Silver 1 carbonate

Manufactured by Merck Group

Silver(I) carbonate is a chemical compound with the formula Ag2CO3. It is a white, crystalline solid used as a laboratory reagent. The primary function of silver(I) carbonate is to serve as a source of silver ions in various chemical reactions and analyses.

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Lab products found in correlation

Sodium hydride, by Merck Group (2 mentions) Celite, by Merck Group (2 mentions) 2 iodobenzonitrile, by ABCR (2 mentions) Triphenylphosphine, by Thermo Fisher Scientific (1 mentions) Lithium hydroxide monohydrate, by Thermo Fisher Scientific (1 mentions) Hydrazine monohydrate, by Merck Group (1 mentions) Methyl iodide, by Merck Group (1 mentions) Phosphorus pentasulfide, by Merck Group (1 mentions) P toluenesulfonyl chloride, by Merck Group (1 mentions) Copper 2 chloride dihydrate, by Merck Group (1 mentions) Methanol, by Merck Group (1 mentions) Sodium hydroxide (naoh), by Merck Group (1 mentions)

2 protocols using silver 1 carbonate

Synthesis of Indolo[2,3-d]benzazepinone Derivatives

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2-Iodobenzonitrile, ethyl-1H-indole-carboxylate and 5-bromo-ethyl-1H-indole-carboxylate were purchased from ABCR. Borane solution (1M in THF), absolute DMF, dimethylaminopyridine, di-tert-butyl-dicarbonate, absolute acetonitrile, palladium(II) acetate, sodium bicarbonate, basic aluminuim oxide, 2-acetylpyridine and 2-formylpyridine were bought from Fisher/Acros Organics. Ethoxy-methylchloride was obtained form TCI. Sodium hydride, phosphorus(V) sulfide, celite, hydrazine monohydrate and methyl iodide were purchased from Sigma Aldrich, while lithium hydroxide monohydrate and triphenylphosphine were from Alfa Aesar. 1-Ethyl-3-(3-dimethylaminopropyl)carbodiimide-hydrochloride was purchased from IRIS biotech. Silver(I) carbonate was purchased from Merck. 2-Iodobenzylamine was prepared by a known method.^{26 (link)} The unsubstituted indolo[2,3-d]benzazepinone (A) was prepared by following published protocols.^{18 (link)–20} The 11-bromo-substituted B was prepared using reported precedures,^{18 (link)–20} with some modifications, a detailed description of the synthesis of B is given in the Supplementary Information file.

Bacher F., Wittmann C., Nové M., Spengler G., Marć M.A., Enyedy E.A., Darvasiova D., Rapta P., Reiner T, & Arion V.B. (2019). Novel latonduine derived proligands and their copper(II) complexes show cytotoxicity in the nanomolar range in human colon adenocarcinoma cells and in vitro cancer selectivity. Dalton transactions (Cambridge, England : 2003), 48(28), 10464-10478.

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Synthesis of Indolo-Benzazepin Derivatives

Cited 1 time

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2-Iodobenzonitrile,
indole-3-carboxaldehyde, and 5-bromoindole-3-carboxaldehyde
were purchased from ABCR. Borane solution (1 M in THF), absolute DMF,
4-dimethylaminopyridine (DMAP), di-tert-butyl-dicarbonate
(Boc₂O), absolute acetonitrile (ACN), palladium(II) acetate,
sodium bicarbonate, tetrabutylammoinium fluoride (TBAF), basic aluminium
oxide, and 2-formylpyridine were bought from Fisher/Acros Organics.
2-Acetylpyridine was obtained from TCI. Sodium hydride (NaH, 60% dispersion
in mineral oil), copper(II) chloride dihydrate, p-toluenesulfonyl chloride, phosphorus pentasulfide, methanol, DCM,
THF, ethyl acetate (EtOAc), hexane, celite, and hydrazine monohydrate
were purchased from Sigma-Aldrich. EDCI·HCl was obtained from
IRIS biotech, while silver(I) carbonate was purchased from Merck.
2-Iodobenzylamine was prepared by a known method.^{65 (link)} The proligands HL⁵–HL¹¹ and the corresponding
complexes 5–11 were prepared as reported previously,^{33 (link),39 (link)} while 5,12-dihydroindolo[3,2-d]benzazepin-7(6H)-one was synthesized by following a literature protocol.^{37 (link)} Absolute hydrazine was preabsoluted over sodium
hydroxide.

Kuznetcova I., Bacher F., Alfadul S.M., Tham M.J., Ang W.H., Babak M.V., Rapta P, & Arion V.B. (2022). Elucidation of Structure–Activity Relationships in Indolobenzazepine-Derived Ligands and Their Copper(II) Complexes: the Role of Key Structural Components and Insight into the Mechanism of Action. Inorganic Chemistry, 61(26), 10167-10181.

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