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3 aminopropyl triethoxysilane

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(3-aminopropyl)triethoxysilane is a silane coupling agent. It is a colorless, clear liquid with a slight amine odor. The compound contains three ethoxy groups and an aminopropyl functional group, which allows it to react with both inorganic and organic materials.

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Lab products found in correlation

Ethanolamine, by Xilong (3 mentions) Acetic anhydride, by Xilong (3 mentions) Tetraethyl orthosilicate, by Maclin Biochemical Technology (2 mentions) Sodium chloride (nacl), by Maclin Biochemical Technology (1 mentions) Ammonium hydroxide solution, by Maclin Biochemical Technology (1 mentions) Triethylamine, by Maclin Biochemical Technology (1 mentions) Citric acid, by Maclin Biochemical Technology (1 mentions) Formamide, by Maclin Biochemical Technology (1 mentions) Acridine orange, by Maclin Biochemical Technology (1 mentions) Anhydrous ethanol, by Sinopharm (1 mentions) N 3 dimethylaminopropyl n ethylcarbodiimide hydrochloride, by Maclin Biochemical Technology (1 mentions) N hydroxysuccinimide, by Maclin Biochemical Technology (1 mentions) Toluene, by Sinopharm (1 mentions) Methanol, by Sinopharm (1 mentions) Acetone, by Sinopharm (1 mentions) Sodium dodecyl sulfate (sds), by Maclin Biochemical Technology (1 mentions) Fluorescein isothiocyanate isomer, by Merck Group (1 mentions) Simvastatin, by Merck Group (1 mentions) Resazurin, by Merck Group (1 mentions) Cetyltrimethylammonium bromide, by Maclin Biochemical Technology (1 mentions)

8 protocols using 3 aminopropyl triethoxysilane

1

Facile Synthesis of Fluorescent Silica Nanoparticles

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Citric acid
(C6H8O7, AR grade), formamide (CH3NO, AR grade), acridine orange (C17H19N3, biotechnology grade), tetraethyl orthosilicate (C8H20O4Si, GC grade), ammonium hydroxide
solution (NH3·H2O, AR grade), triethylamine
(C6H15N, AR grade), glutaric anhydride (C5H6O3, 98%), sodium chloride (NaCl, AR
grade), (3-aminopropyl)triethoxysilane (C9H23NO3Si, 99%), N-(3-dimethylaminopropyl)-N′-ethylcarbodiimide hydrochloride (C8H17N3·HCl, 98.5%), and N-hydroxysuccinimide (C4H5NO3, 99%)
were purchased from Shanghai Macklin Biochemical Co., Ltd. Ethanol
anhydrous (C2H6O, AR grade), methanol (CH4O, AR grade), acetone (C3H6O, AR grade),
and toluene (C7H8, AR grade) were purchased
from Sinopharm Chemical Reagent Co., Ltd. The other reagents used
were of AR grade without further purification, and ultrapure water
was used in all experiments. The miR-92a-3p, DNA probe, amino-modified
DNA (NH2-DNA) probe, and unmatched targets were purchased
from Shanghai Genepharma Co., Ltd. Their sequences are listed in Table S1 of the Supporting Information. The human
serum was isolated from the healthy sample from the Second Hospital
of Shandong University. The apparatus used are given in the Supporting Information.
Sun Z., Tong Y., Zhou X., Li J., Zhao L., Li H., Wang C., Du L, & Jiang Y. (2021). Ratiometric Fluorescent Biosensor Based on Forster Resonance Energy Transfer between Carbon Dots and Acridine Orange for miRNA Analysis. ACS Omega, 6(49), 34150-34159.
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2

Gadolinium-Doped Silica Nanoparticles Synthesis

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Hexadecyl trimethyl ammonium bromide (CTAB, 99%) was purchased from Coolaber Science & Technology. Tetraethoxysilane (TEOS, 99%) was purchased from Fuchen Chemical Reagents (Tianjin, China). 3-Aminopropyl-triethoxysilane (99%) was purchased from Macklin Biochemical Co., Ltd. (Shanghai, China). Gadolinium (III) chloride hexahydrate (GdCl3·6H2O, 99.9%) was purchased from Aladdin Biochemical Technology Co., Ltd. (Shanghai China).
Li Z., Guo J., Zhang M., Li G, & Hao L. (2022). Gadolinium-Coated Mesoporous Silica Nanoparticle for Magnetic Resonance Imaging. Frontiers in Chemistry, 10, 837032.
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3

Multifunctional Nanocarriers for Targeted Drug Delivery

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All reagents were of analytical or HPLC grade and used without any further purification. Tetraethyl orthosilicate (TEOS), cetyl trimethyl ammonium bromide (CTAB), branched polyethyleneimine (PEI) (Mw = 10 kDa), (3-aminopropyl) triethoxysilane (APTES), and sodium dodecyl sulfate (SDS) were purchased from Macklin. Co., Ltd. Fluorescein isothiocyanate isomer (FITC), Simvastatin (SIM), hyaluronidase (HAase), N-hydroxy succinimide (NHS), 1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (EDC), Resazurin, 4,6-diamidino-2-phenylindole (DAPI), and lipopolysaccharide (LPS) were purchased from Sigma-Aldrich Inc. (St. Louis, MO, USA). Sodium hyaluronate (HA) (Mw = 200~400 kDa) was purchased from Bloomage Biotechnology Co., Ltd. (Jinan, China). Oxidized low-density lipoprotein (ox-LDL) was purchased from Yiyuan Biotechnology Co., Ltd. (Bozhou, China). Phosphate buffer tablets were purchased from Amresco Inc. (Cleveland, OH, USA). The mouse ELISA kits to measure the secretion of tumor necrosis factor-α (TNF-α) and interleukin-6 (IL-6) levels were purchased from Beyotime Biotechnology Co., Ltd. (Shanghai, China).
Song K., Tang Z., Song Z., Meng S., Yang X., Guo H., Zhu Y, & Wang X. (2022). Hyaluronic Acid-Functionalized Mesoporous Silica Nanoparticles Loading Simvastatin for Targeted Therapy of Atherosclerosis. Pharmaceutics, 14(6), 1265.
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4

Synthesis of Multifunctional Nanoparticles

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Sodium salicylate (NaSal), triethanolamine (TEA), Tetraethyl orthosilicate (TEOS), cetyltrimethylammonium bromide (CTAB), (3-Aminopropyl) triethoxysilane, iron chloride (FeCl3·6H2O), oleyl alcohol, sodium oleate, HAuCl4·4H2O, diphenyl ether, sodium phosphate dibasic (Na2HPO4), and acetic acid were obtained from Macklin Biochemical Co, Ltd (Shanghai, Chain). Acetone, n-hexane and ethanol were purchased from Fuchen Chemical Reagent Co, Ltd (Tianjin, China). 3,3′,5,5′-tetramethylbenzidine (TMB) was obtained from Aladdin Co, Ltd (Shanghai, China). Hydrochloric acid (HCl), glucose, and H2O2 were ordered from Sinopharm Chemical Reagent Co, Ltd (Shanghai, China). Fluorescein isothiocyanate (FITC) and Methoxy PEG-thiol (mPEG-SH, Mw ​= ​5000) were obtained from xi'an ruixi Biological Technology Co, Ltd (xi'an, Chain). Dimethyl sulfoxide (DMSO) was from Merck Co. Inc. (Germany).
Mao H., Wen Y., Yu Y., Li H., Wang J, & Sun B. (2022). Ignored role of polyphenol in boosting reactive oxygen species generation for polyphenol/chemodynamic combination therapy. Materials Today Bio, 16, 100436.
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5

Captan-based Silica Nanoparticle Synthesis

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Tianjin
Sinos Biochemical
Technology Co., Ltd. supplied captan (97%). Hebei Guanlong Agrochemical
Co., Ltd. supplied captan wettable powder (50%). Shanghai Macklin
Biochemical Co., Ltd. provided (3-aminopropyl)triethoxysilane (APTES)
(98%) and tetraethyl orthosilicate (TEOS) (98%). Sigma-Aldrich Co.
LLC provided 1-(3-(dimethylamino)propyl)-3-ethylcarbodiimide hydrochloride
(EDC) (98%), N,N-dimethylformamide (99.5%), β-glucanase
enzyme (β-glucanase activity of 1 unit may liberate 1.0 M glucose
in 1.0 h), and 2000 MWCO (D2272) dialysis tubing. β-Glucan (70%)
(molecular weight 2.4 × 106 Da), N-hydroxysuccinimide (NHS) (98%), sodium chloroacetate (98%), isopropyl
alcohol (99.5%), and hexadecyltrimethylammonium bromide (CTAB) (99%)
were purchased from Shanghai Aladdin Bio-Chem Technology Co., Ltd.
Tianjin Fuyu Fine Chemical Co., Ltd. provided ethanol (99.7%) and
acetone (99.5%). Guangzhou Chemical Reagent Factory provided the toluene
(99.5%). To create filtered water, a purification system (Likang Biomedical
Technology Holdings Co., Ltd., Taiwan, China) was utilized.
Kaziem A.E., Yang L., Lin Y., Xu H, & Zhang Z. (2022). β-Glucan-Functionalized Mesoporous Silica Nanoparticles for Smart Control of Fungicide Release and Translocation in Plants. ACS Omega, 7(17), 14807-14819.
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6

Bagasse-Based Composite Material Synthesis

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Bagasse was purchased from Guangxi, China (bagasse cellulose content of 80.62 wt%; water content of 10 wt% after pre-treatment). CaCl2 and (NH4)2CO3 purchased from Chengdu Kelong Chemical Co., Ltd. (Chengdu, Sichuan Province, China), both of which are of analytical grade, were utilized as received with no further purification. Ethanolamine and triEthanolamine were purchased from Xilong Science Co., Ltd. (Shantou, Guangdong Province, China), both of which are of analytical grade. 3-aminopropyltriethoxysilane, potassium persulfate (APS), acrylamide (AM), and N,N′-methylene bisacrylamide (MBA) were purchased from Macklin (Shanghai, China), and all chemical reagents utilized in this study were of analytical grade and were utilized as received with no further purification.
Xie X., Ma L., Chen Y., Luo X., Long M., Ji H, & Chen J. (2022). Bagasse Cellulose Composite Superabsorbent Material with Double-Crosslinking Network Using Chemical Modified Nano-CaCO3 Reinforcing Strategy. Nanomaterials, 12(9), 1459.
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7

Superhydrophobic PVA Sponge Fabrication

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The
PVA sponge was purchased
from a local supermarket. 3-Aminopropyltriethoxysilane (KH550, 99%),
CCl4 (98%), and boric acid (H3BO3, 99.5%) were received from Shanghai Macklin Biochemical Co., Ltd.
FDTS and Brilliant Green (CAS: 633-03-4) were purchased from Shanghai
Aladdin BioChem Technology Co., Ltd. n-Hexane (99.5%)
was purchased from Shandong Xiya Chemical Industry Co., Ltd. Sudan
I (CAS: 842-07-9) was bought from Sinopharm Chemical Reagent Co.,
Ltd. TiO2 nanoparticles (CAS: 13463-67-7) were provided
by Hangzhou Hengna New Materials Co., Ltd. Sodium hydroxide (NaOH,
96%) was purchased from Hangzhou Gaojing Fine Chemicals Co., Ltd.
He Z., Wu H., Shi Z., Kong Z., Ma S., Sun Y, & Liu X. (2022). Facile Preparation of Robust Superhydrophobic/Superoleophilic TiO2-Decorated Polyvinyl Alcohol Sponge for Efficient Oil/Water Separation. ACS Omega, 7(8), 7084-7095.
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8

Coir Fiber Reinforced Epoxy Composites

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The coir fibers used in the experiment were obtained from coconuts grown in Hainan Province, China. The epoxy resin E-44 used to make the matrix for the pullout specimens was purchased from Guangdong Province, China, with a density of 1150 kg/m3, a viscosity of 5000–6000 mPa·s, an epoxy value of 0.41–0.47 eq./100 g and a melting point of 145–155 °C. The chemicals used in this experiment have analytical purity, and included the following: sodium hydroxide (NaOH) (MACKLIN, Shanghai, China), ethanol anhydrous (MACKLIN, Shanghai, China), acetic anhydride (XILONG SCIENTIFIC, Shantou, China), and 3-aminopropyltriethoxysilane (MACKLIN, Shanghai, China).
Ru S., Zhao C., Yang S, & Liang D. (2022). Effect of Coir Fiber Surface Treatment on Interfacial Properties of Reinforced Epoxy Resin Composites. Polymers, 14(17), 3488.
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