The largest database of trusted experimental protocols

5 protocols using n methylformamide

1

Synthesis of Organic Compounds

Check if the same lab product or an alternative is used in the 5 most similar protocols
Citric acid (CA), formamide (FA), and DMF were purchased from VWR, urea (>98.3%), N-methylformamide (MFA, 99%), and N,N,N′-trimethylurea (TriMU) from Alfa Aesar, and N,N,N′,N′-tetramethylurea (TetraMU) from TCI. Water was deionized and purified in a Millipore Direct Q Water Purification System.
+ Open protocol
+ Expand
2

Hafnium Tetrachloride Synthesis Protocols

Check if the same lab product or an alternative is used in the 5 most similar protocols
Hafnium(IV) tetrachloride (98%) was used as the Hafnium source. Acetone, acetonitrile, hexanes, methanol, and pentane were all HPLC Plus (>99.9%). Hydrochloric acid (35.0–37.0%), sulfuric acid (95.0–98.0%), Sodium chloride (>99%) and deuterated water (D2O) were used as purchased from Sigma-Aldrich. N-Methyl formamide (99%) and sodium hydroxide pellets (98%) were purchased from Alfa Aesar. Poly(ethylene oxide) (MW 100 000) was purchased from Polysciences Inc. Propylene oxide (99.5%) and Trifluoroacetic acid (99.5%) were purchased from Acros Organics. Perfluorooctanoic acid (>98%) was purchased from TCI America. Ultrapure water (≥18.2 MΩ∙cm) used for synthesis and adsorption kinetics experiments was obtained from a Thermo Scientific Barnstead E-Pure Ultrapure water purification system.
+ Open protocol
+ Expand
3

Synthesis of Chalcogenide Nanocrystals

Check if the same lab product or an alternative is used in the 5 most similar protocols
Antimony acetate (Sb(OAc)3, 99.99% metal basis, Aldrich), bismuth acetate (Bi(OAc)3, 99.999% metal basis, Aldrich), selenium powder (99.99% Strem Chemicals), tellurium powder (99.997% (trace metals basis), Alfa Aesar), Na2S nonahydrate (99,99%, Aldrich), Oleic acid (90% technical grade, Aldrich), Trioctylphosphine (TOP 380, 98%, Cytec), octadecene (ODE, 90% technical grade, Aldrich), hexane (95% RPE-ACS, Carlo Erba), ethanol (anhydrous 99.9%, Carlo Erba), N-methyl formamide (NMFA, 99%, Alfa Aesar.)
+ Open protocol
+ Expand
4

Synthesis of Metal Chalcogenide Nanocrystals

Check if the same lab product or an alternative is used in the 5 most similar protocols
Tin(II)
chloride dihydrate (SnCl2·2H2O, 98%), sodium
hydroxide (NaOH, pellets 98%),
sodium borohydride (NaBH4, 98%), cadmium oxide (CdO, 99.99%),
lead(II) oxide (PbO, 99.99%), and N-methylformamide
(MFA, 99%) were purchased from Fisher Scientific. Selenium powder
(Se, 100 mesh, ≥99.5%), ethylenediamine (en, 99%), 1, 2-ethanedithiol
(EDT, ≥95.0%), anhydrous acetone (extra dry), and ethanol (95%)
were purchased from Sigma-Aldrich. All chemicals were used as received
without further purification. Syntheses were carried out using a vacuum/dry
argon Schlenk line.
+ Open protocol
+ Expand
5

Preparing Black Phosphorus in Inert Atmosphere

Check if the same lab product or an alternative is used in the 5 most similar protocols
All solvents were purchased from Sigma Aldrich unless otherwise noted. The solvents were degassed prior to use and handled under nitrogen. Black phosphorus (smart elements, ~99.998%), red phosphorus (Sigma Aldrich, ≥ 99.999+%), N-methyl-2-pyrrolidone (Sigma Aldrich or Acros Organics, anhydrous, 99.5%) 2-propanol (FisherSci, electronic grade), cyclopentanone (≥ 99%), 1-cyclohexyl-2-pyrrolidone (≥ 99%), 1-dodecyl-2-pyrrolidinone (≥ 99%), benzyl benzoate (≥ 99.0%), 1-octyl-2-pyrrolidone (≥ 98%), 1-vinyl-2-pyrrolidinone (≥ 99%), benzyl ether (≥ 98%), 1,3-dimethyl-2-imidazolidinone (≥ 99%), cyclohexanone (≥ 99.8%), chlorobenzene (≥ 99.5%), dimethylsulfoxide (≥ 99.9%), benzonitrile (anhydrous, ≥ 99%), Nmethylformamide (≥ 99%), dimethylformamide (≥ 99%), benzaldehyde (≥ 99%).
All samples were prepared in a nitrogen-filled glove box (O2 < 1 ppm) and transferred from instrument to instrument using custom-designed glassware with Rotaflo stopcocks. When necessary, instrument loading chambers and/or the entire instrument was enclosed in N2-filled glove bags to provide an inert atmosphere.
+ Open protocol
+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required

Sign up now

Revolutionizing how scientists
search and build protocols!