D8 venture apex diffractometer
The D8 VENTURE APEX diffractometer is a versatile laboratory instrument designed for X-ray diffraction analysis. It provides high-resolution data collection capabilities for a wide range of sample types and applications.
Lab products found in correlation
3 protocols using d8 venture apex diffractometer
X-Ray Structural Analysis of Organic Compounds
Single Crystal X-ray Diffraction Analysis
of
on a MiTeGen loop with grease and examined on a Bruker D8 VENTURE
APEX diffractometer equipped with a photon 100 CCD area detector at
296 (2) K using graphite-monochromated Mo Kα radiation (λ
= 0.71073 Å). Data were collected using the APEX-II software,29 integrated using SAINT30 and corrected for absorption using a multiscan approach (SADABS).31 Final cell constants were determined from full
least squares refinement of all observed reflections. The structure
was solved using intrinsic phasing (SHELXT).32 (link) All non-H atoms were located in subsequent difference maps and refined
anisotropically with SHELXL-2014/7.33 H-atoms
on carbons were added at calculated positions and refined with a riding
model. O–H atoms were located in the difference map and refined
isotropically with U(iso) riding on O with DFIX constraints applied.
The structures of
with the CCDC (CCDC deposition numbers 1945208–1945210).
Single Crystal X-ray Diffraction Analysis
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