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Atr accessory

Manufactured by Specac
Sourced in United Kingdom

The ATR accessory is a device used in infrared spectroscopy to analyze the surface of a sample. It allows for the collection of infrared spectra without the need for sample preparation.

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5 protocols using atr accessory

1

ATR-FTIR Analysis of Polymers and Amorphous Solids

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The IR spectra of bulk polymers, drug and ASDs were collected in the attenuated total reflectance (ATR) mode using a Bruker Vertex 70 FTIR spectrometer (Billerica, MA) equipped with a Golden Gate ATR accessory (Specac, Orpington, Kent, UK). The spectrum of each sample was the average of triplicate runs of 32 scans and a resolution of 4 cm−1. The data were analyzed using OPUS software (version 7.2, Bruker, Billerica, MA).
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2

Solid and Solution FTIR Analysis of DF Na

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A FTIR spectrometer (Tensor 27; Bruker Optics Ltd., Coventry, UK) with a Specac™ multi-bounce (25 reflection, 45º, refractive index of 2.40) ATR accessory (Specac Ltd., Orpington, UK) -ZnSe (7.2 × 1.0 cm 2 ), was used to collect the reference spectra for the solid form of DF Na (ethanolic paste), DF Na in PG (200 mg/mL) and DMSO (100 mg/mL). The ethanol paste of DF Na was prepared by mixing a minimal amount of ethanol with DF Na powder. This paste was then spread evenly on the ZnSe crystal and allowed to dry for about half an hour before collecting spectra [7] .
For analysis of solutions, an aluminum slab was used to form a reservoir using vacuum grease. For each sample 32 scans were collected with a resolution of 4 cm -1 in the range of 4000 cm -1 to 600 cm -1 . The spectra collected were analysed using Opus software version 6.0 (Bruker Optics Ltd., Coventry, UK) and OriginPro 9.0.0 (OriginLab Corp., Northampton, MA, US).
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3

FTIR Spectroscopy using ATR Technique

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Fourier-transform infrared (FTIR) measurements were carried out in attenuated total reflectance (ATR) mode. The infrared spectra of the samples were collected using a Bruker IFS 66/S spectrophotometer (Bruker Optics Ltd., UK), fitted with a Golden Gate ATR accessory from Specac Ltd. (UK). Measurements were carried out over a spectral range of 4,000 to 550 cm -1 with a total of 16 scans acquired at a resolution of 4 cm -1 .
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4

ATR FT-IR Spectroscopic Analysis

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ATR FT‐IR spectra were recorded on a Perkin‐Elmer Spectrum GX spectrometer. The ATR accessory (supplied by Specac Ltd., UK) contained a diamond crystal. A total of 16 scans for each sample were taken with a resolution of 4 cm−1. All spectra were recorded at 21 °C over the wavelength interval between 4000 and 650 cm−1.
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5

FTIR Spectroscopy Using Attenuated Total Reflectance

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Fourier transform infrared
(FTIR) spectra were collected in the wavenumber range of 600–4000
cm–1 using attenuated total reflectance technique
(PerkinElmer Spectrum 100 equipped with a Specac ATR accessory). 16
scans were collected at a resolution of 2 cm–1 at
room temperature.
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