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Tri n propylamine

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Tri-n-propylamine is a clear, colorless liquid chemical compound. It is used as a reagent and intermediate in various organic synthesis and pharmaceutical applications. The core function of tri-n-propylamine is to serve as a base, a nucleophile, and a catalyst in chemical reactions.

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Lab products found in correlation

Phosphoric acid, by Merck Group (1 mentions) Sodium phosphate monobasic dihydrate, by Merck Group (1 mentions) Sodium phosphate dibasic, by Merck Group (1 mentions) Toluene, by Merck Group (1 mentions) Tetrapropylammonium bromide, by Merck Group (1 mentions) 1 3 5 triisopropylbenzene, by Merck Group (1 mentions) 1 bromohexadecane, by Merck Group (1 mentions) Milli q gradient water purification system, by Merck Group (1 mentions) Resorufin, by Merck Group (1 mentions) Hexaammineruthenium 3 chloride, by Merck Group (1 mentions) Ferrocene methanol, by Merck Group (1 mentions) Vanillic acid, by Merck Group (1 mentions) P coumaric acid, by Merck Group (1 mentions) Ethanol, by Merck Group (1 mentions) Triton x 100, by Merck Group (1 mentions) Dimethyl sulfoxide (dmso), by Merck Group (1 mentions) N n dimethylformamide (dmf), by Merck Group (1 mentions) Tetrabutylammonium tetrafluoroborate, by Merck Group (1 mentions) Sulfuric acid, by Merck Group (1 mentions) Potassium ferricyanide, by Merck Group (1 mentions)

Spelling variants of this product

Propylamine (25 citations) N-propylamine (12 citations)

7 protocols using tri n propylamine

1

Photocatalytic Polymerization Reagents

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Tri-n-propylamine (TPrA, MW = 143.27 g mol−1, ≥98% v/v), sodium phosphate monobasic dihydrate (NaH2PO4·2H2O, MW = 156.01 g mol−1, ≥99%), sodium phosphate dibasic (Na2HPO4, MW = 141.96 g mol−1, ≥99.5%) and phosphoric acid (H3PO4, MW = 98.00 g mol−1, ≥85%) were purchased from Sigma-Aldrich. 2.8 μm polystyrene magnetic beads covalently linked to [Ru(bpy)3]2+ were purchased from Roche Diagnostics. Na3[Ir(sppy)3] was purchased from Luminescence Technology Corp. while [Ir(dfppy)2(pt-TEG)]Cl and [Ir(bt)2(pt-TEG)]Cl were synthesised as reported in literature.13 (link)
Fracassa A., Santo C.I., Kerr E., Knežević S., Hayne D.J., Francis P.S., Kanoufi F., Sojic N., Paolucci F, & Valenti G. (2023). Redox-mediated electrochemiluminescence enhancement for bead-based immunoassay. Chemical Science, 15(3), 1150-1158.
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2

Synthesis and Catalytic Evaluation of Mesoporous Materials

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For the preparation of the mesoporous materials, USY Zeolite (CBV780) was supplied by Zeolyst, with a nominal Si/Al ratio of 40, and tetrapropylammonium bromide 98% was purchased from Sigma-Aldrich (St. Louis, MO). Sodium hydroxide (98% pellets) was supplied by Fluka.
For the synthesis of the quaternary ammonium bromide surfactant with the tripropyl head, tri-n-propylamine and 1-bromohexadecane both from Sigma-Aldrich were employed.
For the catalytic evaluation, 1,3,5-triisopropylbenzene (C15H24, 95%, Sigma-Aldrich) was used as feed stock. The chemicals used for GC calibration are:

From Sigma-Aldrich: Benzene (C6H6, ≥ 99.8%), toluene (C6H5CH3, ≥ 99.5%), para-xylene (C6H4(CH3)2, ≥99.5% GC), ortho-xylene (C6H4(CH3)2, ≥99.5% GC), meta-xylene (C6H4(CH3)2, ≥99.5% GC), 1,2,3-trimethylbenzene (C6H3(CH3)3, ≥99.5%, neat, GC), 1,2,4-trimethylbenzene (C6H3(CH3)3, 98%) and, 1,3-diisopropylbenzene (C12H18, 96%).

From Alfa Aesar: cumene (C9H12, 99%) and, 1,4-diisopropylbenzene (C12H18, 99%).

Mendoza-Castro M.J., Qie Z., Fan X., Linares N, & García-Martínez J. (2023). Tunable hybrid zeolites prepared by partial interconversion. Nature Communications, 14, 1256.
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3

Electrochemical Characterization of Ruthenium Complexes

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All chemicals, including hexaammineruthenium(iii) chloride (Ru(NH3)6Cl3), tris(2,2′-bipyridyl) dichlororuthenium(ii) hexahydrate (Ru(bpy)3Cl2), tri-n-propylamine, resorufin, ferrocenemethanol, glucose, and underivatized polystyrene spheres (1.0 μm in diameter, 10 wt%), were obtained from Sigma-Aldrich and used as received. All solutions for electrochemical measurements were prepared from deionized (DI) water (ρ ∼ 18 MΩ cm) generated by a Milli-Q Gradient water purification system (Millipore).
Ma C., Zaino III L.P, & Bohn P.W. (2015). Self-induced redox cycling coupled luminescence on nanopore recessed disk-multiscale bipolar electrodes †Electronic supplementary information (ESI) available. See DOI: 10.1039/c5sc00433k Click here for additional data file.. Chemical Science, 6(5), 3173-3179.
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4

Photochemical Ruthenium Redox Reactions

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The chemical used in all experiments in this work were: tris (2,2′‐bipyridyl) dichlororuthenium(II) hexahydrate (Ru(bpy)3Cl2 ⋅ 6H2O), tri‐n‐propylamine (TPrA), phosphate buffer solutions (PBS), vanillic acid, p‐coumaric acid and ethanol (all purchased from Sigma Aldrich, St. Louis, MO, USA); and Milli‐Q water purchased from APS Water Services Corp., Van Nuys, CA, USA (resistivity ≥18.2 MΩ ⋅ cm). All these chemicals were used as received.
Rivera E.C., Taylor J.W., Summerscales R.L, & Kwon H.J. (2021). Quenching Behavior of the Electrochemiluminescence of Ru(bpy)3 2+/TPrA System by Phenols on a Smartphone‐Based Sensor. ChemistryOpen, 10(8), 842-847.
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5

Antibody Epitope Mapping and Functionalization

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MAb228
(epitope region 26–35) and
MAb19c7 (epitope region 41–49) were purchased from HyTest Company.
The novel antibody, mAb20B3 (epitope 24–39, NYRAYATEPHAKKKSKI),
was custom-generated “in house”. 1-Ethyl-3-[3-dimethylaminopropyl]
carbodiimide hydrochloride (EDC), sulfo-N-hydroxysuccinimide
(NHS), DPBS, 16-MHDA, dimethylsulfoxide (DMSO), N,N-dimethylformamide, tetrabutylammonium tetrafluoroborate,
tri-n-propylamine, and Triton X-100 were purchased
from Sigma-Aldrich and used as received. Ir(6-phenylphenanthridine)2 2-(carboxyethyl-phenyl)pyridine-2-carboxylic acid (Ir–COOH)
was synthesized, as reported elsewhere.53 (link)
Spain E., Carrara S., Adamson K., Ma H., O’Kennedy R., De Cola L, & Forster R.J. (2018). Cardiac Troponin I: Ultrasensitive Detection Using Faradaic Electrochemical Impedance. ACS Omega, 3(12), 17116-17124.
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6

Fabrication of Electrochemical Biosensors

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Clear resin was obtained from Formlabs (Somerville, MA). Pencil graphite (0.5 mm dia., Super Hi-Polymer HB) was supplied by Pentel (Torrance, CA). Au (0.1 mm and 0.5 mm dia.) and Ag (0.5 mm dia.) wires as well as potassium ferricyanide, tris(2,2′-bipyridyl)dichlororuthenium(II) hexahydrate, tri-n-propylamine, salmon testes (ST) ds-DNA (2000 base pairs avg, 41.2% G/C), poly(diallyldimethylammonium chloride (PDDA), sodium phosphate dibasic, and sulfuric acid (98.0%) were obtained from Sigma-Aldrich (St. Louis, MO). NaCl and KCl, were purchased from J.T. Baker (Center Valley, PA). Potassium phosphate monobasic was obtained from Fisher Scientific (Pittsburgh, PA). All solutions were prepared using 18 MΩ·cm water purified by passing house-distilled water through a Hydro Service and Supplies purification system (Durham, NC).
Bishop G.W., Satterwhite-Warden J.E., Bist I., Chen E, & Rusling J.F. (2015). Electrochemiluminescence at Bare and DNA-Coated Graphite Electrodes in 3D-Printed Fluidic Devices. ACS sensors, 1(2), 197-202.
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7

Electrochemical Analysis of Redox Probes

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Methanol (MS grade), triethanolamine (98%), tri-n-propylamine (98%), 2-(dibutylamino)ethanol (99%), tris(2,2′-bipyridine)ruthenium(ii) dichloride hexahydrate and 5,5-dimethyl-1-pyrroline N-oxide (98%) were purchased from Sigma Aldrich (Darmstadt, Germany). PBS buffer solution (pH = 7.5) was purchased from Aladdin (Shanghai, China). The glassy carbon (GC) disk electrode (diameter 0.3 mm), platinum (Pt) plate and Ag/AgCl reference electrode were from Gaoss Union (Wuhan, China). Ultrapure water was produced by using a Milli-Q water purification system (Milford, MA). The solvent was bubbled with pure nitrogen for one hour to deoxygenate and all sample solutions were used immediately after preparation.
Liu J., Yu K., Zhang H., He J., Jiang J, & Luo H. (2021). Mass spectrometric detection of fleeting neutral intermediates generated in electrochemical reactions. Chemical Science, 12(27), 9494-9499.
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