to F-MetOx in MeOD were performed on a Bruker Advance III HD 500 MHz instrument with a 5 mm Prodigy TCI cryoprobe with z-axis gradients. Data was processed and analyzed using Bruker Topspin 3.2.
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