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Lithium hydroxide monohydrate

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Lithium hydroxide monohydrate is a chemical compound with the formula LiOH·H2O. It is a white, crystalline solid that is soluble in water. The primary function of lithium hydroxide monohydrate is to serve as a source of lithium ions and hydroxide ions in various chemical processes and applications.

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Lab products found in correlation

Sodium hydride, by Merck Group (1 mentions) Celite, by Merck Group (1 mentions) Hydrazine monohydrate, by Merck Group (1 mentions) Methyl iodide, by Merck Group (1 mentions) Triphenylphosphine, by Thermo Fisher Scientific (1 mentions) 2 iodobenzonitrile, by ABCR (1 mentions) Silver 1 carbonate, by Merck Group (1 mentions) Orion star a111 benchtop ph meter, by Thermo Fisher Scientific (1 mentions) Sodium hydroxide (naoh), by Merck Group (1 mentions) Potassium hydroxide, by Merck Group (1 mentions) Chelex 100 sodium form, by Merck Group (1 mentions) Cesium hydroxide monohydrate, by Merck Group (1 mentions) Rubidium hydroxide hydrate, by Thermo Fisher Scientific (1 mentions)

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Lithium hydroxide (3 citations)

2 protocols using lithium hydroxide monohydrate

1

Synthesis of Indolo[2,3-d]benzazepinone Derivatives

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2-Iodobenzonitrile, ethyl-1H-indole-carboxylate and 5-bromo-ethyl-1H-indole-carboxylate were purchased from ABCR. Borane solution (1M in THF), absolute DMF, dimethylaminopyridine, di-tert-butyl-dicarbonate, absolute acetonitrile, palladium(II) acetate, sodium bicarbonate, basic aluminuim oxide, 2-acetylpyridine and 2-formylpyridine were bought from Fisher/Acros Organics. Ethoxy-methylchloride was obtained form TCI. Sodium hydride, phosphorus(V) sulfide, celite, hydrazine monohydrate and methyl iodide were purchased from Sigma Aldrich, while lithium hydroxide monohydrate and triphenylphosphine were from Alfa Aesar. 1-Ethyl-3-(3-dimethylaminopropyl)carbodiimide-hydrochloride was purchased from IRIS biotech. Silver(I) carbonate was purchased from Merck. 2-Iodobenzylamine was prepared by a known method.26 (link) The unsubstituted indolo[2,3-d]benzazepinone (A) was prepared by following published protocols.18 (link)–20 The 11-bromo-substituted B was prepared using reported precedures,18 (link)–20 with some modifications, a detailed description of the synthesis of B is given in the Supplementary Information file.
Bacher F., Wittmann C., Nové M., Spengler G., Marć M.A., Enyedy E.A., Darvasiova D., Rapta P., Reiner T, & Arion V.B. (2019). Novel latonduine derived proligands and their copper(II) complexes show cytotoxicity in the nanomolar range in human colon adenocarcinoma cells and in vitro cancer selectivity. Dalton transactions (Cambridge, England : 2003), 48(28), 10464-10478.
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2

Purification of Hydroxide Electrolytes

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Lithium hydroxide monohydrate (99.995% metals basis) was purchased from Alfa Aesar. Sodium hydroxide (semiconductor grade, 99.99% trace metals basis) was purchased from Sigma-Aldrich. Potassium hydroxide (semiconductor grade, 99.99% trace metals basis) was purchased from Sigma-Aldrich. Rubidium hydroxide hydrate (15 to 20% H2O, 99% metals basis) was purchased from Alfa Aesar. Cesium hydroxide monohydrate (99.95% trace metals basis) was purchased from Sigma-Aldrich. The electrolytes used for all reactivity studies were purified with Chelex resin (Sigma-Aldrich, Chelex 100 sodium form). To further remove the trace metal contamination in 0.1 M RbOH, preelectrolysis of the electrolyte in an Ar atmosphere was carried out for 2 hours using electropolished Cu foil electrodes at a constant current density of −5 mA cm−2. The electrolyte pH, which was detected using the Orion Star A111 Benchtop pH Meter (Thermo Fisher Scientific), showed no significant change after the electrolysis.
Malkani A.S., Li J., Oliveira N.J., He M., Chang X., Xu B, & Lu Q. (2020). Understanding the electric and nonelectric field components of the cation effect on the electrochemical CO reduction reaction. Science Advances, 6(45), eabd2569.
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