Oleic acid (90%), 1-octadecene (90%), NH4F (99%), and NaOH (98%) were purchased from Sigma-Aldrich, USA. All acetic lanthanide nanoparticles, including Y(CH3CO2)3·xH2O (99.9%), Gd(CH3CO2)3·xH2O (99.9%), Er(CH3CO2)3·xH2O (99.9%), and Yb(CH3CO2)3·4H2O (99.9%), were also obtained from Sigma-Aldrich.
Gd ch3co2 3 xh2o
Manufactured by Merck Group
Sourced in China
Gd(CH3CO2)3·xH2O is a chemical compound used in laboratory settings. It consists of gadolinium, acetate, and water. The exact number of water molecules (x) can vary. This compound is commonly used as a reagent or precursor in various scientific applications, but a detailed description of its intended use is not provided.
Automatically generated - may contain errors
Lab products found in correlation
1 octadecene, by Merck Group (3 mentions)
Y ch3co2 3 xh2o, by Merck Group (2 mentions)
Oleic acid, by Merck Group (2 mentions)
Sodium hydroxide (naoh), by Merck Group (2 mentions)
Yb ch3co2 3 4h2o, by Merck Group (1 mentions)
Ir 780 iodide, by Merck Group (1 mentions)
Chloroform, by Merck Group (1 mentions)
N n dimethylformamide (dmf), by Merck Group (1 mentions)
4 mercaptobenzoic acid, by Merck Group (1 mentions)
Ethanol, by Sinopharm (1 mentions)
Chloroform, by Sinopharm (1 mentions)
3 protocols using gd ch3co2 3 xh2o
1
Synthesis of Lanthanide Nanoparticles
2
Synthesis of IR-806 Dye Precursors
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Gd(CH3CO2)3·xH2O (99.9%), Nd(CH3CO2)3·xH2O (99.9%), Y(CH3CO2)3·xH2O (99.9%), Yb(CH3CO2)3·xH2O (99.9%), Tm(CH3CO2)3·xH2O (99.9%), NaOH (>98%), NH4F (>98%), chloroform(99.9%), oleic acid (OA, 90%), and 1-octadecene (ODE, 90%) were all purchased from Sigma-Aldrich (Shanghai, China). IR-806 is supported by Dr. Sanyang Han from the University of Cambridge. IR-780 iodide, 4-mercaptobenzoic acid, and N,N-dimethylformamide (DMF, anhydrous, 99.8%), as raw materials of IR-806, were obtained from Sigma-Aldrich (London, UK). Dichloromethane (DCM, AR) and diethyl ether (AR), as solvents for the synthesis of IR-806, were obtained from Lab-Scan (London, United Kingdom). chloroform (AR), cyclohexane (AR), and ethanol (AR) were purchased from Sinopharm Chemical Reagent Co., Ltd. (Shanghai, China). All chemicals and reagents were used as received without further purification unless otherwise noted.
3
Synthesis of Terbium-Doped Nanoparticles
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Europium-doped nanoparticle synthesis and ligand functionalization were performed as previously described 54,70 . Terbium-doped nanoparticles (1% doped) were synthesized using similar procedures. In brief, synthesis proceeded through the addition of 1.98 mL Gd(CH 3 CO 2 ) 3 •xH 2 O and 20 μL Tb(CH 3 CO 2 ) 3 •xH 2 O (Sigma-Aldrich) to stirring 1-oleic acid (4 mL; Alfa Aesar) and 1-octadecene (6 mL; 90% Sigma-Aldrich) at room temperature. From here, synthesis proceeded as usual according to the procedures of Wang et al 54 .
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