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Emstat pico module

Manufactured by PalmSens
Sourced in Netherlands

The EmStat Pico module is a compact and portable electrochemical measurement device designed for laboratory applications. It functions as a potentiostat, providing the necessary voltage and current control for electrochemical experiments. The device supports various electrochemical techniques, enabling researchers to conduct a range of analyses and measurements.

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3 protocols using emstat pico module

1

Electrochemical Nitrite Sensor Development

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Carbon screen-printed electrodes (Dropsens DRP 11L), with carbon working and counter electrodes and a Ag/AgCl reference electrode, were bought from Metrohm (Herisau, Switzerland). Tetradodecylammonium nitrate (TDDA), high-molecular-weight poly (vinyl chloride) (PVC), 2-nitrophenyl octyl ether (NPOE), tetrahydrofuran (THF) stabilized with BHT, potassium chloride, and sodium nitrate were bought from Sigma Aldrich (Burlington, MA, USA). An EmStat Pico module (portable potentiostat) was purchased from PalmSens (Houten, the Netherlands). Gaussian software Gaussian 16 W, version 1.1 (Wallingford, CT, USA), was used to perform the computational study. Illustrative sketches were drawn using BioRender. All statistical analysis was conducted using GraphPad Prism, version 9.3.1 (San Diego, CA, USA).
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2

Electrical Impedance Spectroscopy Characterization

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Measurements of electrical impedance spectroscopy (EIS) were performed at predetermined time points. Multichannel potentiostat (VPM-300) purchased from BioLogic Science Instruments (Seyssinet-Pariset, France) was used to characterize the different designs of impedance sensors. EmStat Pico module (development kit) purchased from PalmSens was used for the measurement of electrochemical signals during the cell cultures. PSTrace software (V5.8.1) was employed for the electrochemical data processing (frequency scanning range of 50 kHz–5 Hz). For electrode materials’ characterization, a classical three-electrodes cell (Ag/AgCl reference and carbon counter electrodes) was used. All other EIS experiments were conducted using the two-electrodes set-up previously described.
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3

Potentiometric Measurements with Portable Probe

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Potentiometric measurements on the eld were performed using an EmStat Pico module (Palm Sens, Houten, The Netherlands) located inside the probe. This whole module is designed around an STM32L476 microcontroller running on an operating system called Chibios. The probe is equipped with a PT1000 temperature probe using a MAX31865 chip. The data is stored internally on a microSD card located on the main board (Fig. S1 †). To perform time-based measurements, an integrated clock with a CR2032 battery is mounted internally.
To perform the calibration step, two small KMPP peristaltic pumps (Kamoer Fluid Tech, Shanghai) were added to the sensing head. The pumps are controlled by a Grove I2C Motor (TB6612) module that can control two pumps. The pumps and the main board are powered by 4 Li-ion batteries (3500 mA h-3.6 V). The main reference electrode was a simple Ag/AgCl coated wire (Metrohm AG, Switzerland).
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