The density of the dope solution was determined using a digital density meter (Model: DMA 5000 M, Anton Paar) with an oscillating capillary U-tube. The measurement of density is based on the frequency of oscillation. An amount of 1 mL sample solution is filled into a U-shaped oscillating capillary tube. The density meter is set in connection with the rolling ball viscometer. For the determination of viscosity and density, PC/DCM dope solutions with 3, 6, 9, 12, 15, 17, 19 and 21 wt % polymer concentrations and PC/NMP solutions with 3, 6, 9, 12, 15, 18 wt % polymer concentrations were used. The same sample solutions were also analyzed for the refractive index using a refractometer (RX5000α, Atago, Washington, DC, USA). The refractometer was first calibrated with distilled water of known refractive index. About 2–3 mL of the sample solution was drawn and put in the sample cone of the refractometer.
Rx 5000α
The RX-5000α is a high-performance lab equipment designed for precise analysis and measurement. It features advanced sensor technology and a user-friendly interface. The core function of the RX-5000α is to provide accurate and reliable data for scientific research and industrial applications.
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9 protocols using rx 5000α
Viscosity, Density, and Refractive Index Characterization of Polymer Solutions
The density of the dope solution was determined using a digital density meter (Model: DMA 5000 M, Anton Paar) with an oscillating capillary U-tube. The measurement of density is based on the frequency of oscillation. An amount of 1 mL sample solution is filled into a U-shaped oscillating capillary tube. The density meter is set in connection with the rolling ball viscometer. For the determination of viscosity and density, PC/DCM dope solutions with 3, 6, 9, 12, 15, 17, 19 and 21 wt % polymer concentrations and PC/NMP solutions with 3, 6, 9, 12, 15, 18 wt % polymer concentrations were used. The same sample solutions were also analyzed for the refractive index using a refractometer (RX5000α, Atago, Washington, DC, USA). The refractometer was first calibrated with distilled water of known refractive index. About 2–3 mL of the sample solution was drawn and put in the sample cone of the refractometer.
Coriander Seed Oil Characterization
Quantitative Analysis of Naphthenic Acids
of NA in dodecane and IL layers was performed using an ATAGO programmable
digital refractometer (RX-5000α) according to an already reported
procedure8 (link) because the quantification of
NA via gas chromatography (GC) and high-pressure liquid chromatography
(HPLC) is quite a cumbersome process because of its complex structure.10 (link),28 (link)−30 (link) The respective concentrations of NA in hydrocarbon
and IL layers were estimated from the graphs of the refractive index
against the mole fraction, as shown in
The possible cross-contamination between both immiscible
solvents
has been verified with the help of 1H nuclear magnetic
resonance (NMR). 1H NMR measurements were done using a
Bruker Avance 500 MHz NMR spectrometer. The NMR spectra of dodecane
and IL layers without the presence of NA but after typical shaking
and decantation procedures are recorded and shown in
found and vice-versa in the IL phase (no trace of dodecane was recorded)
indicating that cross contamination does not occur.
Citrus Juice Quality Analysis
Rheological and Physicochemical Properties of Deep Eutectic Solvents
DESs were investigated by
rheological measurements; the experiments were conducted using a HAAKE
MARS rheometer (Thermo Fisher Scientific, Germany) set with a plate-plate
geometry (20 mm and 0.2 mm gap). A water recirculatory bath (HAAKE
Phoenix II, Germany) was used for temperature control, set to 20.0
± 0.1 °C. The water content of the DES was assessed by Karl
Fischer volumetric titration using a Metrohm 890 Karl Fischer Titrando
apparatus equipped with an 803 Ti Stand to 0.4% accuracy in water
mass content. The refractive indices were measured at the sodium D
line (589.3 nm) using an ATAGO RX-5000α refractometer at 25
°C.
the most relevant properties obtained for the different DESs prepared.
Note that the DESs were also evaluated 30 days after preparation to
infer on the aging effect.
Determining Soluble Solids Concentration
Nitrogen Release from PU-SFe-CRUs
release experiment was conducted to investigate the effects of the
coating ratio, SFeSt3 proportion, and PAPI proportion on
nitrogen release characteristics of the PU-SFe-CRUs. For the effect
of the coating ratio, PU-SFe-CRUs with coating ratios of 1.32, 3.00,
and 4.68%, PAPI proportion of 50.00%, and SFeSt3 proportion
of 0.70% were used. For the effect of SFeSt3 proportion,
PU-SFe-CRUs with a coating ratio of 3.00%, PAPI proportion of 50.00%,
and SFeSt3 proportions of 0.20, 0.70, and 1.20% were used.
For the effect of PAPI proportion, PU-SFe-CRUs with a coating ratio
of 3.00%, SFeSt3 proportion of 0.70%, and PAPI proportions
of 33.18, 50.00, and 66.82% were used. The nitrogen release rates
of the above mentioned PU-SFe-CRUs and PU-CRU (CK) were measured according
to the standard method HG/T 4216-2011.50 Briefly, 10 g CRU were put into a bottle containing 200 mL deionized
water and placed in a biochemical incubator at 25 ± 0.5 °C.
The solution was sampled after 1, 3, 5, 7, 14, 28, 56, and 84 days
of incubation for the determination of the refractive index using
a refractometer (RX-5000α, ATAGO Co., Ltd., Tokyo, Japan) until
the cumulative nitrogen release rate was larger than 80%.
Stability Assessment of CRPP Formulation
The parameters that were determined in order to investigate the chemical stability was antioxidant activity by DPPH (Sigma-Aldrich, MI, USA) scavenging assay [46 (link)], and total phenolic compounds by the Folin–Ciocalteu method (Merck KGaA, Darmstadt, Germany) [47 (link)] at appropriate time intervals (4, 8 and 24 weeks).
Measuring Total Soluble Solids in Sugarcane
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