The following chemicals were used as received: sodium borohydride (99.99%), acrylic acid (99%), PAA powder (MW = 2000) and palladium (II) acetate (98%), naphthalene_d8 (99 atom % D) were purchased from Sigma-Aldrich. Sodium hydroxide (1 M), sulfuric acid (0.5 M), hexanes and ferrous chloride tetrahydrate were obtained from Fisher Scientific. PVDF powder was purchased from Polysciences, Inc. Ammonium persulfate (98%), and N,N’-methylenebisacrylamide (NNMA, 99%) were received from Acros Organics. 3,3',4,4',5-pentachlorobiphenyl (> 97%, neat), biphenyl (> 97%, neat) and their analytical solution (100 ppm in hexane) were obtained from Ultra Scientific. Ethanol (200 proof) was bought from EMD Millipore Corporation. Sodium chloride was purchased from BDH. Full scale PVDF 700 microfiltration membranes were obtained from Nanostone Water, Inc. Deoxygenated water was obtained by purging N2 into deionized ultra-filtered (DIUF) water for 30 minutes.
Naphthalene d8
Manufactured by Merck Group
Sourced in United States, Australia
Naphthalene-d8 is a deuterated form of naphthalene, a polycyclic aromatic hydrocarbon. It is commonly used as a chemical standard and internal reference in analytical techniques such as mass spectrometry and nuclear magnetic resonance spectroscopy.
Automatically generated - may contain errors
Lab products found in correlation
Ferrous chloride tetrahydrate, by Thermo Fisher Scientific (2 mentions)
Phenanthrene d10, by Merck Group (2 mentions)
Acenaphthene d10, by Merck Group (2 mentions)
Chrysene d12, by Merck Group (2 mentions)
Perylene d12, by Merck Group (2 mentions)
Naphthalene, by Merck Group (2 mentions)
Ammonium persulfate, by Thermo Fisher Scientific (1 mentions)
Sodium chloride (nacl), by BD (1 mentions)
Pvdf powder, by Polysciences (1 mentions)
N n methylenebisacrylamide, by Thermo Fisher Scientific (1 mentions)
Palladium 2 acetate, by Merck Group (1 mentions)
Sodium borohydride, by Merck Group (1 mentions)
Acrylic acid, by Merck Group (1 mentions)
Sulfuric acid, by Thermo Fisher Scientific (1 mentions)
Hydrochloric acid (hcl), by Thermo Fisher Scientific (1 mentions)
Sodium borohydride, by Thermo Fisher Scientific (1 mentions)
Sodium chloride (nacl), by Thermo Fisher Scientific (1 mentions)
Hexane, by Thermo Fisher Scientific (1 mentions)
Potassium tetrachloropalladate 2, by Strem Chemicals (1 mentions)
Sodium hydroxide (naoh), by Thermo Fisher Scientific (1 mentions)
7 protocols using naphthalene d8
1
Synthesis and Characterization of PVDF Membranes
2
Membrane Functionalization for Environmental Applications
3
Polycyclic Aromatic Hydrocarbons Analysis
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Standards of PAHs (> 99.0%), acenaphthene-d10 (> 99.0%), phenanthrene-d10 (> 99.0%), chrysene-d12 (> 99.0%), perylene-d12 (> 99.0%), and naphthalene-d8 (> 99.0%) were purchased from Sigma-Aldrich (Shanghai, China). The physical and chemical properties of PAHs are shown in Table S1.
The stock solutions of all the standards were prepared in n-hexane and stored in amber glass vials. All the organic solvents used were of HPLC grade (JT Baker, Shanghai, China). Deionized water was prepared using a Milli-Q plus water purification system (Millipore Corp, Shanghai, China) . Anhydrous sodium sulfate (Na2SO4), silica gel (60-100 mesh), florisil (60-100 mesh), and alumina oxide (100-200 mesh) for clean the samples were baked at 400 °C for 4 h before use to eliminate potential environmental pollution.
The stock solutions of all the standards were prepared in n-hexane and stored in amber glass vials. All the organic solvents used were of HPLC grade (JT Baker, Shanghai, China). Deionized water was prepared using a Milli-Q plus water purification system (Millipore Corp, Shanghai, China) . Anhydrous sodium sulfate (Na2SO4), silica gel (60-100 mesh), florisil (60-100 mesh), and alumina oxide (100-200 mesh) for clean the samples were baked at 400 °C for 4 h before use to eliminate potential environmental pollution.
4
Naphthalene Deodorant Extraction Protocol
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
PUF disks were purchased from Sibata Scientific Technology LTD (Saitama, Japan). n-Hexane (HPLC solvent grade) was purchased from Daejung Chemical & Metals Co. (Siheung, Korea). Naphthalene (≥99%) and Naphthalene-d8 (≥98%) were purchased from Sigma-Aldrich (St Louis, MO, USA). Ball-shaped Naphthalene deodorants were purchased from a local market in Seoul, Korea.
5
GC-MS Analysis of Volatile Compounds
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Analytical-grade chemicals and reagents for preparing standard solutions for GC-MS analysis were used without further purification. Standard 1-octen-3-one (96%), 1-octen-3-ol (≥98%), 3-octanone (≥98%), benzaldehyde (≥99.5%), trans-2-hexen-1-ol (96%), benzyl alcohol (99%+), 1,5-dimethyl naphthalene (98%), 3-methyl-1-butanol (99%+), 1,5-dimethyltetralin (≥90%), phenylethyl alcohol (≥99%), 4-methyl-2-pentanol (98%), glucose (≥99.5%), fructose (≥99%), tartaric acid (99%), naphthalene-d8 (99 atom% D, ≥98% (CP)), 3-octanol (99%), 2-octanol (≥99.5%), zinc nitrate hexahydrate (98%), 2-methylimidazole (98%), and glass wool were purchased from Sigma-Aldrich (Sydney, NSW, Australia). Hexanal (98%), 1-hexanol (99%), menthol (HPLC), and N,N-dimethylformamide (DMF) (99%) were purchased from Alfa Aesar (Scoresby, VIC, Australia). Hexanal-d12 (98.5 atom % D) and 2,4,6-tribromoanisol-d5 (99 atom % D) were purchased from CDN Isotopes (Pointe-Claire, Quebec, Canada). Milli-Q™ water (18 MΩ·cm) was collected through a Millipore™ water purification system (Merk, Bayswater, VIC, Australia). Synthetical grape juice was made using 100 g glucose, 100 g fructose, and 4 g tartaric acid. All solutions were prepared in Milli-Q™ water, with the pH adjusted to 7.0.
6
Polycyclic Aromatic Hydrocarbons Analysis in Gochujang
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Gochujang (Sunchang Gochujang; Chungjungone, Seoul, Korea) used in this study was
composed of brown rice (20.4%), red pepper powder (3%), and red
pepper seasoning (red pepper powder [8.3%], sea salt, garlic, and onion)
with soybeans, alcohol, yeast powder, starch syrup, brown glutinous rice flour,
sea salt, and isomaltooligosaccharide. Folin-Ciocalteu phenol reagent was
purchased from Sigma-Aldrich (St. Louis, MO, USA). All solvents and chemicals
used for PAH analysis were high-performance liquid chromatography grade. PAH
standards (naphthalene, acenaphthylene, acenaphthene, fluorene, phenanthrene,
anthracene, fluoranthene, pyrene, benzo[a]anthracene, chrysene,
benzo[b]fluoranthene, benzo[k]fluoranthene, benzo[a]pyrene,
indeno[1,2,3-cd]pyrene, dibenzo[a,h]anthracene, and benzo[g,h,i]perylene) and
internal standard (ISTD) solution mix (naphthalene-d8,
acenaphthene-d10, phenanthrene-d10,
chrysene-d12, and perylene-d12) were purchased from
Sigma-Aldrich. All the other chemicals were of analytical grade.
composed of brown rice (20.4%), red pepper powder (3%), and red
pepper seasoning (red pepper powder [8.3%], sea salt, garlic, and onion)
with soybeans, alcohol, yeast powder, starch syrup, brown glutinous rice flour,
sea salt, and isomaltooligosaccharide. Folin-Ciocalteu phenol reagent was
purchased from Sigma-Aldrich (St. Louis, MO, USA). All solvents and chemicals
used for PAH analysis were high-performance liquid chromatography grade. PAH
standards (naphthalene, acenaphthylene, acenaphthene, fluorene, phenanthrene,
anthracene, fluoranthene, pyrene, benzo[a]anthracene, chrysene,
benzo[b]fluoranthene, benzo[k]fluoranthene, benzo[a]pyrene,
indeno[1,2,3-cd]pyrene, dibenzo[a,h]anthracene, and benzo[g,h,i]perylene) and
internal standard (ISTD) solution mix (naphthalene-d8,
acenaphthene-d10, phenanthrene-d10,
chrysene-d12, and perylene-d12) were purchased from
Sigma-Aldrich. All the other chemicals were of analytical grade.
7
Analysis of PAH Congeners in Samples
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
PAH congeners were selected based on the priority pollutant addressed by the US EPA. A total of 16 PAHs compounds was taken for the analysis of collected samples; those compounds are Naphthalene (Nap), Acenaphthene (Ace), Acenaphthylene (Acy), Anthracene (Ant), Fluorene (Fl), Phenanthrene (Phe), Fluoranthene (Fla), Pyrene (Pyr), Benzo [a] anthracene (BaA), Chrysene (Chr), Benzo [b]fluoranthene (BbF), Benzo [a]pyrene (BaP), Benzo [k]fluoranthene (BkF), Dibenzo [a,h]anthracene (DahA), Indeno [1,2,3-cd]pyrene (IcdP), Benzo [ghi]perylene (BghiP). The standard mixture of 16 PAHs was bought from Supelco (EPA 610 Polynuclear Aromatic Hydrocarbons mix 2000 μg/mL) (Kuri and Co., Dhaka, Bangladesh). The naphthalene D8 was used as an internal standard purchased from Sigma Aldrich) (Kuri and Co., Dhaka, Bangladesh). Anhydrous sodium sulfate was bought from Sigma Aldrich) (Kuri and Co., Dhaka, Bangladesh). All solvents and reagents were obtained from Applichem (Germany) with high-performance liquid chromatography (HPLC) grade.
About PubCompare
Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.
We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.
However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.
Ready to get started?
Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required
Revolutionizing how scientists
search and build protocols!