GCMS was performed on a GCMS-QP2010 Ultra gas chromatography mass-spectrometer (Shimadzu) equipped with an HP-5MS column (the internal diameter was 0.25 μm and the length was 30 m). The parameters were as follows: helium A was as carrier gas, the temperature of an injector was 250 °C, the flow rate through the column was 2 ml min−1, the thermostat temperature program was a gradient temperature increase from 70 to 250 °C with a step of 10 °C min−1. The range of scanned masses was m/z 35 ÷ 400. The internal standard method using dodecane was used for the quantitative analysis of Mizoroki–Heck products.
Gcms qp2010 ultra gas chromatography
Manufactured by Shimadzu
Sourced in Japan
The GCMS-QP2010 Ultra is a gas chromatograph-mass spectrometer (GC-MS) system manufactured by Shimadzu. It is designed for high-performance analysis of complex samples. The system combines a gas chromatograph for separation of chemical compounds and a mass spectrometer for identification and quantification of those compounds.
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Lab products found in correlation
2 protocols using gcms qp2010 ultra gas chromatography
1
Quantitative GCMS Analysis of Mizoroki–Heck Products
2
GC-MS Analysis of Organic Compounds
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Gas chromatography–mass spectrometry was performed on a GCMS-QP2010 Ultra gas chromatography mass spectrometer (Shimadzu, Kyoto, Japan) equipped with an HP-5MS column (the internal diameter was 0.32 mm, and the length was 30 m). The parameters were as follows: Helium 99.995% purity was the carrier gas, the temperature of the injector was 250 °C, the flow rate through the column was 2 mL/min, and the thermostat temperature program was a gradient temperature increase from 70 to 250 °C with a step of 10 °C/min. The range of the scanned masses was m/z 35–400. The internal standard method using dodecane was used for the quantitative analysis.
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