Tert butylbenzene

Manufactured by Merck Group

Sourced in United States

tert-butylbenzene is an aromatic hydrocarbon compound with the chemical formula C6H5C(CH3)3. It is a clear, colorless liquid with a characteristic odor. tert-butylbenzene is commonly used as a chemical intermediate in the production of various organic compounds.

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Lab products found in correlation

5 protocols using tert butylbenzene

Activated Charcoal-Based EPR Spectroscopy

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Analytical grade chemicals nitrone spin trap phenyl-N-tert-butylnitrone (PBN), tert-butylbenzene, (2,2,6,6-tetramethyl-piperidin-1-yl)oxyl (TEMPO), and 1-λ1-oxidanyl-2,2,6,6-tetramethyl-piperidin-4-ol (TEMPOL) were obtained from Sigma-Aldrich (St. Louis, MO, U.S.). Different types of activated charcoal (A = anasorb 747, B = CSC, and C = JXC (SKC Inc., Eighty Four, PA, U.S., material characteristics provided in Supporting Information Table S1)), Suprasil EPR tubes (4 mm o.d.; Wilmad-Labglass,Vineland, NJ, U.S.), Schlenk line (Chemglass Life Sciences, Vineland, NJ, U.S.), 500–750 μm glass beads (Fisher Scientific, PA, U.S.), and Cambridge filters pads (CFP, Performance Systematix Inc., Grand Rapids, MI, U.S.) were used as supplied. Cigarette holders (Hleeduo ZB-033) were purchased online from Amazon.

Goel R., Bitzer Z.T., Reilly S.M., Bhangu G., Trushin N., Elias R.J., Foulds J., Muscat J, & Richie JP J.r. (2018). Effect of Charcoal in Cigarette Filters on Free Radicals in Mainstream Smoke. Chemical research in toxicology, 31(8), 745-751.

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Cigarette Characterization and Analysis

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The 3R4F research cigarette was obtained from the University of Kentucky (Lexington, Kentucky, USA). All the commercial cigarettes were purchased locally (Hershey, PA): 26 King size (85 mm) and Virginia Slims Gold (100 mm). The cigarette brand varieties were selected based on their market share or unique characteristics. Marlboro, Newport, Pall Mall and Camel were selected for their popularity, with variants of these brands comprising an estimated total US market share of 66%.³¹ Parliament and American Spirit exemplify the types of unique characteristics such as recessed filters and “additive free” formulation, respectively. The cigarettes were stored in their original packaging long term at −20°C in airtight plastic bags. Analytical grade chemicals: nitrone spin trap phenyl-N-tert-butylnitrone (PBN), tert-butylbenzene, 2,2,6,6-tetramethyl-1-piperidinyloxy (TEMPO), 4-hydroxy-2,2,6,6-tetramethylpiperidine 1-oxyl (TEMPOL), heptadecane from Sigma-Aldrich (St. Louis, MO, USA), Suprasil® EPR tubes (4mm o.d;Wilmad-Labglass,Vineland, NJ, USA), Schlenk line (Chemglass Life Sciences,Vineland, NJ, USA) and Cambridge filters pads (Performance Systematix Inc.,Grand Rapids, MI, USA) were used as supplied.

Goel R., Bitzer Z., Reilly S.M., Trushin N., Foulds J., Muscat J., Liao J., Elias R.J, & Richie JP J.r. (2017). Variation in Free Radical Yields from U.S. Marketed Cigarettes. Chemical research in toxicology, 30(4), 1038-1045.

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Polymer Fractionation and Crude Oil Analysis

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Commercially available Torlon® 4000T-LV and Matrimid®5218 were purchased from Solvay Advanced Polymers (Alpharetta, GA) and Huntsman, respectively. SBAD-1, DUCKY-9, and DUCKY-10 polymers were synthesized from literature procedures detailed in two previous publications^{4 ,5 (link)}. Two real crude oils (Permian and Arabian light crude oils) were provided from ExxonMobil Technology and Engineering Company. The experimental results of the two fractionations were published previously^{4 ,5 (link)}. All other chemicals (p-xylylene diamine, lithium nitrate, chloroform, tetrahydrofuran, 1-methylpyrroldone, ethanol, methanol, hexane, toluene, toluene, Tert-butyl benzene, 1,3,5-triiso propyl benzene, n-Octane, iso-Octane, iso-cetane, methylcyclohexane, decalin, 1-methylnaphthalene, o-xylene, propyl benzene, mesitylene, n-butylcyclohexane, tetralin, bi-phenyl, dodecylbenzene, 1,3,5-triphenylbenzene, 1,3,5-Tris[(3-methylphenyl) phenylamino]benzene), methanol, and guaiacol were purchased from Sigma Aldrich, Alfa Aesar, or TCI and used as received.

Lee Y.J., Chen L., Nistane J., Jang H.Y., Weber D.J., Scott J.K., Rangnekar N.D., Marshall B.D., Li W., Johnson J.R., Bruno N.C., Finn M.G., Ramprasad R, & Lively R.P. (2023). Data-driven predictions of complex organic mixture permeation in polymer membranes. Nature Communications, 14, 4931.

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Preparation and Characterization of Mix-MA Monomer Benchmark

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The blend “Mix-MA”, used as
a benchmark monomer, has been prepared with 33.3 wt % of (hydroxypropyl)methacrylate,
33.3 wt % of 1,4-butanediol dimethacrylate, and 33.3 wt % of a urethane
dimethacrylate monomer, obtained from Sigma Aldrich and represented
in Scheme 2. Mix-MA
was already used in previous works.^{3 (link),4 (link)} More particularly,
its viscosity is well adapted for the preparation of formulations.
In addition, interestingly, Mix-MA is not too viscous. Therefore,
oxygen inhibition occurs, and only good-performance systems can polymerize
it. BlocBuilder-MA was obtained from Arkema. tert-Butylbenzene was obtained from Sigma-Aldrich.

Bonardi A.H., Dumur F., Gigmes D., Xu Y.Y, & Lalevée J. (2020). Light-Induced Thermal Decomposition of Alkoxyamines upon Infrared CO2 Laser: Toward Spatially Controlled Polymerization of Methacrylates in Laser Write Experiments. ACS Omega, 5(6), 3043-3046.

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Carbonyl Compound Quantification Protocol

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Acetonitrile (ACN) and hydrochloric acid (12 N HCl) were purchased from Fisher Scientific (Pittsburgh, PA) and used as received. 2,4-Dinitrophenylhydrazine (DNPH) was purchased from BOC Sciences (Shirley, NY) and recrystallized before use to remove water as previously reported.^{31 (link)} Diglyme, phenyl-N-tert-butylnitrone (PBN), 2,2,6,6-tetramethyl-1-piperidinyloxyl (TEMPO), hexane, heptadecane, tertbutylbenzene, and dinitrophenylhydrazones of formaldehyde, acetaldehyde, acrolein, acetone, crotonaldehyde, propionaldehyde, and methyl ethyl ketone (MEK) were all purchased from Sigma-Aldrich (St. Louis, MO) and used as received.

Bitzer Z.T., Goel R., Reilly S.M., Bhangu G., Trushin N., Foulds J., Muscat J, & Richie JP J.r. (2018). Emissions of free radicals, carbonyls, and nicotine from the NIDA Standardized Research Electronic Cigarette and comparison to similar commercial devices. Chemical research in toxicology, 32(1), 130-138.

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