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Dsc 204 f1 phoenix device

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The DSC-204-F1 Phoenix is a differential scanning calorimetry (DSC) device manufactured by Netzsch. It is designed to measure the heat flow and temperature difference between a sample and a reference material as a function of time or temperature. The device allows for precise analysis of thermal properties of materials, such as phase transitions, heat capacity, and thermal stability.

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DSC 204 F1 Phoenix DSC 204 F1 device 204 F1 Phoenix DSC 204 F1 DSC 204 Phoenix DSC 204

2 protocols using dsc 204 f1 phoenix device

1

Thermal Analysis of Material LCST

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A Netzsch instrument DSC-204-F1 Phoenix device was used to perform the experiments of DSC. All the measurements were made under a high purity N2 atmosphere. Scanning was carried out from −30 °C to 50 °C using liquid N2 to cool the system. A heating rate of 3 °C min−1 was chosen. The experimental error in this assay was ±150 J g−1 and ±2 °C. Lower critical solution temperatures (LCST) were determined after DSC curves analysis.
Abel S.B., Rivarola C.R., Barbero C.A, & Molina M. (2020). Electromagnetic radiation driving of volume changes in nanocomposites made of a thermosensitive hydrogel polymerized around conducting polymer nanoparticles. RSC Advances, 10(15), 9155-9164.
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2

DSC Thermal Analysis of Samples

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On a NETZSCH DSC 204 F1 Phoenix device, differential scanning calorimetry (DSC) investigations were carried out. 10 mg samples were heated twice, once at −50 ± 250 °C for the first heat and once at −50 ÷ 350 °C for the second heat, using nitrogen flow at a rate of 10 °C/min. Tg was calculated using the second heating.
Mârșolea (Cristea) A.C., Mocanu A., Stănescu P.O., Brincoveanu O., Orbeci C., Irodia R., Pîrvu C., Dinescu A., Bobirica C, & Rusen E. (2023). Synthesis and characterization of polyurethane flexible foams provided from PET derivatives, fly ash, and glass wastes. Heliyon, 9(12), e23097.
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