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2 protocols using 3 methyl 1 butanol

1

Photocurable Polymer Synthesis Protocol

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2-(Tert-butylamino)ethyl methacrylate (TBEMA, 98%), n-tert-butylethylamine (TBEA, 98%), hexyl isocyanate (98%), and bis(2,4,6-trimethylbenzoyl)-phenylphosphineoxide (Irgacure 819) were purchased from TCI (Tokyo Chemical Industry, Japan). Poly(propylene glycol) acrylate (PPGA, Mn = 475) was received from Sigma-Aldrich (USA). Hexamethylene diisocyanate (HDI, 99%), 4-hydroxybutyl acrylate (HBA, 97%) and Sudan III were obtained from Aladdin (China). 3-Methyl-1-butanol (99.5%) was provided by Macklin (China). All chemicals were used as received.
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2

Volatile Compound Identification Standards

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Standards were purchased for volatile compound identification. 2-Pentylfuran and trans-3-octen-2-one were provided by Sigma Aldrich (St. Louis, MO, USA). Other compounds, including hexanal, benzaldehyde, octanal, nonanal, heptanal, 3-methylbutanal, propanol, pentanol, hexanol, ethanol, 1-octen-3-ol, 3-methyl-1-butanol, 2-methylpropanol, phenethyl alcohol, acetoin, 6-methyl-5-hepten-2-one, 2,3-butanedione, acetic acid, octanoic acid, pentanoic acid, hexanoic acid, γ-undecalactone, ethyl acetate, hexyl acetate, were provided by Macklin (Shanghai, China).
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