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2 protocols using γ methacryloxypropyl trimethoxy silane

1

Bioactive Polymer Composite Synthesis

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Poly(tetrahydrofuran ether glycol) 1000 (PTMEG 1000), 2-hydroxyethyl methacrylate (HEMA), triethylene glycol dimethacrylate (TEGDMA), dibutyltin dilaurate (DBTDL), acrylic acid (AA), isophorone diisocyanate (IPDI), 2,2-dihydroxymethylpropionic (DMPA), γ-methacryloxypropyl trimethoxy silane (γ-MTS), 2,2-dihydroxymethylpropionic, triethylenediamine, camphorquinone (CQ), ethyl-4-dimethylamino-benzoate (EDMAB), acetic acid and nHAp were purchased from Sigma Aldrich Corp, St. Louis (MO, USA). Tetrahydrofuran (THF) was supplied by Tianjin Tiantai Refine Chemicals Co., Ltd. (Tianjin, China). Peptide DDDEEKC was obtained from ChinaPeptide (Shanghai, China). Simulated body fluid (SBF) was obtained from Beijing Leagene Biotechnology Co., Ltd. (Beijing, China). Potassium hydroxide was supplied by Beijing Chemical Co. (Beijing, China).
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2

Synthesis and Characterization of Mycotoxin-Sensitive Polymeric Materials

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N-(β-aminoethyl)-γ-aminopropylmethyldimethoxysilane (AEAPMS, 97%), azobisisobutyronitrile (AIBN, 99%), methacrylic acid (MAA, 99%), γ-methacryloxypropyltrimethoxysilane (MPTMS, 99%), and anhydrous citric acid (99%) were purchased from Sigma-Aldrich (St. Louis, MO, USA, https://www.sigmaaldrich.com/). Acetonitrile and methanol were obtained from Merck (Darmstadt, Germany, http://www.merckmillipore.com/). Zearalenone (ZEA, 99%), deoxynivalenol (DON, 99%), ochratoxin (OTA, 99%), aflatoxin B1 (AFB1, 99%), patulin (99%), beauvericin (BEA, 99%), and T-2 (99%) were from Fermentek (Jerusalem, Israel, https://www.fermentek.com/). Acetic acid (99%) and other chemical reagents were provided by Sinopharm Co. (Shanghai, China, http://www.sinopharmholding.com/en/). All reagents were of analytical grade.
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