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Anhydrous magnesium sulfate mgso4

Manufactured by Thermo Fisher Scientific
Sourced in Belgium

Anhydrous magnesium sulfate (MgSO4) is a drying agent used to remove water from organic solvents and other liquids. It is a white, granular, crystalline substance that is highly hygroscopic, meaning it readily absorbs water from its surroundings. Anhydrous MgSO4 is commonly used in organic chemistry laboratories to dry reaction mixtures, extracts, and other solutions prior to further processing or analysis.

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4 protocols using anhydrous magnesium sulfate mgso4

1

Synthesis of Photocurable PCL-based Hydrogels

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Poly(ε-caprolactone) diol (PCL90-diol; Mn ~10 k g/mol), trimethylamine (Et3N), acryloyl chloride, 4-dimethylaminopyridine (DMAP), 2,2-dimethoxy-2-phenylacetophenone (DMP), 1-vinyl-2-pyrrolidinone (NVP), potassium carbonate (K2CO3), sodium hydroxide (NaOH), potassium hydroxide (KOH), sodium chloride (NaCl), octamethylcyclotetrasiloxane (D4), triflic acid, hexamethyldisilazane (HMDS), ε-caprolactone, stannous 2-ethylhexanoate, sodium chloride (NaCl), sodium bicarbonate (NaCO3), potassium chloride (KCl), dipotassium hydrogen phosphate trihydrate (K2HPO4·3H2O), magnesium chloride hexahydrate (MgCl2·6H2O), calcium chloride (CaCl2), sodium sulfate (Na2SO4), phosphate buffered saline (PBS; pH 7.4), and tris(hydroxymethyl)aminomethane were obtained from Sigma-Aldrich. Anhydrous magnesium sulfate (MgSO4) was obtained from Thermo Fisher Scientific. Tetramethyldisiloxane (tetra-SiH), tetrakis(dimethylsiloxy)siloxane (tetrakis-SiH), and platinum-divinyl-tetramethyldisiloxane complex in xylene (Karstedt’s catalyst) were obtained from Gelest. Reagent-grade dichloromethane (CH2Cl2) and NMR-grade CDCl3 were dried over 4 Å molecular sieves prior to use.
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2

Synthesis and Characterization of Novel Polyurethanes

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(R)-(+)-limonene (LM), hexamethylene diisocyanate (HDI), dibutyltin dilaurate (DBTDL), and sodium tetraphenylborate (NaBPh4) were obtained from Sigma Aldrich (Saint Louis, MO, USA). Squalene (SQ) and 1,8-diazabicyclo(5.4.0)undec-7-ene (DBU) were obtained from Alfa Aesar (Thermo Fisher, Kandel, Germany). Thioacetic acid (TAA) and 2,2-dimethoxy-2-phenylacetophenone (DMPA) were obtained from Acros Organics (Thermo Fisher Scientific, Geel, Belgium). Anhydrous magnesium sulfate (MgSO4) was obtained from (Thermo Fisher Scientific, Geel, Belgium). Sodium hydroxide (NaOH), hydrochloric acid (HCl), chloroform (CHCl3), and methanol (MeOH) were obtained from Scharlab (Barcelona, Spain). All products were used as received. BGDBU, which is a base generator, was synthesized from DBU and sodium tetraphenyl borate according to a reported methodology [24 (link)].
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3

Synthesis of Photocurable Polycaprolactone-Lactide Copolymers

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Polycaprolactone diol (PCL90-diol; Mn ~10,000 g mol−1), ε-caprolactone, L-lactide, D,L-lactide, stannous 2-ethylhexanoate, triethylamine (Et3N), acryloyl chloride, 4-dimethylaminopyridine (DMAP), 2,2-dimethoxy-2-phenylacetophenone (DMP), 1-vinyl-2-pyrrolidinone (NVP), potassium carbonate (K2CO3), sodium hydroxide (NaOH), sodium chloride (NaCl), ethylene glycol and solvents were obtained from Sigma-Aldrich. Anhydrous magnesium sulfate (MgSO4) was obtained from Fisher. Reagent-grade CH2Cl2 and NMR-grade CDCl3 were dried over 4 Å molecular sieves prior to use.
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4

Synthesis of Photocurable PCL-PLLA Hydrogels

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Polycaprolactone diol (PCL90-diol; Mn ~10,000 g/mol), poly(L-lactic acid) (PLLA1700; Mn ~123,000 g/mol), ε-caprolactone, L-lactide, stannous 2-ethylhexanoate, triethylamine (Et3N), acryloyl chloride, 4-dimethylaminopyridine (DMAP), 2,2-dimethoxy-2-phenylaceto-phenone (DMP), 1-vinyl-2-pyrrolidinone (NVP), potassium carbonate (K2CO3), sodium hydroxide (NaOH), phosphate-buffered saline (PBS; 1X, pH = 7.4), ethylene glycol and solvents were obtained from Sigma-Aldrich. Anhydrous magnesium sulfate (MgSO4) was obtained from Fisher. Reagent-grade CH2Cl2 and NMR-grade CDCl3 and D2O were dried over 4 Å molecular sieves prior to use.
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