Transmission electron microscopy (TEM) images and high-resolution TEM (HRTEM) images were captured by Talos F200X electron microscope. Scanning electron microscopy (SEM) images were taken by Nova NanoSEM 450 electron microscope. Energy dispersive spectrometry (EDS) mapping (Talos F200X) and X-ray fluorescence (XRF) (EAGLE III) were used to analyze the composition of elements in nanospheres. The X-ray diffraction (XRD) analysis of samples were operated on X’Pert3 Powder. X-ray photoelectron spectroscopy (XPS) analysis for the valence state of elements in samples were conducted on machine of AXIS-ULTRA DLD-600W. Inductively coupled plasma-mass spectrometry (ICP-MS) analysis for the content of elements in samples was operated on PerkinElmer ELAN DRC-e. The level of DATS in BBCD was determined by thermogravimetric (TG) analyzer (Diamond TG/DTA, PerkinElmer), with an increasing rate of 20°C/min from room temperature to 650°C under air atmosphere. Fourier transform infrared spectroscopy (FT-IR) and UV–vis absorption of the samples were recorded through Nicolet iS50R (Thermo Scientific) and SolidSpec-3700 (Shimadzu) spectrophotometer. FP-6500 (Jasco) spectrometer was used to detect the fluorescence spectra. Fluorescence microscope (Nikon Ti2-U) and flow cytometer (CytoFLEX, Beckman) were used for the fluorometric analysis.
Diamond tg dta
Manufactured by PerkinElmer
Sourced in United States
The Diamond TG/DTA is a thermal analysis instrument designed for precise measurement of weight changes and thermal events in materials during heating or cooling. It provides accurate and reliable data on the thermal properties of a wide range of samples, including polymers, ceramics, and metals.
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Lab products found in correlation
Nicolet is50r, by Thermo Fisher Scientific (2 mentions)
D8 advance, by Bruker (2 mentions)
Asap 2020m, by Micromeritics (2 mentions)
System 2000, by PerkinElmer (2 mentions)
Quanta 200, by Thermo Fisher Scientific (2 mentions)
Spectrum one, by PerkinElmer (2 mentions)
Zetasizer nano, by Malvern Panalytical (2 mentions)
Nova nanosem, by Thermo Fisher Scientific (2 mentions)
Cytoflex, by Beckman Coulter (1 mentions)
Fp 6500, by Jasco (1 mentions)
Elan drc e, by PerkinElmer (1 mentions)
Solidspec 3700, by Shimadzu (1 mentions)
D5000 diffractometer, by Siemens (1 mentions)
S 4800 scanning electron microscope, by Hitachi (1 mentions)
K alpha, by Thermo Fisher Scientific (1 mentions)
Mira4, by TESCAN (1 mentions)
Themis g2 300 microscope, by Thermo Fisher Scientific (1 mentions)
Evo 18 scanning electron microscope, by Zeiss (1 mentions)
Nicolet 6700 spectrophotometer, by Thermo Fisher Scientific (1 mentions)
X ray photo electron spectroscopy xps, by Shimadzu (1 mentions)
53 protocols using diamond tg dta
1
Multimodal Characterization of Nanospheres
2
Thermal Stability of Lipid Emulsions
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The thermal stability of raw LE, LE-NPs, and Poloxamer 188 was detected using a TG analyzer (Diamond TG/DTA; PerkinElmer, Waltham, MA, USA). A 6 mg sample was placed in an inert gas atmosphere (N2) and heated from 40°C to 600°C at a constant heating rate of 10°C/min.
3
Thermal Stability Analysis of Samples
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The thermal stability of the samples were checked by thermogravimetry (TG) analyzer (Diamond TG/DTA PerkinElmer, Waltham, MA, USA). The samples were heated from 50 °C to 400 °C at a 10 °C/min of constant heating rate in nitrogen.
4
Structural and Surface Analysis of Nanofibers
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The crystal structure of the as-prepared nanofibers was characterized using powder X-ray diffraction [XRD, Siemens D-5000 diffractometer with Cu–Kα irradiation (λ = 1.5406 Å)]. The microstructure of the samples was characterized using a HITACHI S4800 scanning electron microscope (SEM), a transmission electron microscope (TEM), and a high-resolution TEM operating at 200 kV. The samples were also analyzed by X-ray photoelectron spectroscopy (XPS, Surface Science Instruments S-probe spectrometer). The Raman spectrum was acquired at room temperature with excitation laser lines of 514 nm (Renishaw). Specific surface areas were measured using a Tristar II 3020 instrument by adsorption of nitrogen at 77 K. The pore diameter distribution of the mesopores was tested by nitrogen adsorption/desorption analysis (MicroActive ASAP 2460). The thermal gravimetric analysis was recorded on a thermogravimetric analyzer (TGA, PerkinElmer, Diamond TG/DTA) with a heating rate of 10 °C min−1 in air from 30 to 800 °C.
5
Multimodal Characterization of MOC Precursor
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SEM was performed at 10 kV on a TESCAN MIRA4 with EDS analysis at 15 kV. XPS was carried out on a Thermo Scientific K-Alpha. XRD was performed on a Bruker C2 Discover X-ray powder diffractometer. The temperature of CP with the MOC precursor during the high-temperature shock process was recorded on a Fluke Process Instrument E1RH-R59-V-0-0. TEM images were obtained using an aberration-corrected FEI Titan Themis G2 300 microscope. Thermogravimetric analysis (TGA) was performed by Diamond TG/DTA (PerkinElmer Instruments) at a heating rate of 20 °C/min in Ar gas. Fourier transform infrared (FTIR) spectra were collected using a Nicolet iS50R (Thermo Scientific). The Co K-edge XANES data were recorded in transmission mode and analyzed using the IFEFFIT program. Co foil, CoO, and Co3O4 were used as references.
6
Comprehensive Characterization of Graphene Oxide
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X-ray diffraction (XRD) analysis using D8 Advance (BRUKER, GER) with Cu Kα radiation (λ = 0.154 nm) was utilized to record the diffraction pattern of GO and f-GNs. The Fourier Transform Infrared (FTIR) spectrum of the GO and f-GNs nanoplates were recorded using a Nicolet 6700 spectrophotometer (Thermo, USA). The sample/KBr ratio in the FTIR studies was about 1/100. The chemical components of GO and f-GNs were studied by X-ray photo-electron spectroscopy (XPS) (Kratos, UK). The morphologies of the original raw GO and f-GNs nanoplates were investigated by Tecnai F20 Transmission Electron Microscopy (TEM) (FEI, USA). The alcohol suspensions of GO and f-GNs were spread on a 200-mesh copper grid for TEM imaging. The surface topography of the sol–gel coatings on the copper alloy was observed by an EVO18 Scanning Electron Microscope (SEM) (Zeiss, GER). Scanning Probe Microscope (SPM) (Vecco, USA) analysis was used to characterize the thickness of GO and f-GNs and the roughness of sol–gel coatings. Thermogravimetric analysis (TGA) was carried out using Diamond TG/DTA (PerkinElmer, USA). The temperature range was 30 °C to 1000 °C at a ramp rate of 10 °C min−1 under nitrogen atmosphere. The average diameter of the graphene distributed in sol was characterized by a S3500 wet and dry laser particle size analyzer (Microtrac, USA).
7
Comprehensive Material Characterization Protocol
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X-ray diffraction of the samples was carried out using Bruker D8 Advance Twin-Twin equipment using Cu-Kα (1.5404 Å) radiation. Powdered samples were dispersed and pressed on the glass plate before taking XRD of the sample. Transmission electron microscopy images of the samples were taken using JEOL JEM 2100 HRTEM operating at 200 kV. Powdered samples were dispersed in ethanol and sonicated and were taken on a carbon grid before TEM measurements. Thermogravimetric analysis (TGA) was performed with a Perkin Elmer, Diamond TG/DTA in a nitrogen atmosphere in the temperature range 15–900 °C at 20 °C/min. Vibrating Sample Magnetometer measurements of the powder samples were performed using Quantum Design Dynacool PPMS in the field range ±50 KOe at 300 K. PL studies of the samples were investigated using an inVia Reflex Raman spectrometer attached with a laser of excitation wavelength 405 nm (Renishaw, UK, Model No. M-9836-3991-01-A).
8
Thermal Characterization of Drug Formulations
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The thermal profile of RSP, CDs, physical mixtures and kneaded products was evaluated using a Perkin-Elmer DIAMOND TG/DTA instrument. For this purpose samples of about 3–4 mg were placed in aluminum crucibles and were analyzed under air atmosphere at a flow rate of 100 mL min−1, over the temperature range of 40–500 °C, with heating rate of 10 °C min−1.
9
Thermogravimetric Analysis of Materials
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Thermogravimetric analysis was performed on Perkin-Elmer Diamond TG/DTA with 20 mL/min high-purity nitrogen as purge gas, and the scan rate of the gas was 10 °C/min from 0 to 800 °C.
10
Comprehensive Characterization of Composite Materials
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The morphology of the composites is observed by the scanning electron microscopy (SU-8100, Hitachi Manufacturing Co., Ltd., Tokyo, Japan), equipped with an energy dispersive spectroscopy system. The X-ray diffractometer (XRD-6000, Shimadzu Co., Ltd., Tokyo, Japan) with a Cu Kα radiation source (radiation = 0.154 nm, 2θ = 10°~90°) and the Raman spectrum are used to analyze the composition of the as prepared materials, which is operated on a Renish in Via Raman system and the Raman shifts are collected in the range of 1000~2000 cm−1. The pore size distribution and the surface area of the composites is evaluated by the analysis of nitrogen adsorption-desorption data on an ASAP 2020M (Micromeritics Instrument Corp., Norcross, GA, USA). Thermogravimetric analysis (TGA) was carried out using Perkin Elmer Diamond TG/DTA (Perkin Elmer Co., Ltd, Waltham, Massachusetts, USA) instrument at a heating rate of 10 °C min−1 from 20 °C to 900 °C under air.
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