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2 protocols using iodotrimethylsilane

1

Synthesis of Colloidal Nanocrystals

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Cs2CO3 (99.9%), octadecene (ODE, 90%), oleic acid (OA, 90%), oleylamine (OlAm, technical grade, 70%), titanium di-isopropoxide bis(acetylacetonate) (TDBA) 75 wt.% in isopropanol, Chlorotrimethylsilane (TMS-Cl, ≥99%), bromotrimethylsilane (TMS-Br, purum, ≥97.0% (AT)), and iodotrimethylsilane (TMS-I, 97.0%) were purchased from Sigma-Aldrich (St. Louis, MO, USA). All chemicals were used without further purification.
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2

Cesium-lead Halide Nanocrystal Synthesis

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Cesium carbonate (Cs2CO3, 99.9%), lead (II) acetate trihydrate (Pb(OAc)2 · 3H2O, 99.999%), benzoyl chloride (99%), benzoyl bromide (97%), and iodotrimethylsilane (97%), oleic acid (OA, technical grade, 90%), oleylamine (OAm, technical grade, 70%), 1-octadecene (ODE, technical grade, 90%) were purchased from Sigma-Aldrich. Toluene, hexanes, and ethyl acetate were purchased from Fisher Scientific. All chemicals were used as received without further purification.
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