4 chlorophenol 4 cp

Manufactured by Merck Group

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4-Chlorophenol (4-CP) is a colorless crystalline solid that is commonly used as an intermediate in the production of various chemicals and pharmaceuticals. It has the chemical formula C6H5ClO. 4-CP is a versatile compound that can be utilized in various industrial and research applications.

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4-chlorophenol (14 citations)

4 protocols using 4 chlorophenol 4 cp

Oxidation of 4-Chlorophenol by Hydrogen Peroxide

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4-chlorophenol (4-CP, 99%, Sigma-Aldrich, St. Louis, MO, USA), p-chlorobenzoic acid (pCBA, 99%, Acros, Geel, Belgium), hydrogen peroxide (33%, Lega, Dzerzhinsk, Russia), sodium bicarbonate (Khimreaktivsnab, Ufa, Russia), 4-aminoantipyrine and potassium ferricyanide (Vekton, St Petersburg, Russia) were used as supplied. Stock solutions of 4-CP and H₂O₂ were prepared in deionized water (18.2 mΩ·cm) produced by a Simplicity^®UV system from Millipore (Burlington, MA, USA).

Popova S., Tazetdinova V., Pavlova E., Matafonova G, & Batoev V. (2022). Characteristics and Sonophotocatalytic Activity of Natural Sphalerite under Ultrasonic (1.7 MHz) and UVA LED (365 nm) Irradiation. Materials, 15(15), 5412.

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Synthesis of Hybrid Nanomaterials

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All chemical reagents used in the experiments were obtained from commercial sources as guaranteed grade reagents. Titanium (IV) isopropoxide 97% (TTIP: Ti[OCH(CH₃)2]₄), 3-butyn-1-ol 97% (HC≡CCH₂CH₂OH or C₄H₆O), 1-octanol 98% (CH₃(CH₂)₇OH), chloroform 99% (CHCl₃), acetone ACS reagent ≥ 99.5% (CH₃COCH₃), ethanol absolute (CH₃CH₂OH), 4-chlorophenol (4-CP), Cu(CH₃COO)₂, ascorbic acid (C₆H₈O₆), hydrazine (N₂H₄), hexadecylamine (HDA), vanadium triisopropoxide (VOTPP), cadmium chloride (CdCl₂), sodium sulfide (Na₂S), and terephthalic acid (TA) were purchased from Sigma-Aldrich (St. Louis, MO, USA). All reagents were of analytical grade and were used without further purification.

Lozano H., Devis S., Aliaga J., Alegría M., Guzmán H., Villarroel R., Benavente E, & González G. (2022). Two-Dimensional Titanium Dioxide–Surfactant Photoactive Supramolecular Networks: Synthesis, Properties, and Applications for the Conversion of Light Energy. International Journal of Molecular Sciences, 23(7), 4006.

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Electrochemical Determination of 4-Chlorophenol

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The 4-chlorophenol (4-CP) was obtained from Sigma-Aldrich (St. Louis, MO, USA). The hydrochloric acid, sulfuric acid, sodium sulfate, and aniline were obtained from Chempur (Piekary Śląskie, Poland). Stock standard solution of 4-CP (0.5 mmol/L) was prepared in 0.1 mol/L Na₂SO₄. Working solutions were prepared as required by dilution with sodium sulfate of the same concentration. The multi-walled carbon nanotubes CNTs (CNT Co., Ltd., Incheon, Korea) and graphite (<45 μm) from Sigma-Aldrich (St. Louis, MO, USA) were used. Paraffin oil was received from Fluka (Buchs, Switzerland).

Kuśmierek K., Skrzypczyńska K., Świątkowski A., Wierzbicka E, & Legocka I. (2022). Electropolymerized Aniline-Based Stainless Steel Fiber Coatings Modified by Multi-Walled Carbon Nanotubes for Electroanalysis of 4-Chlorophenol. Materials, 15(10), 3436.

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Lanthanum-Doped Titanium Dioxide Synthesis

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Titanium(iv) oxysulfate (titanyl sulfate, TiOSO₄, Sigma-Aldrich spol. s.r.o., Prague, Czech Republic) was used as a TiO₂ precursor. Lanthanum(iii) nitrate hexahydrate, La(NO₃)₃·6H₂O Assay Spec. ≥99%, served as the La dopant source. During material synthesis, an aqueous solution of ammonia (NH₃, solution purum p.a., 25–29%, Fisher Scientific, spol. s.r.o., Pardubice Czech Republic) was used for precipitation of the precursor and hydrogen peroxide (H₂O₂, solution purum p.a., 30%, Fisher Scientific, spol. s.r.o., Pardubice Czech Republic) for pH reduction. 4-Chlorophenol (4-CP, purity ≥ 99.9%, Sigma-Aldrich, Prague, Czech Republic) and AEROXIDE TiO₂-P25 (Evonik, Prague, Czech Republic) were used for the photocatalytic experiments.

Bakardjieva S., Mares J., Fajgar R., Zenou V.Y., Maleckova M., Chatzisymeon E., Bibova H, & Jirkovsky J. (2019). The relationship between microstructure and photocatalytic behavior in lanthanum-modified 2D TiO2 nanosheets upon annealing of a freeze-cast precursor. RSC Advances, 9(40), 22988-23003.

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