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2 protocols using 6 methylhept 5 en 2 one

1

Analysis of Volatile Organic Compounds

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Chemical standards of acetone, butane-2,3-dione, butan-2-one, thiophene, dimethyl disulfide, hexanal, heptan-4-one, heptan-2-one, 2-pentylfuran, dimethyl trisulfide, 6-methylhept-5-en-2-one, benzaldehyde, octanal, d-limonene, trans-3-octen-2-one, linalool, 4-methylphenol, 1,3-di-tert-butylbenzene, internal standard (4-methylpentan-2-ol), and sodium chloride (NaCl, ≥99.5%) were supplied by Sigma-Aldrich (Saint Louis, MO, USA). MilliQ water (Millipore, Bedford, MO, USA) was used for the preparation of standards. Hydrochloric acid (HCl, 37%) was purchased from Chempur (Piekary Śląskie, Poland). The 75-μm carboxen/polydimethylsiloxane (CAR/PDMS) (stable flex) solid-phase microextraction (SPME) fibers were purchased from Supelco (Bellefonte, PA, USA).
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2

Synthetic standards for analytical chemistry

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The following synthetic standards were purchased from Sigma-Aldrich and tested in the concentration 5×10-3 µg µL-1: methyl (E)-hex-3-enoate, methyl (E)-hex-2-enoate, 6-methylhept-5-en-2-one, ethyl hexanoate, ethyl (E)-hex-3-enoate, methyl (E)-oct-2-enoate, geranyl acetone, (E,E)-α-farnesene, methyl (2E,6E)-farnesoate, linalool, (E)-non-2-enal, (Z)-non-3-enol, and (Z)-non-2-enol. (Z)-Non-3-enal and (Z)-non-2-enal were prepared in our laboratory from the corresponding alcohols (Hazzard 1973 ). The purchased and synthesised chemicals were of analytical grade purity.
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