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Titan mps microwave

Manufactured by PerkinElmer
Sourced in United States

The Titan MPS Microwave is a laboratory equipment designed for rapid, controlled, and efficient sample preparation. It utilizes microwave technology to facilitate the dissolution and digestion of a wide range of sample types, including organic and inorganic materials. The Titan MPS Microwave provides precise temperature and pressure control to ensure consistent and reproducible results.

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2 protocols using titan mps microwave

1

Mineral Analysis of Restructured Goat Jerky

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To measure the mineral contents in restructured black goat jerky with added USP,
0.3 g of jerky was weighed in a vessel, and 7 mL of HNO3 and 2 mL of
H2O2 solutions were added. Subsequently, the samples
were pretreated for 10 min in a microwave (Titan MPS Microwave, Perkin Elmer,
Waltham, MA, USA) to achieve separation. Once separated, 0.5 g of the sample was
diluted 100-fold in triple distilled water to adjust the final weight to 50 g.
Another 0.2 g of pretreated sample was diluted 100-fold in triple distilled
water to make up the final weight to 20 g at a final concentration of 100 ppm.
These solutions were used in the experiment. The mineral contents of the samples
were determined by measuring ion beam intensity with an inductively coupled
plasma mass spectrometer (NEXION-350X, Perkin-Elmer, Shelton, CT, USA).
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2

Mineral Analysis via ICP-OES

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The mineral content was analyzed using the method of Kang et al. [15 (link)]. Take 500 mg of sample in the vessel, mix 7 mL of HNO3 and 2 mL of H2O2, pre-treat using microwave (Titan MPS Microwave, PerkinElmer, Waltham, MA, USA) for 10 min, and then dilute to 3.4% concentration with tertiary distilled water. For the sample, the concentration of minerals was calculated by measuring the intensity of the ion beam using Inductively Coupled Plasma Optical Emission Spectroscopy (ICP-OES, OPTIMA200 DV, PerkinElmer, Waltham, MA, USA). The analysis conditions are as follows: step 1 (temperature: 145 °C, pressure max: 70 min, ramp time: 5 min, hold time: 5 min, power: 60%), step 2 (temperature: 200 °C, pressure max: 80 min, ramp time: 5 min, hold time: 20 min, power: 90%), step 3 (temperature: 50 °C, pressure max: 80 min, ramp time: 1 min, hold time: 10 min, power: 0%). The standard products for quantification were multi-element calibration standards (ICP multi-element standard solution IV, Sigma–Aldrich Co., St. Louis, MO, USA), and the phosphorus, potassium, magnesium, calcium, and sodium were measured.
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