The catalysts were tested in the HDO of palmitic acid (PA); Sigma Aldrich >99%; as a model compound of fatty acids. For each test, 0.1 g of the catalyst was used with 40 mL of a solution containing PA (39 mM) in n-dodecane (Sigma Aldrich, anhydrous > 99%). The catalysts were tested in a Parr reactor (100 mL) at 280 °C and 5.2 MPa of H2 pressure for 6 hours. The time evolution of the reaction was observed by withdrawing aliquots each hour and analyzing them on a gas chromatograph. Product identification was analyzed on a Hewlett Packard GC-MS instrument with a FID.
N dodecane
Manufactured by Merck Group
Sourced in United Kingdom, United States, Belgium, Germany, Israel
N-dodecane is a clear, colorless, and odorless liquid hydrocarbon compound with the chemical formula CH3(CH2)10CH3. It is a saturated aliphatic compound that is commonly used as a laboratory solvent and chemical reagent.
Automatically generated - may contain errors
Lab products found in correlation
Toluene, by Merck Group (6 mentions)
N hexadecane, by Merck Group (5 mentions)
Dichloromethane, by Merck Group (4 mentions)
N decane, by Merck Group (4 mentions)
Cdcl3, by Merck Group (4 mentions)
Toluene, by Thermo Fisher Scientific (4 mentions)
Dimethyl sulfoxide (dmso), by Merck Group (3 mentions)
2 2 2 trifluoroethyl methacrylate, by Merck Group (3 mentions)
Tetrahydrofuran, by Merck Group (3 mentions)
N octane, by Merck Group (3 mentions)
N hexane, by Merck Group (3 mentions)
Lucifer yellow, by Merck Group (2 mentions)
Stearyl methacrylate, by Merck Group (2 mentions)
Dimethyl sulfoxide (dmso), by Thermo Fisher Scientific (2 mentions)
Ethanol, by Thermo Fisher Scientific (2 mentions)
Dichloromethane, by Thermo Fisher Scientific (2 mentions)
4 4 azobis 4 cyanopentanoic acid, by Merck Group (2 mentions)
Benzyl methacrylate, by Merck Group (2 mentions)
Celltiter 96 aqueous one solution reagent, by Promega (2 mentions)
Dapi fluoromount, by Southern Biotech (2 mentions)
48 protocols using n dodecane
1
Hydrodeoxygenation of Fatty Acids
2
Protective Effects of BBD on Oxidative Stress
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Dimethylsulfoxide (DMSO), lucifer yellow, n-Dodecane, phosphate buffered saline (PBS), theophylline, and verapamil were obtained from Sigma-Aldrich Chemical (St. Louis, MO, USA). Porcine polar brain lipid (PBL) was purchased from Avanti Polar Lipids Inc. (Alabaster, AL, USA). 2′,7′-Dichlorodihydrofluorescein diacetate (H2DCF-DA) was obtained from Molecular Probe (Eugene, Oregon, USA). Fetal bovine serum (FBS) was obtained from Gibco Invitrogen (Grand Island, NY, USA). Dulbecco’s Modified Eagle’s medium (DMEM) were purchased from GIBCO (Grand Island, NY, USA). Anti-phospho-p38, ERK, JNK, and β-actin antibodies were purchased from Abcam (Cambridge, UK). Anti-Akt1 (pSer473) antibody was purchased from Calbiochem (Darmstadt, Germany). 3-bis (3-methoxybenzyl) butane-1,4-diol (BBD) was kindly provided from Joben Bio-Medical Co. (Kaohsiung, Taiwan).
3
Phantom Validation for Diffusion Brain Imaging
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Validation of the acquisition and analysis pipeline was performed by measurements on three phantoms consisting of 15 mm Eppendorf tubes containing either a lyotropic liquid crystal, n‐dodecane (Sigma‐Aldrich, Israel), or tap water. The phantoms were designed to give diffusion properties similar to the main components of healthy living brains: the liquid crystal phantom captures anisotropic diffusion within WM, the dodecane phantom mimics slow isotropic diffusion in the GM, and the water phantom approximates the fast isotropic diffusion of CSF. The liquid crystal is given the nickname “hex” for its reverse hexagonal phase structure, and was prepared according to the protocol described in detail by Nilsson et al52 using 41.94 wt% H2O of Milli‐Q quality, 44.12 wt% of the detergent sodium 1,4‐bis(2‐ethylhexoxy)‐1,4‐dioxobutane‐2‐sulfonate (Sigma‐Aldrich, Sweden), and 13.94 wt% of the hydrocarbon 2,2,4‐trimethylpentane (Sigma‐Aldrich, Sweden).
4
Controlled Radical Polymerization Protocols
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Stearyl
methacrylate (SMA), 2,2,2-trifluoroethyl
methacrylate (TFEMA), n-dodecane, trimethylamine,
butylhydroxytoluene (BHT), tetrahydrofuran (THF), toluene, 2,2-azobis(2-methylpropionitrile)
(AIBN), lauroyl peroxide (Luperox), ruthenium(IV) oxide hydrate, and
sodium periodate were all purchased from Sigma-Aldrich (UK). Monomers
were passed through basic alumina to remove inhibitor prior to use. tert-Butyl peroxy-2-ethylhexanoate (Trigonox 21S, or T21s)
initiator was supplied by AkzoNobel (The Netherlands). d-Chloroform (CDCl3) was purchased from VWR (UK), d2-dichloromethane (CD2Cl2) was obtained from Cambridge Isotope Laboratory (USA), and the 4-cyano-4-((2-phenylethanesulfonyl)thiocarbonylsulfanyl)pentanoic
acid (PETTC) RAFT agent was prepared in-house according to a previously
reported protocol.93 (link) Unless stated otherwise,
deionized water (pH 6) was used for all experiments.
methacrylate (SMA), 2,2,2-trifluoroethyl
methacrylate (TFEMA), n-dodecane, trimethylamine,
butylhydroxytoluene (BHT), tetrahydrofuran (THF), toluene, 2,2-azobis(2-methylpropionitrile)
(AIBN), lauroyl peroxide (Luperox), ruthenium(IV) oxide hydrate, and
sodium periodate were all purchased from Sigma-Aldrich (UK). Monomers
were passed through basic alumina to remove inhibitor prior to use. tert-Butyl peroxy-2-ethylhexanoate (Trigonox 21S, or T21s)
initiator was supplied by AkzoNobel (The Netherlands). d-Chloroform (CDCl3) was purchased from VWR (UK), d2-dichloromethane (CD2Cl2) was obtained from Cambridge Isotope Laboratory (USA), and the 4-cyano-4-((2-phenylethanesulfonyl)thiocarbonylsulfanyl)pentanoic
acid (PETTC) RAFT agent was prepared in-house according to a previously
reported protocol.93 (link) Unless stated otherwise,
deionized water (pH 6) was used for all experiments.
5
Characterization of Al Alloy 7075 Wettability
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Al alloy (7075) samples
were purchased from Northwest Institute of Nonferrous Metal Company,
and the composition is shown inTable 1 . n-Dodecane and hexadecane were purchased
from Sigma-Aldrich. Absolute ethanol, acetone glycerol, ethylene glycol,
olive oil, dichloroethane, and chloroform were from Jilin Hao Di Chemical
Reagent Ltd. Fluoroalkyl silane (1H,1H,2H,2H-perfluorooctyltriethoxysilane)
was purchased from Aladdin.
were purchased from Northwest Institute of Nonferrous Metal Company,
and the composition is shown in
from Sigma-Aldrich. Absolute ethanol, acetone glycerol, ethylene glycol,
olive oil, dichloroethane, and chloroform were from Jilin Hao Di Chemical
Reagent Ltd. Fluoroalkyl silane (1H,1H,2H,2H-perfluorooctyltriethoxysilane)
was purchased from Aladdin.
6
Synthesis and Immobilization of Transaminase Biocatalyst
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Acetone (≥99.9%), (3-aminopropyl)triethoxysilane (APTES; ≥ 98%), 4′-bromoacetophenone (BAP; ≥ 98%), n-dodecane (≥90%), hydrochloric acid (37% wt, aqueous solution), pyridoxal 5′-phosphate hydrate (PLP; ≥ 98%), sodium cyanoborohydride solution (5.0 M in 1 M NaOH; NaBH3CN), sodium hydroxide aqueous solution (50%), sodium pyruvate (≥99%), tetraethyl orthosilicate (TEOS; ≥ 98%), toluene (≥99.8%, anhydrous), trimethyltetradecylammonium bromide (TTAB; ≥ 99%) were purchased from Sigma-Aldrich. 4-Bromo-α-methylbenzylamine (BMBA; ≥ 99%; racemate), dibasic potassium phosphate (≥99%), dimethylsulfoxide (DMSO; ≥ 99.8%) and monobasic potassium phosphate (≥99%) were purchased from Acros Organics. d -Alanine (≥99%) was purchased from CarlRoth. Tetrahydrofuran (THF; ≥ 99.6%) was purchased from VWR Chemicals. Heat-shrinkable polytetrafluoroethylene (PTFE) tube was purchased from RS Components. Codexis generously supplied ATA-117 transaminase. Distilled water was applied for all synthesis and treatment processes.
7
Enzymatic Biocatalysis Protocols
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Ru1 , Ru2 , Ru3 , and n-dodecane were purchased from Sigma-Aldrich and used without further purification. Except for OleT, the genes of all the other enzymes were synthesized from Gene Universal. The recombinant E. coli strains were engineered using standard molecular cloning techniques by restriction enzymes or Gibson assembly. All the other chemicals were purchased from commercial suppliers and used without further purification. See Supplementary Table 1 for all the primers used in this study.
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8
Synthesis and Characterization of Glycerol Monomethacrylate Copolymers
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All reagents were used as received unless
otherwise stated. Benzyl methacrylate (BzMA), n-dodecane,
2-cyano-2-propyl benzodithioate (CPDB), and 4,4′-azobis-4-cyanopentanoic
acid (ACVA) were purchased from Sigma-Aldrich (UK). BzMA inhibitor
was removed by passing this monomer through an inhibitor removal column.
Ethanol, dichloromethane, DMSO, and DMF were purchased from Fisher
Scientific (UK). Glycerol monomethacrylate (GMA) was kindly
donated by GEO Specialty Chemicals (Hythe) and used without further
purification. 2-Hydroxypropyl methacrylate (HPMA) was purchased from
Alfa Aesar (UK) and contained 0.07 mol % dimethacrylate impurity,
as judged by high performance liquid chromatography (HPLC). Deuterated
mEthanol (d4-CD3OD), dimethyl
sulfoxide (d6-DMSO), and dimethylformamide
(d7-DMF) NMR solvents were purchased from
Goss Scientific (UK). Deionized water was obtained using an Elga Elgastat
Option 3A water purifier; its pH was approximately 6.2, and its surface
tension was 72.0 mN m–1 at 20 °C.
otherwise stated. Benzyl methacrylate (BzMA), n-dodecane,
2-cyano-2-propyl benzodithioate (CPDB), and 4,4′-azobis-4-cyanopentanoic
acid (ACVA) were purchased from Sigma-Aldrich (UK). BzMA inhibitor
was removed by passing this monomer through an inhibitor removal column.
Ethanol, dichloromethane, DMSO, and DMF were purchased from Fisher
Scientific (UK). Glycerol monomethacrylate (GMA) was kindly
donated by GEO Specialty Chemicals (Hythe) and used without further
purification. 2-Hydroxypropyl methacrylate (HPMA) was purchased from
Alfa Aesar (UK) and contained 0.07 mol % dimethacrylate impurity,
as judged by high performance liquid chromatography (HPLC). Deuterated
mEthanol (d4-CD3OD), dimethyl
sulfoxide (d6-DMSO), and dimethylformamide
(d7-DMF) NMR solvents were purchased from
Goss Scientific (UK). Deionized water was obtained using an Elga Elgastat
Option 3A water purifier; its pH was approximately 6.2, and its surface
tension was 72.0 mN m–1 at 20 °C.
9
Solvent-Assisted Synthesis of Nanoparticles
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n-Dodecane
(nDD) (99%), acetic acid (AA) (99.85%), n-heptanol
(98%), ZnO, and toluene (99.6%) were purchased from Sigma Aldrich
(Taufkirchen, Bavaria, Germany).
Methanol (MeOH) (99.5%) and
ethanol (EtOH) (96%) were obtained from Fisher Scientific (Loughborough,
England, UK). All the chemical reagents were used as available.
(nDD) (99%), acetic acid (AA) (99.85%), n-heptanol
(98%), ZnO, and toluene (99.6%) were purchased from Sigma Aldrich
(Taufkirchen, Bavaria, Germany).
Methanol (MeOH) (99.5%) and
ethanol (EtOH) (96%) were obtained from Fisher Scientific (Loughborough,
England, UK). All the chemical reagents were used as available.
10
Efavirenz-Loaded Lipid Nanoparticle Formulation
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Efavirenz was obtained from VWR, USA. Dimyristoylphosphatidylcholine (DMPC) and distearoyl-phosphatidylcholine (DSPC) were purchased from Avanti Polar Lipids (Alabaster, AL, USA). Phospholipon 90H (PL-90H) was obtained from Lipoid LLC (Newark, NJ, USA). Cholesterol, n-dodecane, Roswell Park Memorial Institute media (RPMI), AB serum, Phorbol 12- myristate 13-acetate (PMA), poly-lysine and 10% fetal bovine serum (FBS) were purchased from Sigma Aldrich (St. Louis, MO, USA). Inertsil, ODS-3 was purchased from GL sciences, Torrance, CA, USA. Paraformaldehyde (PFA) was purchased from EMD Chemicals, MA, USA. DAPI fluoromount was obtained from Southern Biotech, AL, USA. Rhodamine 123 was purchased from Marker Gene Technologies, Oregon, USA. All the organic solvents were HPLC grade and obtained from Fisher Scientific (Pittsburgh, PA, USA). CellTiter 96® Aqueous One Solution Reagent was purchased from Promega, Madison, WI, USA. CellROX® Deep Red Reagent was obtained from (CAT 10422) Molecular Probes, Eugene, OR, USA.
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