5 bromovanillin

Manufactured by Merck Group

Sourced in United States

5-Bromovanillin is a chemical compound used as a laboratory reagent. It is a derivative of vanillin, with a bromine atom substituted at the 5-position of the aromatic ring. 5-Bromovanillin is commonly used in analytical and organic chemistry applications, but a detailed description of its core function is not available while maintaining an unbiased and factual approach.

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2 protocols using 5 bromovanillin

Synthesis and Characterization of Vanillin Derivatives

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All solvents and substrates (acetyl, benzoyl, and p-toluoyl chloride, methyl acetoacetate, N-methylthiourea, vanillin, 5-bromovanillin, 5-iodovanillin, 5-nitrovanillin) were purchased from Sigma. Vanillic derivatives 1d–k were prepared following the procedures described previously in the literature [26 (link)]. We determined melting points (Mp) on a Mel-Temp apparatus. For recording IR spectra, we used a Perkin–Elmer Spectrum One FT-IR spectrometer on KBr pellet. A Varian Gemini 200 MHz NMR spectrometer (¹H at 200 and ¹³C at 50 MHz) was utilized for NMR characterization of compounds 4a–k. The compounds were dissolved in DMSO-d₆. ¹H and ¹³C NMR spectra are presented in Supplementary Materials (see Figures S1–S22).

Milović E., Janković N., Petronijević J., Joksimović N., Kosanić M., Stanojković T., Matić I., Grozdanić N., Klisurić O, & Stefanović S. (2022). Synthesis, Characterization, and Biological Evaluation of Tetrahydropyrimidines: Dual-Activity and Mechanism of Action. Pharmaceutics, 14(10), 2254.

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Synthesis and Characterization of Lipid Nanoparticles

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Tetronic acid, myristic acid, palmitic acid, 3-aminopyrazole, 5-bromovanillin, triethylamine (Et₃N), thionyl chloride (SOCl₂), 4-dimethylaminopyridine (DMAP), ethyl acetate (EtOAc), benzene, hexanes, ethanol (EtOH), methanol (MeOH), dimethyl sulfoxide (DMSO), dimethylformamide (DMF), methylene chloride (CH₂Cl₂), sephadex G75, phosphate buffered saline (PBS), RPMI-1640, DMEM, fetal bovine serum (FBS), MTT reagent, porcine pancreas lipase and porcine liver esterase were purchased from Sigma-Aldrich or Fisher Scientific, USA. Chloroform solutions of 1,2-distearoyl-sn-glycero-3-phosphoethanolamine-N-[methoxy(polyethylene glycol)2000] ammonium salt (DSPE-PEG2000) and 1,2-dipalmitoyl-snglycero-3-phosphocholine (DPPC) were purchased from Avanti Polar Lipids (Alabaster, USA). Lipophilic tracers DiO and DiI were purchased from Life Technologies, USA. Annexin V-FITC conjugate was ordered from Southern Biotech, USA.

Mikhalin A.A., Evdokimov N.M., Frolova L.V., Magedov I.V., Kornienko A., Johnston R., Rogelj S, & Tartis M.S. (2014). Lipophilic prodrug conjugates allow facile and rapid synthesis of high loading capacity liposomes without the need for post-assembly purification. Journal of liposome research, 25(3), 232-260.

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