Linalool

Manufactured by Thermo Fisher Scientific

Sourced in United States

Linalool is a naturally occurring terpene alcohol found in many plants. It is a colorless liquid with a characteristic floral odor. Linalool is commonly used as a fragrance and flavoring agent in various industries.

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Lab products found in correlation

10 protocols using linalool

Semiconducting SWNT Solution Preparation

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Ninety-five percent semiconducting SWNT solution with a concentration of 0.01 mg/mL was purchased from Nano-Integris Inc. (Skokie, IL, USA). Acetone, propanol, and ammonium hydroxide were acquired from Fisher Scientific Company (Pittsburgh, PA, USA). 3-Aminopropyltriethoxysilane (APTES), 2-ethyl-1-hexanol, 1-tetradence, and phenylacetaldehyde were purchased from Sigma-Aldrich (Saint Louis, MO, USA). Linalool (97%) was obtained from Acros Organics. Milli-Q water was used throughout the experiments. The ssDNA were bought from Integrated DNA Technologies, Inc. (Coralville, IA, USA):

s1-DNA: 5′-CTT CTG TCT TGA TGT TTG TCA AAC-3′ and

s2-DNA: 5′-AAA ACC CCC GGG GTT TTT TTT TTT-3′.

They were prepared with Milli-Q water and stored at −4 °C before use.

Wang H., Ramnani P., Pham T., Villarreal C.C., Yu X., Liu G, & Mulchandani A. (2019). Gas Biosensor Arrays Based on Single-Stranded DNA-Functionalized Single-Walled Carbon Nanotubes for the Detection of Volatile Organic Compound Biomarkers Released by Huanglongbing Disease-Infected Citrus Trees. Sensors (Basel, Switzerland), 19(21), 4795.

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Detailed Reagents and Media Protocols

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In our studies we used geraniol (99%, Acros organics, Poznań, Poland), citral (95%, Sigma Aldrich, Poznań, Poland), beta-pinene (95%, Fluka, Poznań, Poland), nerol (97%, Acros organics, Poznań, Poland), ocimenes (90%, Sigma Aldrich), linalool (97%, Acros organics, Poznań, Poland), and farnesol (96% Acros organics, Poznań, Poland).
The nourishing base CALAYA (Cosibella, Leeds, UK), used for preparing natural cosmetics, contained aqua, Helianthus annuus (Sunflower) seed oil, Polysorbate 20, cetyl alcohol, glyceryl stearate, phenoxyethanol, carbomer, potassium sorbate, and sodium hydroxide.
Microbiological media used in experiments (Graso Biotech, Jabłowo, Poland) were as follows: Mueller–Hinton agar II, Columbia agar with 5% sheep blood, plate count agar, chocolate Agar, mannitol salt agar, BHI broth, and D/E neutralizing broth. Other reagents used in experiments included 0.9% sodium chloride solution (Polpharma, Starogard Gdański, Poland) and 70% ethanol (Chempur, Poznań, Poland).

Fajdek-Bieda A., Pawlińska J., Wróblewska A, & Łuś A. (2024). Evaluation of the Antimicrobial Activity of Geraniol and Selected Geraniol Transformation Products against Gram-Positive Bacteria. Molecules, 29(5), 950.

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Catalytic Synthesis of Terpene Compounds

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The syntheses were performed in the presence of diatomite (100% pure, Nanga, Hobbs, New Mexico) and aluminum potassium alum (100% pure, Nanga, Ufa, Russia) as the catalysts. The organic raw material used in our tests was GA (99% pure, from Acros Organics, Milwaukee, USA). For quantitative analysis which were performed by the gas chromatography method (GC), standards in the form of: citronellol (95% pure, from Sigma Aldrich, Steinheim, Germany), citral (95% pure, Sigma Aldrich, Steinheim, Germany), ocimen (90% pure, from Sigma Aldrich, Milwaukee, WI, USA), beta-pinene (95% pure, from Fluka, Milwaukee, WI, USA), linalool (97% pure, from Acros, Steinheim, Germany), farnesol (96% pure, from Acros, Steinheim, Germany), nerol (97% pure, from Acros, Steinheim, Germany), myrcene (pure technical from Sigma Aldrich, Steinheim, Germany) and geranylgeraniol (85% pure, from Sigma Aldrich, Milwaukee, WI, USA) were used.

Fajdek-Bieda A., Wróblewska A., Miądlicki P, & Konstanciak A. (2022). Conversion of Geraniol into Useful Value-Added Products in the Presence of Catalysts of Natural Origin: Diatomite and Alum. Materials, 15(7), 2449.

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Aniseed Oil and Thymol Solubilization in Phosphate Buffer

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D-Glucose, L-Lysine monohydrochloride and linalool were purchased from Acros Organics, thymol from Applichem and anise oil from Sigma Aldrich (CAS: 8007-70-3, nature identical, synonym: aniseed oil). All solutions (glucose, lysine and the test compounds) were prepared in phosphate buffer 0.1 M, pH 7.2 ± 0.1 (PBS, Bectron, Dickinson and Company, Bergen County, NJ, USA) and Tween 80 (Serva Electrophoresis GmbH, Heidelberg, Germany) which helps to incorporate aniseed oil and thymol in phosphate buffer. As linalool possesses a very good aqueous solubility at pH 7.0, the use of Tween 80 was not necessary [26] (link).
2-Mercaptoethanol (MCE ≥ 99.0%), phthaldialdehyde (OPA ≥ 99.0%) and hydrochloric acid solution (0.1 N) were purchased from Sigma Aldrich (Steinheim, Germany). Sodium hydroxide (≥98%) and boric acid (≥99.5%) were purchased from Honeywell International Inc (Muskegon, MI, USA). Di-potassium hydrogen phosphate, potassium dihydrogen phosphate and sodium acetate trihydrate were purchased from MERCK (Darmstadt, Germany). Water, methanol and acetonitrile (HPLC grade) were purchased from Fisher Scientific (Loughborough, UK).

Vlassopoulos A., Mikrou T., Papantoni A., Papadopoulos G.K., Kapsokefalou M., Mallouchos A., & Gardeli C. (2022). The Effect of Terpenoid Compounds on the Formation of Advanced Glycation Endproducts (AGEs) in Model Systems. Applied Sciences, 12(2), 908-908.

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Pharmaceutical Formulation Development

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Quetiapine Fumarate was obtained as a gift sample from Octopus Pharmaceuticals, Chennai, India. HPMC K 100 was obtained from Hi-media laboratories, Mumbai, India. Poly Vinyl Pyrrolidone K 30 was procured from BASF limited, Rosenberg, Germany. Linalool and 1,8-Cineole were procured from Alfa Aesar, Lancaster, UK. DMSO and Glycerin have been purchased from Merck Limited, Vikroli East, Maharashtra, Mumbai. All other chemicals were of analytical grade.

Bhupathyraaj M., Vijaya Rani K.R., Sridhar S.B., Shareef J., Thomas S., Halligudi N., Sockalingam A., Mohandoss K, & Sundar S. (2022). Effect of Polymers and Permeation Enhancers in the Release of Quetiapine Fumarate Transdermal Patch through the Dialysis Membrane. Polymers, 14(10), 1984.

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Preparation of cannabinoid and terpene solutions

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WIN55,212-2 (Tocris, #1038), α-Humulene (Sigma Aldrich, #53675), β-Pinene (Alfa Aesar, #A17818), Linalool (Alfa Aesar, #A14424), Geraniol (Alfa Aesar, #13736), and β-Caryophyllene (Cayman, #21572) were all prepared as stock solutions in DMSO. Working solutions were then diluted in 10% DMSO, 10% Tween-80, and 80% USP saline for injections. Rimonabant (Tocris, #0923) was made up in DMSO and then diluted to 20% DMSO, 10% Tween-80, and 70% USP saline for injections. Istradefyllene (Tocris, #5147) was made up in DMSO and then diluted to 20% DMSO, 10% Tween-80 and 70% saline for injections. Morphine sulfate pentahydrate (from the NIDA Drug Supply Program) was dissolved in USP saline. Vehicle injections were matched accordingly as a control in each experiment. All solutions were made immediately before use without long-term storage. For in vitro experiments, 100 mM stocks of terpenes, and 10 mM stocks of all other compounds, were made up in DMSO. DMSO concentrations in assays were maintained at 1% or lower. Vehicle controls were matched accordingly.

LaVigne J.E., Hecksel R., Keresztes A, & Streicher J.M. (2021). Cannabis sativa terpenes are cannabimimetic and selectively enhance cannabinoid activity. Scientific Reports, 11, 8232.

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Extraction and Quantification of Volatile Compounds

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Milli-Q water, ethanol (purity: ≥ 99.8%) and zinc sulfate (purity: 99.9%) were purchased from VWR International (Darmstadt, HE, Germany). The solvents dichloromethane (purity: 99.99%) and methanol (purity: ≥ 99.9%) were acquired from Fisher Scientific UK Limited (Loughborough, Leicestershire, UK) and Honeywell (Seelze, NI, Germany). Di-sodium hydrogen phosphate (purity: ≥ 99%) and sodium dihydrogen phosphate monohydrate (purity: ≥ 99%) were obtained from Sigma-Aldrich Chemie GmbH (Taufkirchen, BY, Germany). Potassium ferrocyanide trihydrate (purity: ≥ 99%) was acquired from Acros Organics (Geel, Antwerp Province, Belgium). Citric acid monohydrate (purity: ≥ 99.5%) and geraniol (purity: ≥ 90%) were purchased from Carl Roth GmbH & Co. KG (Karlsruhe, BW, Germany) and the enzyme preparation (β-glucosidase, polygalacturonase) from Oenobrands SAS (Montpellier, Occitanie, France). The compounds citronellol (purity: ≥ 95%), nerol (purity: 98.7%), carvacrol (purity: 99.4%), thymol (purity: > 99.9%), menthol (purity: 99.3%), dihydrocitronellol (purity: 98.3%) and a C 7 -C 30 saturated alkane standard solution (certified reference material) were obtained from Sigma-Aldrich (Steinheim, BW, Germany). nerolidol (cis + trans, purity: 97.5%), farnesol (mixture of isomers, purity: 98.0%), α-terpineol (purity: 96%) and linalool (purity: 98.5%) were purchased from Alfa Aesar (Ward Hill, MA, USA).

Könen P.P., Stötzel I., Schwab W, & Wüst M. (2021). Qualitative profiling of mono- and sesquiterpenols in aglycon libraries from Vitis vinifera L. Gewürztraminer using multidimensional gas chromatography–mass spectrometry. Eur Food Res Technol., 247(5).

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Extraction and Quantification of Volatile Compounds

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Könen P.P., Stötzel I., Schwab W., & Wüst M. (2021). Qualitative profiling of mono- and sesquiterpenols in aglycon libraries from Vitis vinifera L. Gewürztraminer using multidimensional gas chromatography–mass spectrometry. European Food Research and Technology, 247(5), 1117-1124.

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Linalool, 1,8-cineole, and Nerolidol Extraction

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Linalool, 1,8-cineole, and cis/trans-nerolidol were purchased from Thermo Fisher Scientific (Thermo Fisher, Waltham, MA, USA).

Chou M.Y., Andersen T.B., Mechan Llontop M.E., Beculheimer N., Sow A., Moreno N., Shade A., Hamberger B, & Bonito G. (2023). Terpenes modulate bacterial and fungal growth and sorghum rhizobiome communities. Microbiology Spectrum, 11(5), e01332-23.

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Curcumin-Based Nanoformulation Development

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Curcumin (Cur) 97%, oleic acid 90%, stearic acid 97%, polysorbate 20 (tween 20), sodium taurocholate 96%, sodium glycocholate 97.5%, hydrogen peroxide 29%, and deionized water were procured from Alfa Aesar (Thermo Fisher Scientific, Dreieich, Germany), whereas linalool and geraniol were procured from Acros Organics (Thermo Fisher Scientific, Dreieich, Germany). Skweez (contains Imidacloprid 34%) insecticide was purchased locally from Semadak (Damanhur, El Beheira governorate Egypt). All chemical reagents were utilized without being purified, with the exception of Skweez insecticide, which was lyophilized to produce a powder.

Radwan I.T., Ghazawy N.A., Alkhaibari A.M., Gattan H.S., Alruhaili M.H., Selim A., Salem M.E., AbdelFattah E.A, & Hamama H.M. (2024). Nanostructure Lipid Carrier of Curcumin Co-Delivered with Linalool and Geraniol Monoterpenes as Acetylcholinesterase Inhibitor of Culex pipiens. Molecules, 29(1), 271.

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