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Asap 2010

Manufactured by M&M Mass Spec Consulting
Sourced in United States

The ASAP 2010 is a mass spectrometer designed for rapid sample analysis. It is a compact, benchtop instrument that utilizes atmospheric pressure ionization techniques to ionize and detect a wide range of chemical compounds. The ASAP 2010 provides accurate mass measurements and can be used for qualitative and quantitative analysis of various sample types.

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4 protocols using asap 2010

1

Comprehensive Characterization of Material

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Scanning electron microscope (SEM) and transmission electron microscope (TEM) testing were performed on a JSM-6610 and a JEM-2010 electron microscope, respectively. X ray diffraction (XRD) measurements were carried out on a XRD-7000 X-ray diffractometer using Cu Kα radiation at λ = 0.154 nm. The thermal stability was measured with a NETZSCH 409PC in dry air. The specific surface area and pore-size distribution were determined by the Brunauer–Emmett–Teller (BET) measurement by employing an ASAP-2010 surface area analyser. Raman spectra were collected by an Invia Refl (Renishaw, UK) under ambient conditions, from 2000 to 400 cm–1 with 532.8 nm laser light. X-ray photoelectron spectroscopy (XPS) characterization was carried out in an ESCALAB 250Xi electron spectrometer.
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2

Characterization and Suspension of MgONPs

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The MgONPs were purchased from Sigma-Aldrich. These particles were distributed in deionized water and poured into a matrix potting medium (Pindstrup Mosebrug A/S, Shanghai, China) to conduct the plant experiment. The practical size of the particles was characterized using TEM (JEM-2100, JEOL, Tokyo, Japan) and SEM (S-570, Hitachi, Tokyo, Japan), and the particles were characterized in detail as described in our previous study [13 (link)]. The nitrogen adsorption–desorption isotherms of the MgONPs were evaluated using a Micromeritics Analyzer (ASAP 2010, Norcross, GA, USA) with nitrogen. The zeta potential of the MgONP in the matrix extraction was evaluated using a Malvern Zetasizer Nano Series (Malvern, UK). The matrix was suspended in deionized water to filtrate until the large particle residue was removed to obtain the matrix extraction. The MgONPs were suspended in deionized water to obtain the final suspension concentration of 250, 150 and 50 μg/mL and sonicated for 30 min for experimental use.
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3

Characterization of Aluminosilicate Catalysts

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Recording of the Powder X-ray diffraction (XRD) patterns was carried out with a Shimadzu Lab XRD-6000 X-ray Diffractometer using nickel-filtered Cu Kα radiation. Determination of the Si/Al ratio was performed with the use of inductively coupled plasma (ICP) on a Thermo IRIS Intrepid ⅡXSP atomic emission spectrometer that followed the dissolution of the specimens in HF solution. N2 was put to use as an adsorbate in an ASAP 2010 system of Micromeritics under liquid-N2 temperature for the purpose of measuring the samples' areas of BET particular surface. NH3-TPD analysis was carried out on a self-developed tool. The measurement mechanism was carried out in accordance with the former literature reports [12] . Pyridine adsorption fourier transform infrared (FTIR) spectrum was attained in accordance with the literature as well [13] . Testing of the TG-DSC profiles was carried out on TG-8120 tool, in an air stream at a heating rate of 20 K min-1 from 306 to 1073 K.
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4

Porous Adsorbent Material Characterization

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These analyses included the measure of the specific area, the volume and the average size of the adsorbent pores, by the BJH method. These parameters were determined by nitrogen adsorption-desorption (at 77 K) using an ASAP 2010 Micromeritics apparatus. The dry samples were degassed under vacuum condition (50 mtorr) at 300 °C for 1 h. Then the specific area was obtained by using the Brunnauer, Emmet and Teller (BET) protocol.
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