The largest database of trusted experimental protocols

7 protocols using 1 6 hexanedithiol

1

Bioinspired Tissue Engineering Scaffolds

Check if the same lab product or an alternative is used in the 5 most similar protocols
Ethanol (≥99.8%), poly(ethylene glycol) (PEG, Mn = 8000 g mol−1); poly(ethylene glycol) diacrylate (PEG-DA, Mn = 700 g mol−1); 1,6-hexanedithiol (HT); triethylamine; tetrahydrofuran; toluene; pentaerythritol tetrakis (3-mercaptopropionate) (QT); Irgacure 2959; phosphate-buffered saline without calcium and magnesium (PBS) were purchased from Sigma-Aldrich. Thioglycerol (≥98%, MT) was purchased from TCI. Tetraethoxysilane (TEOS, 98%) and calcium nitrate tetrahydrate (99.0–103%) were purchased from Alfa Aesar. For preparing the Simulated Body Fluid (SBF): sodium chloride, sodium hydrogenocarbonate, dipotassium hydrogenophosphate trihydrate and calcium chloride dihydrate were purchased from Sigma-Aldrich; magnesium chloride hexahydrate from Acros Organics; sodium disulfate, potassium chloride and tris(hydroxymethylaminomethane) from Alfa Aesar. All chemicals were used as purchased.
+ Open protocol
+ Expand
2

Electrochemical Characterization of Ferrocenyl-Thiol Monolayers

Check if the same lab product or an alternative is used in the 5 most similar protocols
NaCl, KCl, KH2PO4, NaH2PO4, and NaOH were acquired from Fischer Scientific (NJ, USA). 6-Ferrocenyl-1-hexanethiol, ferrocenemethanol (FcMeOH), 6-mercapto-1-hexanol, 1,6-hexanedithiol, dimethylsulfoxide (DMSO), phosphate-buffered saline, trifluoroacetic acid (TFA), and tris(2-carboxyethyl)phosphine hydrochloride (TCEP) were obtained from Sigma-Aldrich (MO, USA). Maleimide-modified methylene blue was obtained from ATTO-TEC GmbH (Siegen, Germany), ethanol was obtained from Gold Shield Distributors (CA, USA), H2SO4 was obtained from EMD (USA), and 2 mm gold electrodes, fritted Ag|AgCl electrodes, and platinum wire were obtained from CH Instruments (TX, USA). Microcloth (2–7/8″), 1 μm monocrystalline diamond suspension, and 0.05 μm micropolish alumina powder were obtained from Buehler (IL, USA). All were used as received. We used for all electrochemical measurements an Ag/AgCl reference, a platinum counter electrode, and a CH Instrument 660D potentiostat.
+ Open protocol
+ Expand
3

Synthesis and Characterization of Thiol-Ene Hydrogels

Check if the same lab product or an alternative is used in the 5 most similar protocols
Epichlorohydrin, 2-mercaptoethanol, 5-Vinyl-2-norbornene, polybutadiene(90% 1,2-vinyl), 1,6-hexanedithiol, 1,8-octanedithiol, pentaerythritol tetraacrylate (PETA), diurethane dimethacrylate (DUDMA), pyrogallol, and 2,4-diethyl-9H-thioxanthen-9-one were purchased from Sigma-Aldrich. Bis(2-mercaptoethyl) sulfide and 1,10-Decanedithiol were purchased from TCI America. All the chemicals were used as received.
+ Open protocol
+ Expand
4

Synthesis of Metallic Nanoparticles

Check if the same lab product or an alternative is used in the 5 most similar protocols
Gold (III) chloride hydrate (HAuCl4·aq, ∼50% Au basis), silver nitrate (AgNO3, ACS reagent, ≥99.0%), chloroplatinic acid hexahydrate (H2PtCl6·6H2O, ACS reagent, ≥37.5% Pt basis), palladium chloride (PdCl2, ≥99.9%), oleylamine (70%, technical grade), 1,2-dichloropropane (99%), 1-dodecanethiol (≥98%), 1-propanethiol (99%), 1,6-hexanedithiol (>97%), hexane (technical grade), chloroform (≥99.5%) and the other chemicals used in the experiments without special mention were all purchased from Sigma-Aldrich. Concentrated hydrochloric acid (HCl, 37%) and ethanol (99.9%, absolute) were purchased from Merck. Sodium borohydride (NaBH4, ≥99.0%) was purchased from Fluka. All the reagents were used as received without further purification.
+ Open protocol
+ Expand
5

Synthetic Protocols for Polymer Characterization

Check if the same lab product or an alternative is used in the 5 most similar protocols
The following chemicals were used as received: acetone (Sigma-Aldrich, ≥99.0%), chloroform (CHCl3: VWR Chemicals, 99%), d-chloroform (CDCl3: Apollo, >99%), 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU: Sigma-Aldrich, 98%), diethyl ether (Et2O: Sigma-Aldrich, ≥99.8%), N,N dimethylformamide (DMF: Fisher Scientific, LR grade), 2,6-di-tert-butyl-4-methylphenol (BHT: Alfa Aesar, 99%), ethyl acetate (EtOAc: Fisher Scientific, LR grade), hexane (Hex: VWR Chemicals, 99%), magnesium sulfate (MgSO4: anhydrous, Fisher Scientific, LR grade), 3-mercapto-1-propanol (Tokyo Chemical Industry Ltd. UK, 96%), 1,3-propanediol (Sigma-Aldrich, 98%), propiolic acid (Acros Organics, 98%), silica gel (SiO2: Apollo Scientific, 40-63 micron), sodium chloride (NaCl: Fisher Scientific, > 99%), sodium hydrogen carbonate (NaHCO3: Fisher Scientific, >99%), sulfuric acid (Fisher Scientific, >95%), triethylamine (Et3N: Fisher Scientific, LR grade). 1,6-hexanedithiol (Sigma-Aldrich, ≥97%) was vacuum distilled prior to use and stored in Young’s tapped ampuoles under N2. Poly(l-lactic acid) (PLLA) (Ingeo™ Biopolymer 3100HP) was ordered from NatureWorks.
+ Open protocol
+ Expand
6

Synthesis and Characterization of Gold and Silver Nanoparticles

Check if the same lab product or an alternative is used in the 5 most similar protocols
Chemicals. Natural graphite (SP-1) was purchased from Bay Carbon (Bay City, MI). Gold(III) chloride hydrate (HAuCl 4 Á aq, B52% Au basis), silver nitrate (AgNO 3 , ACS reagent, Z99.0%), L-ascorbic acid (BioXtra, Z99.0%, crystalline), KMnO 4 , H 2 SO 4 (98%), H 2 O 2 (30%), hexane (technical grade), oleylamine (70%, technical grade), octylamine (99%), ODT (98%) 1-dodecanethiol (DDT,Z98%), 1-octanethiol (OT, 98.5%), 1-propanethiol (PT, 99%), 11-mercapto-1-undecanol (MUDO, 98%), 6-mercapto-1-hexanol (MHO, 97%), 11-mercaptoundecanoic acid (MUDA, 95%), 3-mercaptopropionic acid (MPA, Z99%), benzeneethanethiol (BET, 98%) and 1,6-hexanedithiol (HDT, Z97%) were purchased from Sigma-Aldrich. Sodium borohydride (NaBH 4 , Z99.0%) was purchased from Fluka. Concentrated hydrochloric acid (HCl, 37%) and ethanol (99.9%, absolute) were purchased from Merck. Ultrapure Milli-Q water (Milli-Q System, Millipore, Billerica, MA) was used in all the experiments. All the reagents were used as received without further purification.
+ Open protocol
+ Expand
7

Synthesis of Cadmium Selenide Nanocrystals

Check if the same lab product or an alternative is used in the 5 most similar protocols
Cadmium oxide (99.5%), stearic acid (SA, reagent grade, 95%), 1-octadecene (ODE, technical grade, 90%), selenium powder (100 mesh, 99.99% trace metals basis), trioctyl phosphine (TOP, 97%), silver nitrate ( puriss, ≥99.8%), trisodium citrate dihydrate (ACS reagent, ≥99.0%), sodium borohydride (ReagentPlus, 99%), glycerol (for molecular biology, ≥99.0%), hydrogen peroxide (30% w/w in water), 1,6-hexanedithiol (HDT, 96%), toluene (HPLC grade), 2-propanol (HPLC grade), methyl acetate (anhydrous, 99%), and acetonitrile (HPLC grade) were purchased from Sigma-Aldrich and used as received. Deionized (DI) water (>18 mΩ cm) was obtained from a Millipore Direct Q3 UV water purification system.
+ Open protocol
+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required

Sign up now

Revolutionizing how scientists
search and build protocols!