Sylgard 184 poly(dimethylsiloxane) (PDMS) prepolymer was purchased from Dow Corning (Midland, MI, USA). SU-8 3050 photoresist was purchased from Microchem (Newton, MA, USA). Absolute grade ethanol, tetraethyl orthosilicate (TEOS, 98%), 3-(trimethoxysilyl)propyl methacrylate (TPM, 98%), poly(vinyl alcohol) (PVA, 87–89%) and 2-hydroxy-2-methylpropiophenone (Darocur 1173) were purchased from Sigma-Aldrich (St. Louis, MO, USA). Ammonium hydroxide 25% solution in water (NH4OH) was obtained from Acros Organics (Morris Plains, NJ, USA). 1,10-Decanediol dimethacrylate (DDMA) was purchased from Polyscience (Warrington, PA, USA). Deionized water (>18 k ohm) was obtained using Milli-Q water. All raw materials were used without further purification.
3 trimethoxysilyl propyl methacrylate tpm
Manufactured by Merck Group
Sourced in United States
3-(trimethoxysilyl)propyl methacrylate (TPM) is a silane coupling agent used as a laboratory reagent. Its core function is to provide a chemical link between inorganic and organic materials.
Automatically generated - may contain errors
Lab products found in correlation
Tetraethyl orthosilicate teos, by Merck Group (2 mentions)
2 hydroxy 2 methylpropiophenone darocur 1173, by Merck Group (1 mentions)
Polyvinyl alcohol (pva), by Merck Group (1 mentions)
Su 8 3050 photoresist, by MicroChem (1 mentions)
Hydrochloric acid (hcl), by Thermo Fisher Scientific (1 mentions)
Ammonium hydroxide nh4oh, by Thermo Fisher Scientific (1 mentions)
2 2 0 azobis 2 methylpropionitrile aibn, by Merck Group (1 mentions)
Divinylbenzene dvb, by Merck Group (1 mentions)
4 styrenesulfonic acid sodium salt hydrate nass, by Merck Group (1 mentions)
Ethanol etoh, by Avantor (1 mentions)
4 tert butylcatechol, by Merck Group (1 mentions)
Dimethyl sulfoxide (dmso), by Merck Group (1 mentions)
Potassium persulfate, by Merck Group (1 mentions)
Styrene, by Merck Group (1 mentions)
Sorbitan monooleate span 80, by Merck Group (1 mentions)
Divinylbenzene, by Merck Group (1 mentions)
2 ethylhexyl acrylate eha, by Merck Group (1 mentions)
Ammonium persulfate ap, by Merck Group (1 mentions)
Ammonium hydroxide solution nh4oh, by Merck Group (1 mentions)
4 protocols using 3 trimethoxysilyl propyl methacrylate tpm
1
Fabrication of PDMS-Based Microfluidic Devices
2
Fluorescent Polymer Synthesis Protocol
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Materials 4-Styrenesulfonic acid sodium salt hydrate (NaSS, Sigma-Aldrich), 2,2 0 -azobis(2-methylpropionitrile) (AIBN, 98%, Sigma-Aldrich), methanol (MeOH, absolute HPLC, Biosolve Chimie), divinylbenzene (DVB, technical grade 80%, Sigma-Aldrich), methacryloxyethyl thiocarbamoyl rhodamine B (PolyFluor s 570, Polysciences), ammonium hydroxide (NH 4 OH, 28-30 wt% in water, Acros Organics), 3-(trimethoxysilyl)propyl methacrylate (TPM, Z97%, Sigma-Aldrich), dimethyl sulfoxide (DMSO, Sigma-Aldrich), gellan gum (gellan, powder, Alfa Aesar), ethanol (EtOH, absolute, VWR Chemicals), Norland optical adhesive 81 (UV glue, Norland), pyrromethene BODIPY TM 493/503 (BODIPY, Invitrogen TM ), potassium chloride (KCl, Z99%, Acros Organics), n-decane (Z99%, Carl Roth GmbH) and hydrochloric acid (HCl, 37% in water, Acros Organics) were used as received. Styrene (Z99%, containing 4-tert-butylcatechol as a stabilizer, Sigma-Aldrich) was purified through a column packed with silica gel (high purity grade: Davisil Grade 633, Sigma-Aldrich) and aluminum oxide powder (Z98%, Honeywell Fluka). The water used in all experiments was purified by filtration through Millipore filters (18.2 MO cm at 25 1C).
3
Synthesis of Polymeric Microparticles
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MTMS (Sigma), divinylbenzene (DVB), styrene, (Aldrich), (±)-2-ethylhexyl acrylate (EHA) (Aldrich), 3-(trimethoxysilyl)propyl methacrylate (TPM) (Sigma), sorbitanmono-oleate (Span80) (Aldrich), potassium persulfate, calcium chloride hexahydrate (Aldrich), methyl alcohol, oxalic acid, and aqueous ammonia were used without further purification.
4
Silica Nanoparticle Synthesis with Methacrylate
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We used the following materials as received: tetraethyl orthosilicate (TEOS, 98.0%, Sigma-Aldrich), an ammonium hydroxide solution (NH4OH, 28–30%, Sigma-Aldrich), 3-(trimethoxysilyl)propyl methacrylate (TPM, 98%, Sigma-Aldrich), 1,1-difluoroethylene VDF (Apollo Scientific), and ammonium persulfate (APS, >98.0%, Sigma-Aldrich).
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