X-ray photoelectron spectroscopy (XPS) was used to analyze the surface chemistry of the coated BNC grafts [39 (link)]. Therefore, rectangular samples (0.5 × 0.5 cm) were cut from coated BNC grafts and freeze dried. Then, the samples were analyzed by XPS using a PHI 5600 ESCA System (Physical Electronics Inc., Division of ULVAC-PHI, 18,725 Lake Drive East in Chanhassen, MN 55317, USA), equipped with a Spherical Capacitor electron energy Analyzer (energy resolution 25 meV, PHI 5600 ESCA System) and a Dual Anode X-ray Source operating with Mg K-alpha at 14 kV and 400 W. The analyzed lateral area had a diameter of 800 µm, using a detection angle (Source to SCA) of 54°. To define the atomic concentration of the analyzed elements, multiplex spectra were measured for each sample.
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