UV/Vis spectra were obtained on an Agilent (USA) Cary 300 UV-visible spectrophotometer with a path length of 10 mm. 1H and 2D- (gCOSY, gHSQC, and gHMBC) NMR spectral data were measured on an Agilent (USA) 600 MHz NMR spectrometer equipped with a cold probe, and the chemical shifts were recorded as δ values (ppm). Low-resolution HPLC/MS data was measured using an Agilent 6120 single quadrupole LC/MS system. High-resolution ESI-MS data was obtained using an Agilent iFunnel 6550 Q-TOF instrument fitted with an electrospray ionization (ESI) source coupled to an Agilent (USA) 1290 Infinity HPLC system. Flash column chromatography was carried out on Waters Sep-Pak® Vac 35cc (10g) C18 or silica cartridges. The isolation of metabolites was performed using an Agilent (USA) Prepstar HPLC system with an Agilent (USA) Polaris C18-A 5 μm (21.2 × 250 mm) column, a Phenomenex (USA) Luna C18(2) (100Å) 10 μm (10.0 × 250 mm) column, and an Agilent (USA) Phenyl-Hexyl 5 μm (9.4 × 250 mm) column.
Ifunnel 6550 q tof instrument
Manufactured by Agilent Technologies
Sourced in United States
The IFunnel 6550 Q-TOF instrument is a high-resolution mass spectrometer designed for analytical applications. It employs quadrupole time-of-flight (Q-TOF) technology to provide accurate mass measurements and detailed structural information about analytes. The instrument features an IFunnel ion source and advanced optics to enhance sensitivity and resolution.
Automatically generated - may contain errors
Lab products found in correlation
Prepstar hplc system, by Agilent Technologies (2 mentions)
1290 infinity hplc system, by Agilent Technologies (2 mentions)
Cary 300 uv visible spectrophotometer, by Agilent Technologies (2 mentions)
Sep pak vac 35cc 10g c18, by Waters Corporation (2 mentions)
Polaris c18 a 5 μm 21.2 250 mm column, by Phenomenex (2 mentions)
Luna c18 2 100 10 μm 10.0 250 mm column, by Agilent Technologies (2 mentions)
Phenyl hexyl 5 μm 9.4 250 mm column, by Agilent Technologies (2 mentions)
6120 single quadrupole lc ms system, by Agilent Technologies (2 mentions)
600 mhz nmr spectrometer, by Agilent Technologies (2 mentions)
2 protocols using ifunnel 6550 q tof instrument
1
Analytical Characterization of Metabolites
2
Analytical Characterization of Metabolites
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UV/Vis spectra were obtained on an Agilent (USA) Cary 300 UV-visible spectrophotometer with a path length of 10 mm. 1H and 2D- (gCOSY, gHSQC, and gHMBC) NMR spectral data were measured on an Agilent (USA) 600 MHz NMR spectrometer equipped with a cold probe, and the chemical shifts were recorded as δ values (ppm). Low-resolution HPLC/MS data was measured using an Agilent 6120 single quadrupole LC/MS system. High-resolution ESI-MS data was obtained using an Agilent iFunnel 6550 Q-TOF instrument fitted with an electrospray ionization (ESI) source coupled to an Agilent (USA) 1290 Infinity HPLC system. Flash column chromatography was carried out on Waters Sep-Pak® Vac 35cc (10g) C18 or silica cartridges. The isolation of metabolites was performed using an Agilent (USA) Prepstar HPLC system with an Agilent (USA) Polaris C18-A 5 μm (21.2 × 250 mm) column, a Phenomenex (USA) Luna C18(2) (100Å) 10 μm (10.0 × 250 mm) column, and an Agilent (USA) Phenyl-Hexyl 5 μm (9.4 × 250 mm) column.
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