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2 protocols using tri methoxysilyl propyl methacrylate

1

Thermoplastic Fiber Braiding Optimization

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The methodology of the current study was carried out through two stages. The first stage was for testing different percentage combinations of glass fiber/PP (GF/PP) thermoplastic fibers braiding. Materials specification of this stage are mentioned in Table 1. Three main materials categories were used: E-GF treated with starch (ECE225, and count of “22 Tex”) and thermoplastic yarns of polypropylene (PP) with a count of 300 denier, all of which were donated by AGY industries, located in the Aiken, SC, USA. The third category was two types of chemical agents for better coupling and adhesion between two matrices as: Maleic anhydride powder with 99% concentration and tri-methoxysilyl propyl methacrylate with 98% concentration, both purchased from Sigma Aldrich, Steinheim am Albuch, Baden-Württemberg, (Germany), for treating PP yarns and GF surfaces, respectively.
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2

Synthesis and Characterization of Graphene-Reinforced Polymeric Biomaterials

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Materials: Trimethylene carbonate (1,3-dioxane-2-one, TMC) was obtained from ForYou Medical (China) and used as received. Graphite powder was obtained from Bay Carbon. N,Ndimethylformamide (DMF), trimethylamine (TEA), phosphorus pentoxide (P2O5), trimethoxysilylpropylmethacrylate, hydrazine monohydrate (N2H4 64-65 %, reagent grade, 98%), ethylene carbonate, trimethylolpropane, stannous octoate (Sn(Oct)2), hydroquinone, methacrylic anhydride and triethylamine were sourced from Sigma-Aldrich. Chloroform, potassium persulfate (K2S2O8) and potassium permanganate (KMnO4) were obtained from Chem-Supply. Sulphuric acid (H2SO4) and 30% hydrogen peroxide (H2O2) were purchased from Ajax Finechem. 1-[4-(2-hydroxyethoxy) phenyl]-2-hydroxy-2-methyl-1-propane-1-one (Irgacure 2959) was purchased from Ciba (Ciba®, Switzerland). Dichloromethane (>99.5%) was purchased from VWR chemicals, Belgium. Milli-Q water with a resistivity of 18.2 mΩ cm -1 was used in all preparations.
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