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Micro melting point apparatus

Manufactured by Thermo Fisher Scientific
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The Micro-melting point apparatus is a laboratory instrument used to determine the melting point of small samples. It provides accurate and precise melting point measurements for a variety of materials, including organic compounds, pharmaceuticals, and polymers. The instrument features a microscope and a heated stage to observe and record the melting behavior of the sample.

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Lab products found in correlation

Eca 500 spectrometer, by JEOL (1 mentions) Si gel 60, by Merck Group (1 mentions) Silica gel 60 f254, by Merck Group (1 mentions) Silica gel 60, by Macherey-Nagel (1 mentions)

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Melting point apparatus

2 protocols using micro melting point apparatus

1

Analytical Techniques for Chemical Characterization

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Thin layer chromatography (TLC) analysis was carried out on pre-coated Si-gel plates (Merck Kieselgel 60 F254), and the UV lamp of Spectroline, ENF-240 C/F model was used to see the spot in TLC. VLC was carried out using Merck Si-gel 60. Melting points were determined on a Fisher Jhons micro-melting point apparatus and were uncorrected. UV-Vis and IR spectra were measured with Beckman DU-7000 and Varian 2000 FTIR spectrophotometers, respectively. 1 H-NMR spectrum was recorded with a JEOL ECA 500 spectrometer, operating at 500.00 MHz and 13 C-NMR operating at 125 MHz.
Suhartati T., Epriyanti E., Borisha I., Yandri Y., Suwandi J.F., Yuwono S.D., Qudus H.I., & Hadi S. (2020). In Vivo Antimalarial Test of Artocarpin and in vitro Antimalarial Test of Artonin M Isolated from Artocarpus. Revista de Chimie, 71(5), 400-408.
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2

Purification and Characterization of Organic Compounds

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Commercially available reagents and solvents were used without further purification. Reactions were monitored by thin-layer chromatography (plates coated with Silica gel 60 F254 from Merck). Silica gel 60 (70-230 mesh from Macherey-Nagel) was used for flash chromatography.
Melting points were measured on a Fisher micromelting point apparatus and are uncorrected.
Meguellati A., Ahmed-Belkacem A., Nurisso A., Yi W., Brillet R., Berqouch N., Chavoutier L., Fortuné A., Pawlotsky J.M., Boumendjel A, & Peuchmaur M. (2016). New pseudodimeric aurones as palm pocket inhibitors of Hepatitis C virus RNA-dependent RNA polymerase. European journal of medicinal chemistry, 115.
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