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Thermo k alpha spectrometer

Manufactured by Thermo Fisher Scientific
Sourced in United Kingdom

The Thermo K-Alpha spectrometer is a versatile X-ray photoelectron spectroscopy (XPS) instrument designed for surface analysis. It provides high-resolution, quantitative elemental and chemical state information about the surface of a wide range of materials. The spectrometer utilizes a monochromatic Al Kα X-ray source and a high-performance electron energy analyzer to deliver precise data about the composition and chemistry of sample surfaces.

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2 protocols using thermo k alpha spectrometer

1

X-ray Photoelectron Spectroscopy Protocol

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XPS was performed using a Thermo K-Alpha spectrometer (Thermo Scientific, Inc., UK). All spectra were obtained using an Al Kα micro-focused monochromatized source with a resolution of 0.1 eV, pass energy of 50 eV, and spot size of 400 μm.
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2

X-ray Photoelectron Spectroscopy of Dried Samples

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Surface compositions and chemical states were obtained after drying the samples at 120°C for 1 h and conducting X-ray photoelectron spectroscopy (XPS) using a Thermo K Alpha + spectrometer (Thermo Scientific) operating at around 10−8 to 10−9 Torr with a Al Kα radiation source (1,486.7 eV). High resolution spectra were collected for cobalt (Co 2p) and silica (Si 2p) to assess the oxidation states with the peaks normalised to the carbon peak (285.0 eV).
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