Chemical Co. (Milwaukee, WI) unless otherwise indicated. NMR spectra
were recorded on a Varian UNITY INOVA spectrometer. Chemical shifts
(δ) are reported in parts per million (ppm) downfield from tetramethylsilane.
Ultraviolet (UV) spectra were recorded on an Agilent model 8453 or
a Hewlett-Packard model 8451A diode array spectrophotometer. Elemental
analyses were performed by Midwest Microlab (Indianapolis, IN). Chromatography
was performed on a Biotage SP1 flash purification system. Prepacked
silica gel flash chromatography columns were purchased from Silicycle
(Quebec City, Canada) or from Yanazen Science Inc. (San Bruno, CA).
Compounds
described. In addition to NMR, UV, and HPLC with HRMS, CHN combustion
analysis was performed to determine purity of compounds. All compounds
were ≥95% pure.