Chemicals and materials were purchased from the following vendors. Fmoc-L-Lys(Boc)-OH (FAA1125, Iris Biotech); polystyrene-Me-NH2 resin (100–200 mesh; BR-1000C, Iris Biotech); dichloromethane (L13089.AP, VWR); methanol (20834.291, VWR); dimethylformamide (210585000, VWR); acetonitrile (K981-1L, VWR); Fmoc-AHX-OH (045380, Fluorochem); 4-pentynoic acid (164204, Fluorochem); 1-hydroxybenzotriazole hydrate (M02875, Fluorochem); N,N-diisopropylcarbodiimide (132050, Fluorochem); 2,6-dimethylbenzoic acid (A15014, Alfer Aesar); diethylamine (AB182463, ABCR), trifluoroacetic acid (AB212435, ABCR) and syringe reactors (V050PE063, Multi Syn Tech).All purifications were carried out using a Jasco preparative reversed-phase high-performance liquid chromatography (HPLC) system, equipped with a RP-C18-column and an applied flow rate of 20 mL/min. Peak detection was carried out at 210 nm. High-resolution mass spectrometry (HRMS) analyses were performed at a Bruker μTOF ESI-Spectrometer using the direct flow-injection method.
Fmoc l lys boc oh
Manufactured by Iris Biotech
Sourced in Germany
Fmoc-L-Lys(Boc)-OH is a protected amino acid used in solid-phase peptide synthesis. It serves as a building block for the construction of peptide and protein structures.
Automatically generated - may contain errors
Lab products found in correlation
Methanol, by Avantor (1 mentions)
Acetonitrile, by Avantor (1 mentions)
Dimethylformamide, by Avantor (1 mentions)
N n diisopropylcarbodiimide, by Fluorochem (1 mentions)
Ethanol, by Merck Group (1 mentions)
Acetonitrile, by Merck Group (1 mentions)
Dichloromethane, by Merck Group (1 mentions)
Dimethylformamide, by Merck Group (1 mentions)
Trifluoroacetic acid tfa, by Merck Group (1 mentions)
Triisopropylsilane tips, by Thermo Fisher Scientific (1 mentions)
N methylmorpholine, by Thermo Fisher Scientific (1 mentions)
N n n n tetramethyl o 1h benzotriazol 1 yl uronium hexafluorophosphate hbtu, by Iris Biotech (1 mentions)
2 protocols using fmoc l lys boc oh
1
Synthesis and Characterization of Peptide Derivatives
2
Peptide Synthesis with Fmoc Chemistry
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Ultrapure water (Milli-Q, ρ >18 MΩ⋅cm) was used in all the experiments. Acetonitrile (ACN), dichloromethane (DCM), dimethylformamide (DMF) and ethanol (EtOH) were obtained from Sigma-Aldrich and were used without further purification. The synthesis of all peptides required N,N,N′,N′-Tetramethyl-O-(1H-benzotriazol-1yl)uronium hexafluorophosphate (HBTU) (Iris Biotech GmbH, Germany), acetic anhydride and piperidine (Sigma-Aldrich, Germany) and N-methylmorpholine (NMM), Nmethylpyrrolidinone (NMP) (Alfa Aesar, Haverhill, MA, USA) as reagents. Fmoc-L-Cys (Trt)-OH, Fmoc-L-Lys(Boc)-OH, Fmoc-L-Gly-OH, Fmoc-L-Thr(tBu)-OH and Fmoc-L-Arg(Pbf)-OH were obtained from Iris Biotech GmbH (Germany). Fmoc-L-Ala-Wang resin (100-200 mesh), Fmoc-L-Arg(Pbf)-Wang resin (100-200 mesh) and Fmoc-L-Asn(Trt)-OH were obtained from Novabiochem (Germany). Trifluoroacetic acid (TFA) was purchased from Sigma Aldrich (Germany) and triisopropylsilane (TIPS) from Alfa Aesar (Haverhill, MA, USA).
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