2 cyano 2 propyl dithiobenzoate

Manufactured by Strem Chemicals

Sourced in United Kingdom

2-Cyano-2-propyl dithiobenzoate is a chemical compound used in various laboratory applications. It is a white to pale yellow crystalline solid. The primary function of this product is as a reagent or an intermediate in organic synthesis.

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Lab products found in correlation

2 hydroxypropyl methacrylate, by Thermo Fisher Scientific (3 mentions) Hplc grade solvents, by Thermo Fisher Scientific (1 mentions) Anhydrous ethanol, by Merck Group (1 mentions) Cystamine dihydrochloride, by Merck Group (1 mentions) 4 4 azobis 4 cyanopentanoicacid acva v 501, by Merck Group (1 mentions)

Spelling variants of this product

2-Cyano-2-propyl dithiobenzoate (CPDB) (4 citations)

3 protocols using 2 cyano 2 propyl dithiobenzoate

Synthesis of glycerol monomethacrylate polymers

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Glycerol monomethacrylate
(GMA; 99.8%) was
donated by GEO Specialty Chemicals (Hythe, UK) and used without further
purification. 2-Hydroxypropyl methacrylate (HPMA) and 4,4′-azobis(4-cyanopentanoic
acid) (ACVA; V-501; 99%) were purchased from Alfa Aesar (Heysham,
UK). 2-Cyano-2-propyl dithiobenzoate (CPDB, 80% as judged by ¹H NMR spectroscopy) was purchased from Strem Chemicals (Newton,
UK). CD₃OD (99.8%) was purchased from Goss Scientific (Nantwich,
UK) and used as received. All solvents were of HPLC quality; they
were purchased from Fisher Scientific (Loughborough, UK) and used
as received.

Canton I., Warren N.J., Chahal A., Amps K., Wood A., Weightman R., Wang E., Moore H, & Armes S.P. (2016). Mucin-Inspired Thermoresponsive Synthetic Hydrogels Induce Stasis in Human Pluripotent Stem Cells and Human Embryos. ACS Central Science, 2(2), 65-74.

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Synthesis of GMA-based Polymers

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Materials. Glycerol monomethacrylate (GMA; 99.8%) was provided by GEO Specialty Chemicals (Hythe, UK) and used as received. 2-Hydroxypropyl methacrylate (HPMA) and 4,4′-azobis(4-cyanopentanoic acid) (ACVA, a.k.a. V-501; 99%) were obtained from Alfa Aesar (Heysham, UK). 2-Cyano-2-propyl dithiobenzoate (CPDB, 80% purity) was purchased from Strem Chemicals (Newton, UK). CD3OD (99.8%) was sourced from Goss Scientific (Nantwich, UK). HPLC-grade solvents were purchased from Fisher Scientific (Loughborough, UK) and were used as received.

Binch A.L.A., Ratcliffe L.P.D., Milani A.H., Saunders B.R., Armes S.P, & Hoyland J.A. (2021). Site-Directed Differentiation of Human Adipose-Derived Mesenchymal Stem Cells to Nucleus Pulposus Cells Using an Injectable Hydroxyl-Functional Diblock Copolymer Worm Gel. Biomacromolecules, 22(2).

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Synthesis of Functional Monomers and Initiators

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Glycerol monomethacrylate (GMA; 99.8 %) was donated by GEO Specialty Chemicals (Hythe, UK) and used without further purification. 2-Hydroxypropyl methacrylate (HPMA) was purchased from Alfa Aesar (Heysham, UK). 2-Cyano-2-propyl dithiobenzoate (CPDB, 80 % as judged by 1 H NMR spectroscopy), and 4-cyano-4-(thiobenzoylthio)pentanoic acid (CPADB, 97 %) were purchased from Strem Chemicals (Cambridge, UK). Bis(2-(methacryloyloxy)ethyl disulfide monomer (DSDMA) monomer 32 and 4-cyano-4-(thiobenzoyl) sulfanyl) pentanoic succinimide ester (SCPDB) 39 agent were synthesized according to previously reported protocols.
4,4'-Azobis(4-cyanopentanoic acid) (ACVA; V-501; 99 %), Cystamine dihydrochloride (98 %), D 2 O and anhydrous ethanol (99 %) were purchased from Sigma-Aldrich (UK). CD 3 OD (99.8 %) and CD 2 Cl 2 (99.8 %) were purchased from Goss Scientific (Nantwich, UK) and used as received.
All solvents were of HPLC quality; they were purchased from Fisher Scientific (Loughborough, UK) and used as received.

Warren N.J., Rosselgong J., Madsen J, & Armes S.P. (2015). Disulfide-Functionalized Diblock Copolymer Worm Gels. Biomacromolecules, 16(8).

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