Antimony 3 iodide

Manufactured by Merck Group

Antimony(III)iodide is a chemical compound with the formula SbI3. It is a crystalline solid that is used as a laboratory reagent.

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Lab products found in correlation

Oleic acid, by Thermo Fisher Scientific (1 mentions) Sodium thiocyanate, by Merck Group (1 mentions) Hexane, by Thermo Fisher Scientific (1 mentions) Methanol, by Thermo Fisher Scientific (1 mentions) Tin 2 acetate, by Merck Group (1 mentions) 1 octadecene, by Merck Group (1 mentions) 2 methylimidazole, by Merck Group (1 mentions)

Close spelling variants of this product

Antimony

2 protocols using antimony 3 iodide

Synthesis of Metal Halide Nanocrystals

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1-Octadecene (ODE, technical grade, 90%),
potassium thiocyanate (KSCN, 99%) sodium thiocyanate (NaSCN, 98%),
and tin(II) acetate (Sn(OAc)₂) from Sigma-Aldrich; antimony(III)
iodide (SbI₃, 99.9%), bismuth(III) iodide (BiI₃, 99.999%), tin(II) iodide (SnI₂, 99%), tin(II) sulfate
(SnSO₄, 95%), and bismuth(III) chloride (BiCl₃, 99%) from Strem; oleic acid (technical grade, 90%) from Alfa Aesar;
hexanes (99.9%) and methanol (99.9%) from Fisher. All chemicals were
used as received without further purification.

Roth A.N., Porter A.P., Horger S., Ochoa-Romero K., Guirado G., Rossini A.J, & Vela J. (2024). Lead-Free Semiconductors: Phase-Evolution and Superior Stability of Multinary Tin Chalcohalides. Chemistry of Materials, 36(9), 4542-4552.

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Synthesis of (2-MIm)SbI4 Crystals

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The starting materials were commercial antimony(III) iodide (Sigma-Aldrich, ≥99.8%) and 2-methylimidazole (Sigma-Aldrich, ≥99%). (2-MIm)SbI 4 crystals were prepared by dissolving stoichiometric amounts of SbI 3 and 2-MIm in diluted HI solution. Dark red, plate-like single crystals were grown from an aqueous solution by slow evaporation at constant room temperature (300 K).

Gągor A., Banach G., Węcławik M., Piecha-Bisiorek A, & Jakubas R. (2017). The lone-pair-electron-driven phase transition and order-disorder processes in thermochromic (2-MIm)SbI₄ organic-inorganic hybrid. Dalton transactions (Cambridge, England : 2003), 46(47).

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