The FTIR Nicolet iS 10 spectrometer (Thermo Fisher Scientific, Waltham, MA, USA) was used to examine the chemical functional groups of the tested filaments. The spectral range was from 4000 to 500 cm−1, using 16 scans with a resolution of 4 cm−1.
Ftir nicolet is10 spectrometer
Manufactured by Thermo Fisher Scientific
Sourced in United States
The FTIR-Nicolet iS10 spectrometer is a Fourier Transform Infrared (FTIR) spectrometer. It is designed to analyze the composition of samples by measuring the infrared absorption spectrum. The spectrometer uses an interferometer to generate and detect infrared radiation, which is then analyzed to provide information about the molecular structure of the sample.
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Lab products found in correlation
Simultaneous thermal analyzer, by Netzsch (1 mentions)
K alpha x ray photoelectron spectrometer, by Thermo Fisher Scientific (1 mentions)
Nova nanosem 450, by Thermo Fisher Scientific (1 mentions)
Icap6300 icp aes, by Thermo Fisher Scientific (1 mentions)
Facscanto 2 flow cytometer, by BD (1 mentions)
Zetasizer nano zs90, by Malvern Panalytical (1 mentions)
U 4100 spectrometer, by Hitachi (1 mentions)
5 protocols using ftir nicolet is10 spectrometer
1
Chemical Functional Group Analysis
2
Characterization of Metal-Organic Frameworks
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All reagents
and solvents used
in the experiments were commercially available and used without further
purification (Innochem, China). The FT-IR absorption spectra for Cd-CP,
Hg@Cd-CP and Pb@Cd-CP were collected from KBr pellets using a Thermo
Scientific FTIR-Nicolet iS10 spectrometer in the range of 4000–400
cm–1 (Thermo Scientific, U.S.A.). Powder X-ray diffraction
(PXRD) was performed in the 2θ range of 5–50° on
a Rigaku X-ray diffractometer with Cu Kα radiation (λ
= 1.5418 Å) (Rigaku, Japan). Elemental analyses were carried
out on a PerkinElmer 2400C elemental analyzer (Elementar, Germany).
TGA data were acquired using a Mettler-Toledo simultaneous thermal
analyzer from room temperature to 800 °C under an N2 atmosphere at a heating rate of 10 °C min–1 (Netzsch, Germany). XPS was performed using a K-Alpha X-ray photoelectron
spectrometer (Thermo Scientific, USA). The morphology and energy-dispersive
spectroscopy (EDS) data of Cd-CP, Hg@Cd-CP, and Pb@Cd-CP were obtained
using a Nova NanoSEM 450 field-emission scanning electron microscope
(SEM) at 10 Kv (Thermo Scientific, U.S.A.). The concentration of metal
ions was determined with an iCAP6300 ICP-AES (Thermo Scientific, U.S.A.).
and solvents used
in the experiments were commercially available and used without further
purification (Innochem, China). The FT-IR absorption spectra for Cd-CP,
Hg@Cd-CP and Pb@Cd-CP were collected from KBr pellets using a Thermo
Scientific FTIR-Nicolet iS10 spectrometer in the range of 4000–400
cm–1 (Thermo Scientific, U.S.A.). Powder X-ray diffraction
(PXRD) was performed in the 2θ range of 5–50° on
a Rigaku X-ray diffractometer with Cu Kα radiation (λ
= 1.5418 Å) (Rigaku, Japan). Elemental analyses were carried
out on a PerkinElmer 2400C elemental analyzer (Elementar, Germany).
TGA data were acquired using a Mettler-Toledo simultaneous thermal
analyzer from room temperature to 800 °C under an N2 atmosphere at a heating rate of 10 °C min–1 (Netzsch, Germany). XPS was performed using a K-Alpha X-ray photoelectron
spectrometer (Thermo Scientific, USA). The morphology and energy-dispersive
spectroscopy (EDS) data of Cd-CP, Hg@Cd-CP, and Pb@Cd-CP were obtained
using a Nova NanoSEM 450 field-emission scanning electron microscope
(SEM) at 10 Kv (Thermo Scientific, U.S.A.). The concentration of metal
ions was determined with an iCAP6300 ICP-AES (Thermo Scientific, U.S.A.).
3
Analytical Balance and FTIR Spectroscopy
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All weighing was carried out using
an Ohaus DV215CD analytical balance (Parsippany, NJ, USA) with a precision
of five decimal places (i.e., 0.00001 g).
The IR analyses were
performed with an FTIR Nicolet IS10 spectrometer (Thermo Scientific,
Waltham, MA, USA) equipped with a smart ITR module for ATR measurements
in the spectral range from 3500 to 650 cm–1 and
operated with the Omnic 9 software for IR spectroscopy (Thermo Scientific,
Waltham, MA, USA).
an Ohaus DV215CD analytical balance (Parsippany, NJ, USA) with a precision
of five decimal places (i.e., 0.00001 g).
The IR analyses were
performed with an FTIR Nicolet IS10 spectrometer (Thermo Scientific,
Waltham, MA, USA) equipped with a smart ITR module for ATR measurements
in the spectral range from 3500 to 650 cm–1 and
operated with the Omnic 9 software for IR spectroscopy (Thermo Scientific,
Waltham, MA, USA).
4
FTIR Spectroscopy of Sample Characterization
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A Thermo Fisher Scientific FTIR Nicolet iS10 spectrometer was used to record the FTIR spectrum of the samples in the range of 650–4000 cm−1, and 16 scans were performed at a resolution of 4 cm−1.
5
Comprehensive Characterization of Nanoparticle Formulations
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Inductively coupled plasma mass spectrometry (ICP-MS) was recorded on a 7700x (Agilent, USA) spectrometer. The ultraviolet-visible (UV-vis) spectra were performed on a Hitachi U-4100 spectrometer. The Fourier transform infrared (FTIR) spectra were acquired by a Thermo Scientific FTIR-Nicolet iS10 spectrometer in the range 4000−400 cm−1. Dynamic light scattering (DLS) and zeta potential were performed at 25°C on Zetasizer Nano ZS90 (Malvern Instruments Ltd, UK). The morphology and energy-dispersive spectroscopy (EDS) data of BSA/Ga/HBrQ NPs and GO/Ga/HBrQ NPs were obtained using a Nova NanoSEM 450 field-emission scanning electron microscope (SEM) at 10 kV and using a JEM-2100 transmission electron microscope (TEM) at 200 kV, and X-ray spectroscopy (XPS) data were acquired using a K-Alpha+ X-ray photoelectron spectrum. Luminescence spectroscopy analysis of BSA/Ga/HBrQ NPs and GO/Ga/HBrQ NPs was performed on a Lengguang (Shanghai, China) F98 fluorescence spectrophotometer. Cells were counted by Countstar cell automatic counter from Advanced Lab Instrument & Technology Co., Ltd. Microplate Reader (Infinite® 200 Pro NanoQuan, Tecan, Swiss). Flow Cytometry was performed on a BD FACS Canto II flow cytometer. Small Animal Live Imaging System (PerkinElmer IVIS, USA).
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