Eucommia ulmoides gum (EUG) was provided by Beijing University of Chemical Technology, and was purified as follows: dissolved it in toluene and removed the insoluble materials by centrifugation, followed by precipitated in alcohol to get pure EUG (Mn = 1.2 × 106, PDI = 1.2). Titanium tetrachloride (AR, 99%) was purchased from Sinopharm Chemical Reagent Co., Ltd, acetic acid (AR, 98%) and other solvents were purchased from Beijing Chemical Works. The processing agents, such as dicumyl peroxide (DCP) and carbon black were commercially available and were used as received.
Titanium tetrachloride
Manufactured by Sinopharm
Titanium tetrachloride is a colorless, fuming liquid that is a versatile chemical compound used in various industrial applications. It is the primary precursor for the production of titanium metal and titanium dioxide pigments. Titanium tetrachloride is a highly reactive substance that must be handled with care and appropriate safety measures.
Automatically generated - may contain errors
Lab products found in correlation
Acetone, by Sinopharm (2 mentions)
Anhydrous ethanol, by Sinopharm (2 mentions)
Acetic acid, by Beijing Chemical Works (1 mentions)
Acetonitrile, by Thermo Fisher Scientific (1 mentions)
Ammonium fluoride, by Sinopharm (1 mentions)
Valeronitrile, by Thermo Fisher Scientific (1 mentions)
Ruthenium 535 bistba n719, by Solaronix (1 mentions)
Guanidinium thiocyanate, by Avantor (1 mentions)
Ethanol, by Sinopharm (1 mentions)
Sodium borohydride, by Sinopharm (1 mentions)
Sodium hydroxide (naoh), by Sinopharm (1 mentions)
Anhydrous glucose, by Sinopharm (1 mentions)
Hexadecyl trimethyl ammonium bromide, by Sinopharm (1 mentions)
Tinchloride pentahydrate, by Sinopharm (1 mentions)
Tert butyl alcohol, by Sinopharm (1 mentions)
Acetonitrile, by Sinopharm (1 mentions)
Hydrochloric acid (hcl), by Sinopharm (1 mentions)
Isopropanol, by Sinopharm (1 mentions)
4 protocols using titanium tetrachloride
1
Eucommia ulmoides Gum Isolation and Characterization
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Eucommia ulmoides gum (EUG) was provided by Beijing University of Chemical Technology, and was purified as follows: dissolved it in toluene and removed the insoluble materials by centrifugation, followed by precipitated in alcohol to get pure EUG (Mn = 1.2 × 106, PDI = 1.2). Titanium tetrachloride (AR, 99%) was purchased from Sinopharm Chemical Reagent Co., Ltd, acetic acid (AR, 98%) and other solvents were purchased from Beijing Chemical Works. The processing agents, such as dicumyl peroxide (DCP) and carbon black were commercially available and were used as received.
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Eucommia ulmoides gum (EUG) was provided by Beijing University of Chemical Technology, and was purified as follows: dissolved it in toluene and removed the insoluble materials by centrifugation, followed by precipitated in alcohol to get pure EUG (Mn = 1.2 × 106, PDI = 1.2). Titanium tetrachloride (AR, 99%) was purchased from Sinopharm Chemical Reagent Co., Ltd, acetic acid (AR, 98%) and other solvents were purchased from Beijing Chemical Works. The processing agents, such as dicumyl peroxide (DCP) and carbon black were commercially available and were used as received.
2
Fabrication of Dye-Sensitized Solar Cells
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Fuorinated tin oxide (FTO, ~7 Ω/cm2) glasses were bought from Nippin Sheet Glass Co., Ltd. Sodium hydroxide (NaOH, 96.0%), titanium tetrachloride (TiCl4, 99.0%), ammonium fluoride (NH4F, 96.0%), hydrochliric acid (HCl, 36%~38%wt), ethanol (99.7%) and acetone (99.5%) were purchased from Sinopharm Chemical Reagent Co. Ltd. Ruthenium 535-bisTBA (N719) was purchased from Solaronix. Guanidinium thiocyanate (GuSCN, 99.0%) was from Amresco. Titanium powder (Ti, 99.99%), lithium iodide (LiI, 99.999%), iodine (I2, 99.99%), 1-methyl-3- propylimidazolium iodide (PMII, 98%), 4-tert-butylpyridine (4-TBP, 96%) and tert-butyl alcohol (99.5%) were obtained from Aladdin. Acetonitrile (99.8%) and valeronitrile (99%) were from Alfa Aesar. All solvents and chemicals were reagent grade and were used without further purification.
3
Synthesis of Tin Oxide Nanoparticles
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All reagents are analytical grade and do not require further purification when used. Anhydrous Ethanol (CH3CH2OH > 99.8 %), tin chloride pentahydrate (SnCl4·5H2O), Titanium tetrachloride (TiCl4), anhydrous glucose (C6H12O6), sodium hydroxide(NaOH), hexadecyl trimethyl ammonium bromide (CTAB), acetic acid (CH3COOH), and sodium borohydride (NaBH4) were all purchased from Shanghai Sinopharm Chemical Reagent Co., Ltd.
4
Fabrication of Dye-Sensitized Solar Cells
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Pure titanium target (φ50 × 4 mm, ≥99.995%) was purchased from the Deyang ONA New Materials Co., Ltd. F-doped SnO2 transparent conductive glass (FTO, 30 × 30 × 2.2 mm, square resistance ≤ 7 Ω □−1, transmittance ≥ 80%) was purchased from the South China Science & Technology Co., Ltd. Tetrabutyl titanate (≥98%), titanium tetrachloride (≥98%), hydrochloric acid (36–38 wt%), anhydrous ethanol (≥99.7%), acetone (≥99.5%), isopropanol (≥99.7%), tert-butyl alcohol (TBA, ≥99.7%) and acetonitrile (≥99.5%) were purchased from the Sinopharm Chemical Reagent Co., Ltd. Di-tetrabutylammonium cis-bis (isothiocyanato) bis (2,2′-bipyridyl-4,4′-dicarboxylato) ruthenium(ii ) (N719, ≥99%), lithium iodide (99.9% trace metals basis), iodine (≥99.99% trace metals basis), 4-tert-butyl pyridine (TBP, 96%) and surlyn polymer frame (25 μm) were purchased from Shanghai Aladdin Bio-Chem Technology Co., Ltd. Gold counter-electrode and deionized water were made in our laboratory. The FTO was washed with acetone, isopropanol and deionized water before use.
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