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Anhydrous isopropyl alcohol

Manufactured by Merck Group

Anhydrous isopropyl alcohol is a clear, colorless, volatile liquid. It is a high-purity solvent used in various laboratory applications. The product's core function is to provide a reliable, consistent, and contaminant-free solvent for experimental and analytical procedures.

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3 protocols using anhydrous isopropyl alcohol

1

Perovskite Solar Cell Fabrication

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Nickel(II) nitrate hexahydrate (Ni(NO3)2·6H2O, 99.999%), anhydrous dimethyl sulfoxide (CH3)2SO, DMSO, 99.9%), N,N-dimethylformamide (HCON(CH3)2, DMF, 99.8%), anhydrous mono chlorobenzene (C6H5Cl, CB, 99.8%), and anhydrous isopropyl alcohol ((CH3)2CHOH, IPA, 99.7%) were purchased from Sigma-Aldrich Korea (Seoul, Republic of Korea) PMMA ((C5O2H8)n, 950,000 Mw) was purchased from Kayaku Advanced Materials (Westborough, MA, USA). Methyl ammonium iodide (CH3NH3I, MAI) and lead(II) iodide (PbI2, 99.9985%) for the perovskite precursor were purchased from Greatcell Solar (Queanbeyan, NSW, Australia) and Alfa Aesar (Haverhill, MA, USA), respectively. Ethylene glycol (HO(CH2)2OH, EG, 99%) and IPA for the nickel oxide (NiOx) precursor were purchased from Daejung Chemicals and Metals (Siheung, Republic of Korea). Phenyl-C61-buthyric acid methyl ester (C72H14O2, PCBM60) was purchased from Nano-C (Westwood, MA, USA). Bathocuproine (C26H20N2, BCP, 98%) and a colloidal suspension of ZnO nanoparticles were procured from Tokyo Chemical Industry Co. Ltd. (Tokyo, Japan) and Nanograde (Zurich, Switzerland), respectively. All materials were used as received without further purification.
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2

Fabrication of High-Efficiency Perovskite Solar Cells

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Titanium diisopropoxide
bis(acetylacetonate), acetylacetone, anhydrous isopropyl alcohol,
4-tert-butylpyridine (TBP), LiClO4 (99.90%),
and anhydrous acetonitrile (ref. 271004, 99.80%) were purchased from
Sigma-Aldrich and used without additional purification. Screen-printable
TiO2 pastes (30NR-D, WER2-O) and FTO-coated glasses (7
Ω/sq) were from GreatCell Solar. Screen-printable glass paste
to produce glass frit for the device sealing was based on Bi and Zn
oxides. The thermoplastic sealant (Meltonix 1170–60, 60 μm
Surlyn) and the screen-printable graphite/carbon-black paste (Elcocarb
B/SP) were acquired from Solaronix. Complexes Co(III/II)tris(bipyridyl)tetracyanoborate
(Eversolar Co-300 and Co-200) were from Everlight and Y123 organic
sensitizer was ordered from Dyenamo. Titanium tetrachloride (99.90%)
and t-butanol (99.5%) were purchased from Acros Organics.
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3

Solvent Purification and Reagent Preparation

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All reaction solvents were purified using a Seca solvent purification system by Glass Contour, with the exception of methanol, iso-propyl alcohol, and tert-butyl alcohol. Methanol was purified by distillation over magnesium, and anhydrous iso-propyl alcohol, tert-butyl alcohol, and 1,4-dioxane were purchased from Sigma-Aldrich and used as received. N,N-dicyclohexylamine, 2,2,6,6-tetramethylpiperidine, and DMPU were distilled over CaH2. n-butyllithium (in hexanes) was purchased from Sigma-Aldrich. The molarity of n-butyllithium solutions were determined by titration with N-benzylbenzamide. All other reagents were used as received without further purification, unless otherwise stated.
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