Thermal studies (TGA/DTG) were carried out on TGA/DSC 3 + Thermogravimetric Analyzer (Mettler Toledo Corp., Zurich, Switzerland) and the samples were heated up to 1000 °C at rate of 10 °C·min−1 in an inert nitrogen atmosphere.
Tga dsc 3 thermogravimetric analyzer
Manufactured by Mettler Toledo
Sourced in Switzerland
The TGA/DSC 3+ thermogravimetric analyzer is a laboratory instrument designed to measure the changes in the weight and thermal properties of a sample as a function of temperature or time. It can perform both thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) measurements simultaneously.
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Lab products found in correlation
7 protocols using tga dsc 3 thermogravimetric analyzer
1
Thermal Analysis of Materials
2
Thermogravimetric Analysis of Gel Moisture
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Thermogravimetric analysis (TGA) was performed by using a TGA/DSC 3+ thermogravimetric analyzer (Mettler Toledo, Greifensee, Switzerland) to study the residual moisture content of the gels before and after vacuum drying. Samples were exposed first to dry N2 for 10 min at 25°C, and then heated to 120°C (10°C min−1) and held for 1 hour, before being cooled back to 25°C.
3
Thermal Decomposition of Epoxy Resin
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In order to obtain the TG/DSC curves of epoxy resin decomposition in SF6/N2 mixture, TGA/DSC 3+ thermogravimetric analyzer of Mettler Toledo company was used in the experiment. At first three parameters including thermal conductivity, density and specific heat capacity were calculated in order to keep the accuracy of experiments after filling them in the sheet of parameters of TG/DSC instrument.
4
Thermal Analysis of Materials
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Thermogravimetric analysis (TG) of the materials was performed on a thermal analyzer (NETZSCH STA449F3, NETZSCH, Selb, Germany) with a gas flow rate of 80 mL/min under nitrogen atmosphere. The heating rate was 10 °C/min and the temperature ranged from 40 °C to 800 °C.
Thermogravimetric analysis–Fourier transform infrared spectroscopy (TG–FTIR) was performed via a TGA/DSC3 thermogravimetric analyzer (METTLER TOLEDO, Greifensee, Switzerland) linked with a Nicolet FTIR IS50 spectrometer (Thermo Fisher) at a heating rate of 10 °C/min within a temperature range of 40 °C to 800 °C under a N2 flow of 50 mL/min. The temperature of the transfer line in the TG–FTIR system was 200 °C.
Thermogravimetric analysis–Fourier transform infrared spectroscopy (TG–FTIR) was performed via a TGA/DSC3 thermogravimetric analyzer (METTLER TOLEDO, Greifensee, Switzerland) linked with a Nicolet FTIR IS50 spectrometer (Thermo Fisher) at a heating rate of 10 °C/min within a temperature range of 40 °C to 800 °C under a N2 flow of 50 mL/min. The temperature of the transfer line in the TG–FTIR system was 200 °C.
5
Thermal Analysis of Novel Compounds
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All chemical precursors and reactants were acquired from standard suppliers and used as received. The synthesis of precursors 2, 3, 4, 5, 8, 10, and 11 has been carried out according to literature procedures.[17 , 27 , 28 ] DSC was performed on Thermal Analysis DSC 3+ from Mettler Toledo. Thermogravimetric analysis (TGA) was performed on a TGA/DSC 3+ – Thermogravimetric Analyzer with high temperature furnace (HT) from Mettler Toledo under nitrogen flow with a heating rate of 10 °C min−1 from 25 to 300 °C.
6
Analytical Characterization of Materials
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All chromatographic analyses were conducted on SHIMADZU series high performance liquid chromatography system, which consists of LC-10ATVP pump, CTO-10ASVP column oven, equipped with SIL-10AVP injection valve and SPD-M10AVP UV detector. Fourier transform infrared spectroscopy (FTIR) was obtained on an IRTracer-100 Fourier transform infrared spectrometer (Shimadzu, Kyoto, Japan). Thermogravimetric analysis (TGA), Differential Scanning Calorimetry (DSC) and Derivatives Thermogravimetry (DTG) were performed on a TGA/DSC 3+ Thermogravimetric Analyzer (Mettler Toledo, Columbus, OH, USA) at room temperature to 800 °C at a heating rate of 10 °C/min. Nitrogen adsorption and desorption were performed on an ASAP2020 nitrogen adsorption and desorption instrument (Micromeritics, Norcross, GA, USA).
7
Characterization of MOF@Substrate Structures
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JEOL JSM 7000 scanning electron microscopy
(SEM) was used to characterize morphologies of the obtained structures.
Fourier transform infrared (FTIR) characterization was done on Thermal
Nicolet 6700. Samples were scanned 64 times, and spectra were obtained
with wavelengths from 4000 to 500 cm–1. Gas sorption
data were collected using a Quantachrome Instrument (v 5.2) at 77
K measuring nitrogen adsorption. Samples were previously degassed
for 24 h at 393 K. Thermogravimetric analysis (TGA) was performed
using a Mettler TGA/DSC 3+ thermogravimetric analyzer. Thermograms
were recorded at a heating rate of 10 °C/min between 37 and 600
°C in a flow of argon at 20 mL/min. X-ray diffraction (XRD) of
MOF@substrate structures was carried out on a Bruker D8 ADVANCE powder
diffractometer with a scan speed of 1° min–1, a step size of 0.01°, and a 2θ range of 2–45°.
(SEM) was used to characterize morphologies of the obtained structures.
Fourier transform infrared (FTIR) characterization was done on Thermal
Nicolet 6700. Samples were scanned 64 times, and spectra were obtained
with wavelengths from 4000 to 500 cm–1. Gas sorption
data were collected using a Quantachrome Instrument (v 5.2) at 77
K measuring nitrogen adsorption. Samples were previously degassed
for 24 h at 393 K. Thermogravimetric analysis (TGA) was performed
using a Mettler TGA/DSC 3+ thermogravimetric analyzer. Thermograms
were recorded at a heating rate of 10 °C/min between 37 and 600
°C in a flow of argon at 20 mL/min. X-ray diffraction (XRD) of
MOF@substrate structures was carried out on a Bruker D8 ADVANCE powder
diffractometer with a scan speed of 1° min–1, a step size of 0.01°, and a 2θ range of 2–45°.
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