1,7,7-Trimethylbicyclo[2.2.1]heptan-2-one (( ±)-Camphor, > 95%), DL-2,3-dihydroxybutanedioic acid (DL-tartaric acid, ≥ 99%), trimethyl orthoformate (99%), sulfuric acid (95–98%), sodium bicarbonate (NaHCO3, 99.0%), ethylene glycol (EG, 1,2-ethanediol ≥ 99.8%), 1,4-butanediol (99%), 1,6-hexanediol (99%), dimethyl terephthalate (99%), titanium(iv) isopropoxide, (99.995%) and chloroform-d (99.8 atom % D), and deuterated trifluoroacetic acid were purchased from Sigma-Aldrich. ( ±)-Camphor was recrystallized from ethanol.
Dimethyl terephthalate
Manufactured by Merck Group
Sourced in Belgium
Dimethyl terephthalate is a chemical compound used as a raw material in the production of polyester resins and fibers. It is a colorless, crystalline solid with a melting point of approximately 140°C. Dimethyl terephthalate is a key intermediate in the synthesis of various polyester products.
Automatically generated - may contain errors
Lab products found in correlation
Ethylene glycol, by Merck Group (2 mentions)
1 4 butanediol, by Merck Group (2 mentions)
Chloroform d, by Merck Group (1 mentions)
Titanium 4 isopropoxide, by Merck Group (1 mentions)
Sulfuric acid, by Merck Group (1 mentions)
Sodium bicarbonate, by Merck Group (1 mentions)
Camphor, by Merck Group (1 mentions)
1 6 hexanediol, by Merck Group (1 mentions)
Dl tartaric acid, by Merck Group (1 mentions)
Trimethylorthoformate, by Merck Group (1 mentions)
Deuterated trifluoroacetic acid, by Merck Group (1 mentions)
Dmso d6, by Merck Group (1 mentions)
Succinic acid, by Merck Group (1 mentions)
Phosphoric acid, by Merck Group (1 mentions)
Zinc acetate, by Merck Group (1 mentions)
Cdcl3, by Merck Group (1 mentions)
Glycolic acid, by Merck Group (1 mentions)
Methanesulfonic acid, by Merck Group (1 mentions)
Zinc acetylacetonate, by Merck Group (1 mentions)
Antimony 3 oxide, by Merck Group (1 mentions)
5 protocols using dimethyl terephthalate
1
Synthesis and Characterization of Camphor Derivatives
2
Synthesis of Polymer Precursors
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Glycolic acid, dimethyl
terephthalate, adipic acid, succinic acid, bismuth(III) subsalicylate,
antimony(III) oxide, zinc acetylacetonate, zinc acetate, methanesulfonic
acid, phosphoric acid, DMSO-d6, and CDCl3 were purchased from Sigma-Aldrich. 1,4-Butanediol,
tin(II) 2-ethylhexanoate, and titanium butoxide were purchased from
VWR, Alfa Aesar. Zirconium(IV) acetylacetonate was purchased from
Strem Chemicals U.K., Ltd. Irgafos 126, Irgafos 168, and Joncryl ADR
4468 were from BASF.
terephthalate, adipic acid, succinic acid, bismuth(III) subsalicylate,
antimony(III) oxide, zinc acetylacetonate, zinc acetate, methanesulfonic
acid, phosphoric acid, DMSO-d6, and CDCl3 were purchased from Sigma-Aldrich. 1,4-Butanediol,
tin(II) 2-ethylhexanoate, and titanium butoxide were purchased from
VWR, Alfa Aesar. Zirconium(IV) acetylacetonate was purchased from
Strem Chemicals U.K., Ltd. Irgafos 126, Irgafos 168, and Joncryl ADR
4468 were from BASF.
3
Synthesis and Characterization of Organic Compounds
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Dimethyl terephthalate (qNMR), furfuryl alcohol (96%w), maleic anhydride (99%w), hydroxylamine hydrochloride (99%w), triethanolamine (99%w), hydrochloric acid (37%w) and DMSO (98%) were purchased from Merck. VWR provided the ethanol (96%v). The d6-DMSO was purchased from Eurisotop. The water used in the synthesis and characterization was distilled using a SI Analytics distillation unit.
4
Skin Tissue Engineering with PCL Biomaterials
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Poly(ε-caprolactone) (PCL, Mn = 80 kg/mol), poly(ε-caprolactone) diol (Mn = 530 g/mol), isophorone diisocyanate (IPDI), triphenylphosphine (TPP), phenothiazine (PTZ), dimethylterephthalate (DMT), Brij®35 and phosphate buffered saline (PBS) were purchased from Merck (Belgium). 2,6-di-tert-butyl-4-methylphenol (BHT) was obtained from Innochem (Belux). Deuterated Chloroform was purchased from EurIsotop (Belgium). Ethoxylated and propoxylated pentaerythritol triacrylate (EPPETA) and bismuth neodecanoate catalyst were kindly provided by Allnex (Belgium). Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide (TPO-L) was provided by Lambson (UK). Chloroform and acetone were purchased from ChemLab (Belgium). Hydrocortisone was purchased from the Apothecary of the Ghent University Hospital, (UZ Ghent, Ghent, Belgium). The skin samples were obtained from residual waste from a subcutaneous mastectomy. Small containers with 10% formol were purchased from VWR Chemicals (Fontenay-Sous-Bois, France) and automatic hematoxylin and eosin (HE) staining of the paraffin slices was used (T181 Tissue- Tek Prisma Plus, Sakura Finetek, Antwerp, Belgium).
5
Synthesis of Polyester Precursors
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Dimethyl terephthalate, 1,8-octanediol, ethylene glycol and 1,4-butanediol were purchased from Merck while 1,6hexanediol and 1,12-dodecanediol were obtained from Tokyo Chemical Industry. All other chemicals and solvents were purchased from Sigma-Aldrich. All rea-gents and solvents were reagent grade and used without further purification if not otherwise specified.
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