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Thioacetamide

Manufactured by Sinopharm
Sourced in China

Thioacetamide is a chemical compound commonly used in research and industrial applications. It is a white crystalline solid that is soluble in water and various organic solvents. Thioacetamide's core function is as a reagent and precursor in chemical synthesis. It has applications in the fields of analytical chemistry and materials science, but its specific uses should be determined by the intended application and handling should follow appropriate safety protocols.

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17 protocols using thioacetamide

1

Graphene Oxide-Nafion Nanocomposite Synthesis

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Graphene oxide nanosheets (Nanjing XFNANO Materials Tech), Nafion (Sigma-Aldrich), Cobalt acetate, hexamethylenetetramine (C6H12N4), thioacetamide (TAA) and all others reagents were purchased from Sinopharm.
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2

Synthesis of Ti3AlC2 Powder

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Ti3AlC2 powder was purchased from 11 Technology. Hydrochloric acid (HCl), sodium tetrafluoroborate (NaBF4), hydrofluoric acid (HF, 40 wt%), tungsten chloride (WCl6), thioacetamide (TAA), and dimethylformamide (DMF) were provided by Sinopharm.
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3

Rare-Earth Oxide Nanocrystal Synthesis

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Rare earth oxide (Y2O3, Yb2O3, Tm2O3, 99.99 wt%) were all purchased from Shang Macklin Biochemical Co. Ltd., China. Sodium hydroxide (NaOH, 98 wt%), ammonium fluoride (NH4F, 98 wt%), oleic acid (OA, 90%), trisodium citrate dihydrate (C6H5Na3O7·2H2O, 98 wt%), ammonia aqueous solution (NH3·H2O, 25–28% wt%), cadmium chloride (CdCl2, 99 wt%), and ethanol (99.7 wt%) were purchased from Aladdin Industrial Corporation, China. Hydrochloric acid (HCl, 36–38 wt%) was supplied by Wu Xi City Yasheng Chemical Co. Ltd., China. Thioacetamide (TAA, 99.0 wt%) was purchased from Sinopharm Chemical Reagent Co. Ltd., China. All raw materials were used as starting materials without further purification.
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4

Hydrothermal Synthesis of BTIS Heterojunction

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BTIS was synthesized using a hydrothermal method as follows. 1 mmol of In(NO3)3·xH2O (99.99%, Aladdin Industrial Corporation) and 2.4 mmol of thioacetamide (99.0%, Sinopharm Chemical Reagent Co, Ltd) were dissolved in 80 mL of deionized water with magnetically stirring for 15 min. Then, 0.065 g of commercial BaTiO3 (99.5%, Aladdin Industrial Corporation) was added and continued stirring for 10 min, followed by ultrasonicating for 2 min. Then the mixture was poured into a 100 ml Teflon lined stainless-steel autoclave and maintained at 180 °C for 12 h. Finally, the as-obtained precipitates was washed with distilled water and ethanol alternately and subsequently dried in an oven at 80 °C for 12 h. The as-prepared powder is denoted by BTIS.
In order to elucidate the effect of the core–shell structured heterojunction BT/IS on the photocatalytic properties, pure IS was prepared using the identical procedure but without BT added. Simultaneously, the above-said commercial BT was characterized by using identical techniques with BTIS and IS as comparison.
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5

Synthesis and Characterization of Metal Nanoparticles

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Tetrachloroauric acid tetrahydrate (HAuCl4·4H2O), sodium citrate tribasic dihydrate (TSC, 99.0%), silver nitrate (AgNO3, 99.0%), hydrochloric acid (HCl, 36.0−38.0 wt%), L-ascorbic acid (AA, 99.0%), ammonia solution (NH3H2O, 25.0−28.0 wt%), hydrogen peroxide (H2O2, 30.0 wt%), hexamethylenetetramine (HMT, 99.5%), thioacetamide (TAA, 99%), and cadmium acetate (CH3COO)3Cd were purchased from Sinopharm Chemical Reagent Co. Ltd. (Shanghai, China). Sodium borohydride (NaBH4, 99%), hexadecyltrimethylammonium chloride (CTAC, 97%), hexadecyltrimethylammonium bromide (CTAB, 99.0%), sodium iodide (NaI, 99.5%), and potassium chloroplatinite (K2PtCl6, 99.5%) were purchased from Aladdin Reagent. The chemicals were not further purified and were used straight from the original packaging. Deionized (DI) water with a resistivity of 16.8 Ω·cm was used throughout the experiments.
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6

Colloidal Nanoparticle Synthesis

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Bismuth neodecanote, oleic acid (90 %), cadmium oxide (99.99 %), bis(trimethylsilyl) sulfide ((TMS)2S), hexadecylamine (90 %), tri-n-octylphosphine oxide (90 %), and trioctylphosphine (97 %) were purchased from Aldrich. Oleyl amine (90 %) was purchased from Aladdin. Thioacetamide and selenium powder were purchased from Sinopharm. 1,2-Dipalmitoyl-sn-glycero-3-phosphoethanol-amine-N-[methoxy(polyethylene glycol)-2000] (PEG-DSPE, 99 %) was purchased from Avanti. All chemicals were used as received, unless otherwise stated.
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7

Synthesis of Copper Nanoparticles Using Stannic Chloride

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Copper acetate hydrate (CuAc2·H2O), stannic chloride pentahydrate (SnCl4·5H2O), hydrogen peroxide (H2O2, 30 wt%), thioacetamide (TAA), and N,N-dimethylformamide (DMF) were obtained from Sinopharm Chemical Reagent Co., Ltd. Sodium azide (NaN3), t-butanol (t-BuOH), benzoquinone, and methylene blue (MB) were purchased from Aladdin Chemical Reagent Co., Ltd. 5,5-dimethyl-1-pyrroline N-oxide (DMPO) and 2,2,6,6-tetramethylpiperidine-1-oxyl (TEMPO) were bought from Adamas Reagent, Ltd. All reagents were purchased as received and used without any further purification.
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8

Synthesis of Zinc-Indium Sulfide Nanomaterials

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Zinc chloride (ZnCl2), indium chloride tetrahydrate (InCl3·4H2O), thioacetamide (TAA), cetyltrimethylammonium bromide (CTAB), palladium chloride (PdCl2), methanol, and ethanol were purchased from Sinopharm Chemical Reagent Co. Ltd.(Shanghai, China). and Macklin Reagent Co. Ltd. (Shanghai, China).
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9

Synthesis of Functionalized Nanoparticles

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All chemicals were analytical grade and used without further purification. Hexadecyltrimethylammonium bromide (C19H42NBr, CTAB), silver nitrate (AgNO3), sodium borohydride (NaBH4), l-ascorbic acid (C6H8O6, AA), hydrochloric acid (HCl, 37 wt%) and benzotrifluoride (C7H5F3, BTF) were purchased from Sigma Aldrich. Benzyl alcohol (C7H8O, BA), benzaldehyde (C7H6O, BAD) and sodium oleate (C18H33O2Na, NaOL) were purchased from Aladdin. 4-Methylbenzyl alcohol (C8H10O), 4-methoxybenzyl alcohol (C8H10O2), 4-chlorobenzyl alcohol (C7H7ClO), and 4-hydroxybenzyl alcohol (C7H8O2) were supplied by Alfa Aesar. Cadmium acetate (C4H6O4Cd, Cd(Ac)2), thioacetamide (C2H5SN, TAA), chloroauric acid tetrahydrate (HAuCl4·4H2O), glycine acid (C2H5NO2, Gly), anhydrous ethanol (C2H5OH, EtOH) and chloroplatinic acid hexahydrate (H2PtCl6·6H2O) were obtained from Sinopharm Chemical Reagent Co., Ltd (Shanghai, China). Deionized water used in the synthesis was obtained from local sources.
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10

Synthesis of Nanoparticles Using Chemical Reagents

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Chloroauric acid (99.99%), sodium hydroxide (99.7%), L-ascorbic acid (AA, 99.7%), sodium borohydride (96.0%), lead acetate (99.5%), thioacetamide (TAA, 99.0%), hexamethylenetetramine (HMT, 99.0%), hexadecyltrimethylammonium bromide (CTAB, 99.0%), and hydrochloric acid (36–38%) were purchased from Sinopharm Chemical Reagent Co. Ltd. (Shanghai, China). Deionized water with a resistivity of about 18.25 MΩ·cm was used as the solvent in all experiments.
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