Acryloyl chloride

Manufactured by Fujifilm

Sourced in Japan

Acryloyl chloride is a chemical compound used in various laboratory applications. It is a colorless, pungent liquid that is highly reactive and serves as a precursor for the synthesis of other compounds. The core function of acryloyl chloride is to provide a reactive group that can be used in chemical reactions, particularly in the preparation of polymers and other materials.

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Lab products found in correlation

3 protocols using acryloyl chloride

Fabrication of Fluorinated Polymer Nanocomposites

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The
material 2-(perfluorooctyl)ethyl
acrylate (FAC₈) was provided by Daikin Industries Co.,
Ltd. and was distilled under vacuum before polymerization. The material
2,2′-azobis(isobutyronitrile) (AIBN, Wako) was recrystallized
from methanol. Dopamine hydrochloride (Sigma-Aldrich) and acryloyl
chloride (Wako) were used as received. Triethylamine (Wako) and methanol
(MeOH, Wako) were distilled before use. Hexafluoroisopropanol (HFIP)
and dichloropentafluoropropanes (HCFC-225s, a mixture of 225ca, CF₃CF₂CHCl₂, and 225cb, CCl₂FCF₂CHClF) were obtained from Wako Pure Chemical Industries
and Asahi Glass Co., respectively. Halloysite nanotubes (HNTs) with
external diameter of 30–70 nm and length of 1–3 μm
were purchased from Sigma-Aldrich.

Ma W., Ameduri B, & Takahara A. (2020). Molecular Aggregation Structure and Surface Properties of Biomimetic Catechol-Bearing Poly[2-(perfluorooctyl)ethyl acrylate] and Its Application to Superamphiphobic Coatings. ACS Omega, 5(14), 8169-8180.

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Synthesis and Characterization of Multifunctional Polymer Conjugates

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Tetra‐poly(ethyl glycol)‐amine (Sunbright PTE‐050PA; Mn, 5328 g/mol) was purchased from NOF Corporation (Tokyo, Japan). N,N,N′,N′‐tetramethylethylenediamine (TEMED), dichloromethane, acryloyl chloride, triethylamine, ammonium persulfate (APS), hydrochloric acid, methanol, and diethyl ether were purchased from Wako Pure Chemical Industries (Osaka, Japan). Dimethyl sulfoxide, 2‐morpholineoethanesulfonic acid and 4‐dimethylaminopyridine (DMAP) were obtained from Nacalai Tesque (Kyoto, Japan). Dextran with a weight‐averaged molecular weight of 40 000 (Dex), diethylenetriaminepentaacetic acid (DTPA) anhydride, manganese chloride, first generation polypropylenimine tetramine dendrimer (DAB‐Am‐4), and rhodamine 6G were purchased from Sigma‐Aldrich (St. Louis, Missouri). Water was purified with a Milli‐Q apparatus (Millipore, Bedford, Massachusetts). A detailed materials preparation protocol has been published previously.16, 17, 18

Eguchi Y., Murayama S., Kanamoto H., Abe K., Miyagi M., Takahashi K., Ohtori S, & Aoki I. (2019). Minimally invasive manganese‐enhanced magnetic resonance imaging for the sciatic nerve tract tracing used intra‐articularly administrated dextran–manganese encapsulated nanogels. JOR Spine, 2(2), e1059.

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Preparation of Functionalized Porous α-Alumina

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The porous α-alumina porous support (o.d. of 1.9–2.3 mm, average pore diameter of about 150 nm) was supplied by AIST (Japan). Tetraethyl orthosilicate (TEOS; >95.0%), HCl (35%), acryloyl chloride (>98.0%), acrylic acid (>98.0%), ammonium peroxodisulfate (APS; >98.0%), toluene (>95%), tetrahydrofuran (THF; >99.5%), acetic acid (>99.7%), L-lactic acid (85.0%–92.0%), phenol (>99.0%), 0.2 mol/L HCl, and 0.2 mol/L sodium hydroxide aqueous solution were purchased from FUJIFILM Wako Pure Chemical Corp., Osaka, Japan. 4-(4,6-Dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride (>95.0%), ethanol (>99.5%), methanol (>99.8%), sodium tetraborate decahydrate (99.5–101.0%), disodium hydrogen phosphate dodecahydrate (>99.0%), and sodium dihydrogen phosphate dihydrate (99.0–102.0%) were purchased from Kanto Chemical Co., Ltd., Tokyo, Japan. 3-Aminopropyltrimethoxysilane (APTMS; >96.0%) was purchased from Tokyo Chemical Industry Co., Ltd., Tokyo, Japan. Sodium acetate (>98.0%) was purchased from Nacalai Tesque Inc., Kyoto, Japan. All chemicals were used without purification. Water was obtained from a water purification system (WG-204, Yamato Co., Tokyo, Japan).

Sato T., Makino K., Tamesue S., Ishiura G, & Itoh N. (2023). Preparation and Permeation Properties of a pH-Responsive Polyacrylic Acid Coated Porous Alumina Membrane. Membranes, 13(1), 82.

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