Xpert 3 x ray diffractometer

Manufactured by Malvern Panalytical

The XPERT-3 X-ray diffractometer is a laboratory instrument designed for the analysis of crystalline materials. It utilizes X-ray diffraction technology to provide detailed information about the atomic and molecular structure of a wide range of materials. The core function of the XPERT-3 is to collect and analyze X-ray diffraction patterns, which can be used to identify unknown crystalline substances, determine the crystal structure of materials, and quantify the composition of multi-phase samples.

Automatically generated - may contain errors

Lab products found in correlation

K alpha xps spectrometer, by Thermo Fisher Scientific (1 mentions) Rf 5301pc spectrometer, by Shimadzu (1 mentions) A300 spectrometer, by Bruker (1 mentions) Fluotime 200 spectrometer, by PicoQuant (1 mentions) Tecnai f20, by Thermo Fisher Scientific (1 mentions) Evo ma10, by Zeiss (1 mentions) Uv 3600 spectrophotometer, by Shimadzu (1 mentions)

Spelling variants of this product

X-ray diffractometer (112 citations) XPERT-3 X-ray (2 citations)

3 protocols using xpert 3 x ray diffractometer

XRPD Analysis of Palbociclib Solid Dispersion

Check if the same lab product or an alternative is used in the 5 most similar protocols

Example 11

The palbociclib solid dispersion prepared with PVP-VA64 in Example 4 was sent for XRPD test. The XRPD test was performed with Panalytical's XPERT-3 X-ray diffractometer. About 10 mg of sample was evenly tiled on a monocrystalline silicon sample tray and subjected to the XRPD test with the following parameters: scanning range (2θ°): 3-40; scanning step (2θ°):0.0263; scanning time (seconds): 46.665; K-Alpha wavelength (Å): 1.54060; K-Alpha2 wavelength (Å): 1.54443; Power setting: 40 mA, 45 kV. The obtained XRPD pattern was shown in FIG. 8.

US11464779B2. Pharmaceutical formulation of palbociclib and a preparation method thereof (2022-10-11). Shenzhen Pharmacin Co., Ltd. [CN]. Inventors: Zeren Wang [US], Jun Xu [US], Long Qu [CN].

+ Open protocol

+ Expand

XRPD Characterization of Palbociclib Solid Dispersion

Check if the same lab product or an alternative is used in the 5 most similar protocols

Example 10

The palbociclib solid dispersion prepared with PVP-K30 in Example 3 and the API of palbociclib both were sent for XRPD test. The XRPD test was performed with Panalytical's XPERT-3 X-ray diffractometer. About 10 mg of sample was evenly tiled on a monocrystalline silicon sample tray and subjected to the XRPD test with the following parameters: scanning range (2θ°): 3-40; scanning step (2θ°):0.0263; scanning time (seconds): 46.665; K-Alpha wavelength (Å): 1.54060; K-Alpha2 wavelength (Å): 1.54443; Power setting: 40 mA, 45 kV. The obtained XRPD pattern of the API of palbociclib was shown in FIG. 6; and the XRPD pattern of the solid dispersion prepared with PVP-K30 was shown in FIG. 9.

US11464779B2. Pharmaceutical formulation of palbociclib and a preparation method thereof (2022-10-11). Shenzhen Pharmacin Co., Ltd. [CN]. Inventors: Zeren Wang [US], Jun Xu [US], Long Qu [CN].

+ Open protocol

+ Expand

Comprehensive Characterization of Nanomaterials

Check if the same lab product or an alternative is used in the 5 most similar protocols

The surface morphology was observed by Zeiss EVO MA10 scanning electron microscope (SEM) and FEI Tecnai F20 field-emission transmission electron microscope (TEM). The elemental mapping was collected by the FEI Tecnai F20 equipped with an energydispersive X-ray spectroscope (EDS) under STEM mode. X-ray diffraction (XRD) patterns were measured with PANalytical X'Pert3 X-ray diffractometer. X-ray photoelectron spectroscopy (XPS) was performed by the Thermo Scientific K-Alpha + XPS spectrometer. All binding energies were calibrated with respect to C 1 s peak at 284.8 eV. Electron paramagnetic resonance (EPR) spectra were measured with a Bruker A300 spectrometer. Raman spectra were collected by a HORIBA iHR320 Raman microscope with a 514-nm laser. UV-visible absorption spectra were measured using Shimadzu UV-3600 spectrophotometer with an integrated sphere. Photoluminescence (PL) spectra were analyzed using Shimadzu RF-5301PC spectrometer. Time-resolved photoluminescence (TRPL) spectra were measured by the PicoQuant Fluo Time 200 spectrometer coupled with a TimeHarp 260 time-correlated single-photon counting (TCSPC) system.

Peng Y., Du M., Zou X., Jia G., Permatasari Santoso S., Peng X., Niu W., Yuan M, & Hsu H.Y. (2022). Suppressing photoinduced charge recombination at the BiVO₄||NiOOH junction by sandwiching an oxygen vacancy layer for efficient photoelectrochemical water oxidation. Journal of colloid and interface science, 608(Pt 2).

+ Open protocol

+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Revolutionizing how scientists
search and build protocols!